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研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c... 
2013-01-28 85 5.8

研究了退火温度和退火时间对电沉积硅钢试样中的断面层组织、硅在试样中的分布情况、织构分布和磁性能的影响。结果表明:退火温度为1000℃、退火时间为210 min时得到的试样晶粒分布均匀、硅在试样中分布均匀、硅平均浓度为6.3715%(接近6.5%)。试样的织构分析及磁性能检测的结果表明,在较高温度下延长退火时间可增加{100}和{110}面织构,降低铁损,所得试样的磁性能较为良好。 The effect of annealing temperature and time on the microstructure, distribution of silicon,texture and magnetism of the high silicon steel prepared by electrodeposition was investigated. The results showed that after annealing at 1000℃ for 210 min, the mean grain size of steel was about 190 μm with a uniform grain size distribution, and the silicon is also uniformly distributed on the entire cross section with an average Si concentration 6.3715%(close to 6.5%); With the increasing annealing tim... 
2014-07-28 85 5.8

试验研究了球刻痕法对高磁感取向硅钢的铁损、矫顽力、相对磁导率、巴克豪森噪声等磁学性能的影响.研究结果表明:经过球刻痕处理后,高磁感取向硅钢的铁损明显降低,矫顽力下降,8 mm球刻痕过后铁损值与矫顽力分别下降16.2%和14.7%,且铁损和矫顽力均随刻痕间距降低而减少.刻痕后的高磁感取向硅钢磁导率在高磁感应强度下明显上升,刻痕后巴克豪森噪声值明显降低,经过对比分析确定8 mm为球刻痕的最佳刻痕间距.从磁畴观察、细化磁畴的原理等方面解释了细化磁畴对高磁感取向硅钢性能的影响原因. The effects of the ball scribing on magnetic properties of high permeability grain-oriented silicon steels,including the iron loss,coercive force,relative permeability,and Barkhausen noise were investigated. The results showed that the iron loss and coercive force of the high permeability grain-oriented silicon steels apparently decreased 16. 2% and 14. 7% respectively after 8 mm ball scribing and they both decreased with the decrease of the scribing spacing at the same magnetic flux density. At... 
2013-11-28 85 5.8

一种厚度≤0.15mm无取向硅钢带,其组分及wt%为:Si:2.0~6.5%,Mn:0.13~0.40%,S≤0.020%,P≤0.020%,Als:0.15~0.9%,C≤0.010%;工艺:经冶炼、浇注成坯后热轧至中间坯厚度;冷轧;常温脱脂;光亮罩式退火;经碱洗后涂覆;分条。本发明在保证铁损P1.0/400£13W/kg,磁感B2000³1.5T下,还使钢带厚度公差不超过±0.005mm,最小叠装系数³0.92完全满足连续冲制要求。
2021-11-15 85 6.8

本发明公开了一种自主学习的高硅钢软磁复合铁芯智能化生产系统及生产方法,属于软磁复合铁芯智能化生产技术领域。本发明的生产系统包括数据输入模块、数据分析模块、数据输出模块、通信模块、数据修正模块;生产方法为:用户通过输入模块选择目标性能参数及生产控制模式,系统生成生产过程关键参数,并由输出模块输出给用户;用户确认后形成控制指令,并发送至生产设备进行生产。本发明的系统不仅能够根据高硅钢铁芯产品的目标性能参数自动生成合理的操作条件,还能根据历史数据和产品检化结果对系统内置的关系模型不断进行优化、完善,能够有效提高产品产量和质量、减少浪费、降低成本。
2021-03-26 85 6.8

采用中、厚板坯生产技术对取向硅钢进行了研制和开发,对热轧及后工序样品进行了金相组织观察和EBSD分析,探讨了两种组织及织构的差异性,研究结果表明:除高温退火样品外,中板坯生产的取向硅钢各工序样品平均晶粒尺寸大;厚板坯生产的取向硅钢热轧和常化样品亚表层Goss织构强;中板坯和厚板坯的脱碳退火板织构没有明显区别。中板坯生产的取向硅钢成本低,产品磁性能和质量与厚板坯相当。 Grain oriented silicon steel was researched and developed by medium thickness slab and thick slab.Microstructures observation and EBSD analysis to the samples of hot rolling and following processes were carried out,respectively.The differences between the two kinds of microstructures and textures were discussed.The results show that the average grain sizes of every process samples are larger except that of high temperature annealing samples of grain oriented silicon steel produced by medium thic... 
2014-03-28 85 5.8

本发明涉及取向硅钢技术领域,且公开了包括以下步骤:步骤一:冶炼,冶炼经转炉和RH精炼后得到钢水,在进行冶炼的过程中通入空气并设置总进气量100‑300Nl/min,且通入的空气中氧含量为20‑21%之间。该磁性优良的高磁感取向硅钢的气氛控制工艺,通过在不同的流程中,加入一定配比的氧气和氮气的含量,有效的提升每个阶段的气氛控制精度,从而得到最终的高磁感取向硅钢达到优良,避免了因气压、流量等因素影响最终高磁感取向硅钢磁力效果,炉渣中FeO含量减少,提高钢回收率和炉衬寿命,进而也起到降低生产成本的效果,且进行精确的气氛控制,使得在进行高磁感取向硅钢的冶炼中,使得冶炼的效果更好,使得冶炼出来的高磁感取向硅钢的磁性更加的优良。
2020-12-14 85 6.8

