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借助高温激光共聚焦显微镜,在线观察了不同Mn含量的无取向硅钢中夹杂物的尺寸、类型、数量变化。结果表明,Mn含量(质量分数)为0.77%、0.32%时,试样中的夹杂物数量分别约为1000万个/mm3、1600万个/mm3。Mn含量较高的钢种,会优先析出球形、椭球形MnS夹杂物,其析出数量较少,尺寸相对较大,可以有效抑制AlN、CuxS夹杂物析出;Mn含量较低的钢种,会在试样再加热后冷却过程中,先析出相当数量MnS夹杂物,并作为AlN夹杂物析出核心,形成MnS+AlN复合夹杂物。这种复合夹杂物数量较多,尺寸也较大。 Based on the high temperature confocal microscope, the chage of size, type, and quantity of inclusions in non-oriented silicon steels with different Mn content were observed by in-situ SEM. Results show that the inclusion quantities are 10 million per mm3 and 16 million per mm3,while the mass fractions of Mn are 0.77% and 0.32%, respectively. In the silicon steel with higher Mn content, the spherical and ellipsoidal MnS inclusion will precipitate first, which can retard the precipitation of AlN ... 
2014-05-28 143 5.8

根据相关的取向电工钢典型专利技术,概述了日本高磁感低铁损取向电工钢低温板坯加热、抑制剂合理调节、关键成分Mn、C、Sn和Sb调节与利用、新型退火剂和绝缘溶液的制备及细化磁畴等生产工艺最新动态和进展情况,并提出了国内企业申请取向电工钢专利时应当借鉴之处。 According to related typical patent technology for grain-oriented electrical steel sheets,the recent trends and progress situation for production process of grain-oriented electrical steel sheets with high magnetic flux density and low core loss in Japan are summarized including low temperature slab heating,suitably regulating inhibitors,adjusting and utilizing key element Mn,C,Sn and Sb,manufacturing for new annealing agent and insulating solutions,and fining magnetic domain,and some suggestion... 
2011-02-28 143 5.8

本发明一种铝镇静含硅钢的脱氧方法,包括转炉冶炼、LF炉精炼工序,转炉工序:转炉出钢过程采用含硅脱氧剂进行脱氧,出钢完毕后,向钢液表面加入顶渣改质剂,数量为400±25kg/炉,所述顶渣改质剂的成分及其质量百分含量为:Al2O3:9%±1%,CaO:27.5%±1.5%,SiO2:3%±1%,Al:50%±2%,CaF2:7%±1%。精炼工序:采用铝脱氧剂进行脱氧、造渣。本发明通过两步脱氧工艺,大幅降低脱氧成本同时提高钢水质量,由于硅脱氧相对于铝脱氧在钢水中形成的夹杂物更容易上浮,所以也提高了钢水纯净度,提高钢水质量。
2021-04-07 143 6.8

通过测试取向硅钢不同工艺条件下的碳含量,探讨了CGO取向硅钢碳含量控制的最优处理条件,研究了脱碳温度和脱碳时间对相同初始碳含量取向硅钢的脱碳效果的影响。结果表明,在气氛为(15%~20%)H2+(75%~80%)N2,炉压差为10~20 Pa的条件下,CGO取向硅钢合适的脱碳温度为1 073 K~1 123 K,脱碳时间为10~20 min。在该处理条件下,能取得较好的脱碳效果。 By means of testing carbon content of oriented silicon steel below the distinct technical conditions,inquires the excellent handle terms of carbon content controlling for CGO oriented silicon steel,studies effects of decarburization annealing temperature and decarburization annealing time to the oriented silicon steel decarburization efficiency in same initial carbon content.The results show that,under the condition of atmosphere(15% ~ 20%) H2+(75% ~ 80%)N2 and furnace pressure difference 10 ~ 2... 
2013-03-28 143 5.8

