硅钢资料

【机构】 武汉钢铁学院轧钢七二级电工钢结业小组； ...

一种提高有效氮和底层质量的高磁感取向硅钢制造方法：冶炼后连铸成坯；对铸坯加热；热轧、常化及酸洗后时效冷轧；在湿式气氛下脱碳退火；在湿式混合气氛下均热；在湿式混合气氛下渗氮退火；进行后工序。本发明与现有技术相比，通过合理控制渗氮过程，提高渗氮后钢板基体内氮含量与总氮量之间的比例达到80%以上，使无点状露晶产生，最终获得产品的底层质量优异。

分析了电感耦合等离子体发射光谱法(ICP-AES)测定硅钢中铌的检测过程,讨论了该检测过程中不确定度的主要来源,建立了该方法的定量的数学模型,并根据这一模型计算出了检测结果的合成标准不确定度和扩展不确定度。 The measurement of niobium content in silicon steel by inductively coupled plasma atomic emission spectrometry(ICP-AES) was analyzed,by which the main factors affecting the uncertainty of the measurement were ascertained and the calculation formula was given.Finally,according to the formula the combined uncertainty and expanded uncertainty were obtained. 

通过观察冲剪边缘组织,测量冲剪边缘的显微硬度、残余应力的分布情况和磁性能的变化研究了冲剪加工对无取向硅钢50WW800边缘组织和磁性能的影响。对冲剪后硅钢片进行750℃退火,分析退火对组织和磁性能的影响。结果表明,硅钢片剪切边缘会存在0.4 mm的形变硬化层,边缘应力大,铁损增加。退火后变形减小,形变硬化层变小,残余应力大幅度减少,铁损减少。 The influence of punching process on cutting edge microstructure and magnetic properties of non-oriented silicon steel 50WW800was studied by observing microstructure and measuring microhardness near cutting edge.The residual stress distribution in the silicon steel tooth and magnetic properties were measured.Effect of annealing at 750 ℃ on microstructure and magnetic properties of the silicon steel was analyzed.The results show that a cut-edge hardening layer up to 0.4 mm is observed,residual st... 

采用EBSD技术研究了有、无拉应力作用下无取向硅钢在晶粒长大过程中织构转变及晶界变化的规律。结果表明:在晶粒生长期间,无应力作用下的硅钢中,{111}〈112〉,{111}〈110〉织构组分强化,而{100}〈001〉织构组分弱化;与无拉应力作用下的情况相比,施加5MPa的拉应力时,{111}〈112〉,{111}〈110〉织构组分强化的速率下降,{100}〈001〉织构组分变化不明显。对于在晶粒生长期间持续变化的{111}〈112〉,{111}〈110〉和{100}〈001〉织构组分而言,虽然有、无拉应力作用下硅钢的{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率均下降,而{100}〈001〉织构组分的高取向差角度晶界频率则上升,但当有拉应力作用后,{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率下降的速率变小,{100}〈001〉织构组分的高取向差角度晶界频率上升的速率稍有变小。通过对无取向硅钢在晶粒长大过程中织构转变及晶界变化规律的研究,分析了合金原子在晶界的偏聚行为。 The rules of texture and grain boundary transformation in the nonoriented silicon steel under applied stress or without applied stress during grain growth were investigated by EBSD.The results show that the {111}〈112〉 and {111}〈110〉 components in the nonoriented silicon steel without stress are strengthened during grain growth whereas {100}〈001〉 component is weakened,but the growth rate of {111}〈112〉 and {111}〈110〉 component decreases,while the area fraction of {100}〈001〉 component doesn’t chang... 

【作者】 谌剑； ...

采用X-射线衍射分析技术测定了取向硅钢热轧板在不同压下率下不同厚度处的织构。结果表明,在压下率低于80%的情况下,几乎所有试样的不同厚度处的织构均为旋转立方织构类型{100}<011>,但不同压下率、不同厚度处的织构强度存在很大差异;在压下率大于80%的情况下,不同试样的不同厚度处的织构类型发生了变化,其织构类型为旋转立方织构或高斯织构{011}<100>,且当织构类型为旋转立方织构时,织构强度存在很大差异,而当织构类型为高斯织构时,织构强度差异相对较小。 The texture of the grain oriented silicon steel hot rolled plate at different compressibility has been measured.The experimental results have shown that the texture of all samples at different thickness is {100}<011> when the compressibility is below 80%,and its intensity at different compressibility and thickness is difference.The texture of all samples at different thickness is variable when the compressibility is above 80%,it is {100}<011> or {011}<100>,and the intensity of ... 

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

本发明公开了一种高磁感取向硅钢高效脱碳退火工艺，主要工艺流程为：炼钢连铸→热轧→酸洗常化→冷轧→脱碳和初次再结晶退火→渗氮处理(低温Hi‑B)→涂覆氧化镁隔离剂→高温退火→拉伸平整退火→涂覆绝缘涂层→精整，低温HiB不同于高温Hi‑B的工艺流程主要是在脱碳退火后增加了渗氮段。本发明在保证产品实物质量不低于现有水平(国内领先水平)的前提下，使Hi‑B钢退火效率达到世界领先，制造成本大幅降低。

【机构】 武钢研究院； ...

一种取向硅钢环形炉钢卷冷却装置，涉及冶金领域。该取向硅钢环形炉钢卷冷却装置用于控制环形炉的冷却一段内钢卷的冷却速度，其包括设于冷却一段的炉体内耐火层和绝热层之间的至少一块冷却板及多条设于绝热层内的冷却管，冷却管与一块冷却板贴合接触，冷却管设有用于控制流量的流量控制阀，绝热层还连接有贯穿其以对冷却板的温度进行检测的第一热电偶。本申请提供的取向硅钢环形炉钢卷冷却装置可满足不同品种和规格取向硅钢对冷却速度的要求，能够在满足出炉钢卷板形质量要求基础上减少钢卷在冷却一段的处理时间，提高环形炉的生产效益，同时能够减轻因钢卷重量波动、台车空装等因素对钢卷磁性能和板形质量的影响。

本发明公开了一种消除取向硅钢单边浪缺陷的方法，其包括如下步骤：1)、制作专用盖板；所述专用盖板包括环形板，所述环形板外边缘设有多个剪开处；2)、将待装炉的取向硅钢钢卷吊运至高温退火炉炉台；3)、将专用盖板铺于取向硅钢钢卷上端面外圈；4)、将专用盖板上的各剪开处向下弯折，勾住取向硅钢钢卷外沿；5)、扣上内罩，内罩底边砂封；6)、钢卷进炉，完成高温退火过程。本发明能有效保护钢卷边部，防止钢卷上端面翻边；该方法还能将钢卷内部水分排出，避免钢带表面氧化。