研究了常化对CSP流程生产的wSi=1.6%的无取向电工钢组织、织构和成品磁性能的影响。结果表明,经CSP流程生产,且在相同的冷轧及退火制度下,经1 000℃×2min常化处理的wSi=1.6%的无取向电工钢热轧板,其最终退火成品的铁损P15/50比不常化试样下降了10.5%,磁感B50比不常化试样提高了2.5%;常化使wSi=1.6%的无取向电工钢成品的平均晶粒尺寸增大,成品铁损P15/50相应减小;同时,常化使wSi=1.6%的无取向电工钢成品中高斯织构的强度增加,γ纤维织构的强度减弱,这有利于成品磁感B50的提高。 The effect of normalizing on microstructure,texture and magnetic properties of non-oriented electrical steel with wSi=1.6% produced by CSP process was investigated.The results show that,under the same cold rolling and annealing system,the iron loss(P15/50) of annealed samples whose hot bands has been normalized by 1 000 ℃×2 min process decreases by 10.5% and magnetic induction(B50) increases by 2.5% compared with the samples whose hot bands was not normalized.The average grain size of non-orient... 
2012-11-28 85 5.8

本发明公开了一种提高薄板坯连铸生产高铝无取向硅钢可浇性的方法,在保证生产顺行、质量稳定的基础上,能使高铝无取向硅钢连浇炉数由10炉提高至16炉,在提高小时产量、降低生产成本方面效果显著。
2021-03-25 85 6.8

综述了国内外大钢铁企业与研究机构采用获得抑制剂法生产低温高磁感取向硅钢的开发及应用情况,分析了以该法生产高磁感取向硅钢过程中抑制剂的控制技术,包括固有抑制剂组成方案、气态渗氮方式与工艺及高温退火工艺的制定.研究表明,固有抑制剂组成方案的设计思路大体一致,化合物抑制剂以AlN为主、硫化物为辅,同时添加少量Sn,Sb等单元素抑制剂,但组成元素含量存在一定差别;在脱碳退火后用NH3进行非平衡渗氮处理已成为气态渗氮的主要方式,但最佳方式仍未明确,具体选择需依据实际生产条件,相应脱碳及渗氮工艺的控制条件差别较大;高温退火工艺中升温制度差别不大,升温阶段退火气氛中N2含量的选择存在差别.此外,分析了抑制剂控制技术目前存在的关键问题,并指出了进一步的研究方向. The current application and exploitation on production of low-temperature high magnetic induction grain-oriented silicon steel with acquired inhibitor method at both iron and steel enterprises and research institutions in the world are reviewed. The control techniques of inhibitors, which include the composition design for inherent inhibitors, nitriding method and process, and secondary recrystallization annealing, are thoroughly analyzed and proposed. It is indicated that the design ideas for i... 
2014-01-28 85 5.8

本实用新型公开了一种硅钢片绝缘测试装置,包括检测箱体、固定调节装置、探测装置和绝缘探测仪,所述固定调节装置、探测装置和绝缘探测仪设于检测箱体内,固定调节装置包括底座、支撑杆、放置板、夹板和夹持螺杆,所述支撑杆设于底座上,支撑杆上设有旋转腔,旋转腔内设有旋转电机,放置板旋转设于旋转腔上,旋转电机输出端设于放置板上,所述夹板滑动设于放置板两侧,夹持螺杆旋转设于放置板上;本实用新型属于绝缘测试领域,具体是一种通过固定调节装置可将硅钢片夹持固定,便于不同位置的调节,通过探测装置进行探测,并通过绝缘探测仪的检测于控制计算机将数据呈现和计算,减少手动操作,提高安全性的硅钢片绝缘测试装置。
2021-11-20 85 6.8

本发明属于冶金技术领域,涉及一种超短流程稀土取向硅钢及其制备方法,化学组成及其重量百分比为Si:2.0~4.5%,C:≤0.003%,Y:0.001~0.05%,Mn:0.15~0.35%,Al:0.03~0.04%,Cu:0~0.5%,S:0.025~0.04%,N:0.011~0.013%,其余为Fe和不可避免的杂质元素。制备工艺包括:钢水冶炼、薄带连铸、冷轧、再结晶退火。与常规生产方式相比,取消了连铸、粗轧、热连轧、常化和脱碳退火等工序,极大简化了生产流程。通过添加稀土元素钇,促进了抑制剂的析出,还显著细化了薄带连铸硅钢的凝固组织,提高组织均匀性,获得了均匀细小的等轴晶,优化了取向硅钢的性能。
2021-12-02 84 6.8

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