本发明实施例公开了一种硅钢稀酸废水零排放处理方法和系统,所述方法包括:获得稀酸废水;对所述稀酸废水中的含硅固体杂质进行分离与回收,以获得稀酸废水净化液和含硅脱水泥饼;将所述稀酸废水净化液进行两级电吸附分盐处理,利用直流电场将稀酸废水中氯化亚铁组份浓缩分离,以获得分盐浓水和分盐淡水;将所述分盐浓水与酸再生工艺耦合,以获得再生盐酸;将所述分盐淡水调质再生处理,以获得铁系絮凝剂和再生工业净化水。所述硅钢稀酸废水零排放处理方法和系统,可以较低成本和能耗实现硅钢稀酸性废水全回用,真正实现废水零排放;可回收稀酸废水中的铁素和稀盐酸,不产生固体废物,可彻底实现废弃物资源化利用。
2020-12-16 143 6.8

通过固溶度积公式计算及热模拟实验,对不同热装和加热温度条件下的无取向硅钢铸坯中析出相进行了研究.在低于950℃热装时,铸坯中AlN的析出量和尺寸不再变化,但MnS和AlN-MnS的数量及平均尺寸随着热装温度降低而进一步增加,并在温度低于600℃时达到最大值后保持不变.与1200℃相比,1100℃加热的铸坯中AlN、MnS的总固溶量相对更少.相比850℃热装,600℃热装再加热到1100℃的铸坯中AlN和MnS的总固溶量更少,且AlN和MnS尺寸更大.合适的热装温度和加热温度分别为600℃和1100℃. Based on solubility product calculation and thermal simulation experiments,precipitated phases in continuous casting slabs of non-oriented silicon steel were systematically studied at different hot charging and heating temperatures.When the hot charging temperature is below 950 ℃,the content and size of AlN remain unchanged,but the quantity and size of MnS and AlN-MnS increase when the hot charging temperature decreases,reach maximum and remain unchanged when the hot charging temperature is belo... 
2013-08-28 143 5.8

本发明公开了一种宽频率低铁损无取向电工钢及其制备方法,属于无取向电工钢生产制造技术领域。它从电工钢表面向内依次包括0.005mm~0.1mm的渗透层和钢材内芯;所述渗透层是由硅原子向电工钢内渗透形成,渗透层中的硅元素含量为3wt%~8wt%;所述钢材内芯包括2.0wt%~5.5wt%的硅元素和不少于93.2wt%的铁元素。本发明能保证无取向电工钢具有低频低铁损性能同时有效降低高频条件下的铁损,具体铁损性能为:铁损P1.5/50≤2.35W/kg,铁损P1.0/400≤13.8W/kg。
2021-11-09 143 6.8

通过试验确定氩气分析流量为3.5L/min,静态流量为0.75L/min,冲洗时间为3s,预燃时间为12s,积分时间为5s的激发条件,采用火花源原子发射光谱法测定取向硅钢中碳、硅、锰、磷、硫。分别采用铣床铣样、砂轮磨样两种制样方式进行了精密度考察,发现制样方式对结果影响不大;讨论了取向硅钢样品中碳、硅、锰、磷、硫测定时可能存在的共存元素干扰,发现硅对锰元素的干扰不可忽略,采用干扰系数法进行了校正,据此拟合得到各元素校准曲线的相关系数均在0.999 0以上。精密度考察结果表明,碳、硅、锰、磷、硫的相对标准偏差(n=10)在0.71%~9.4%之间。对两块取向硅钢生产样品进行分析,并与钢铁研究总院进行比对分析,结果一致,且偏差均在允许范围内。 Carbon,silicon,manganese,phosphorus and sulfur in oriented silicon steel were determined by spark source atomic emission spectrometry.The selected excitation conditions were as follows:the analytical flow rate of argon was 3.5L/min,the static flow rate was 0.75L/min,the flush time was3s,the precombustion time was 12sand the integration time was 5s.Two sample preparation methods,including milling machine and grinding wheel,were investigated.The precision test results showed that,the determination... 
2013-10-28 143 5.8

研究二次冷轧压下率对于硅的质量分数为3.0%的无取向硅钢组织结构和磁性能的影响。结果表明:当第二次冷轧压下率从0变化至16.7%时,铁损逐渐增加,磁感逐渐降低。当第二次冷轧压下率大于16.7%时,随压下率的增加,铁损逐渐减小,磁感逐渐增加。当第二次冷轧压下率大于38%时,二次冷轧法所能获得的磁性能明显优于一次冷轧法。 Effect of double cold reduction on magnetic,microstructure and texture of 3.0% Si non-oriented silicon steel sheets was investigated.The results show that the iron loss increases and magnetic induction reduces as the percentage redcution in secondary cold rolling changes from 0 to 16.7%.The core loss can be reduced remarkably,and magnetic induction can get a little benefit if the percentage redcution in double cold reduction is higher 16.7%.In case of higher than 38% of the percentage redcution ... 
2012-11-28 143 5.8

本发明公开了一种适用于无取向硅钢极薄带表面涂覆的涂液,它由水溶性丙烯树脂、成膜助剂、耐盐雾助剂、流平剂、纳米氢氧化锆、消泡剂、水按质量比100:(2~8):(1~3):(1~5):(0~1):(0.1~0.5):(70~130)组成。将该涂液在无取向硅钢极薄带表面可表现出良好的涂覆性,经烘烤固化后形成的绝缘涂层表面透明光滑,附着性和绝缘性能优良,可有效提升无取向硅钢极薄带的综合性能,适合推广应用。
2021-09-30 143 6.8

通过对湿H2气氛下,相同退火温度、不同退火时间的CGO硅钢初次再结晶样品进行金相组织观察,并进行了EBSD微观织构分析,研究了CGO硅钢初次再结晶过程中的组织及再结晶织构演变行为。结果表明,在湿H2气氛下,820℃保温,CGO硅钢初次再结晶过程约在120 s时完成。随着退火时间的延长,γ面上{111}<112>织构含量逐渐减少,{111}<110>织构先减少后增多,随着再结晶的完成,部分{111}<112>取向晶粒向高斯{110}<001>取向转化的同时,也向{111}<110>取向转化,高斯{110}<001>织构含量逐渐增多。高斯取向晶粒较多是由{111}<112>取向晶粒转化而来,同时也证明了CGO硅钢高斯取向晶粒的二次再结晶异常长大生长机制为择优形核。 Microstructure development and texture evolution of conventional grain oriented silicon steel,which were annealed at same annealing temperature and different annealing time under wet H2 atmosphere,were investigated through metallographic observation and electron backscattered diffraction analyzing.The results show that the primary recrystallization finishes in 120 s at 820 ℃ under wet H2 atmosphere.With the extending of annealing time,{111}<112> texture decreases,{111}<110> texture d... 
2012-12-28 143 5.8

本实用新型公开了一种无取向硅钢的绝缘涂料喷涂装置,包括喷涂支架,所述喷涂支架安装有输送装置,所述喷涂支架的顶端侧壁水平方向固定有横向支撑板;本实用新型通过电机与第二行程开关接触启动工作,带动齿轮转动,驱动支撑杆左移,使喷涂喷头左移喷涂硅钢左端上表面,当电机接触到第一行程开关后,使电机工作带动齿轮反向转动,驱动支撑杆和喷涂喷头右移,在一定范围内,使喷涂喷头可以喷涂不同宽度的硅钢,通过施力转动螺杆,使螺杆左移、右移,使第一行程开关在水平方向移动,调节第一行程开关和第二行程开关之间的水平距离,从而调节喷涂喷头水平方向活动范围,根据硅钢宽度需求喷涂。
2021-11-23 142 6.8

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