硅钢资料

分析了电感耦合等离子体发射光谱法(ICP-AES)测定硅钢中铌的检测过程,讨论了该检测过程中不确定度的主要来源,建立了该方法的定量的数学模型,并根据这一模型计算出了检测结果的合成标准不确定度和扩展不确定度。 The measurement of niobium content in silicon steel by inductively coupled plasma atomic emission spectrometry(ICP-AES) was analyzed,by which the main factors affecting the uncertainty of the measurement were ascertained and the calculation formula was given.Finally,according to the formula the combined uncertainty and expanded uncertainty were obtained. 

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

一种含Bi高磁感取向硅钢热轧带钢边部质量控制方法：炼钢；连铸；铸坯加热；粗轧，粗轧道次不低于4道次，各道次压下率控制在20~33%；规精轧及进行后工序。本发明通过对热轧工序的控制，能使热轧带钢边部开裂的尺寸降低至不超过5mm，且边部开裂≤2mm比率能达到95%以上，后工序切边量很少甚至无需切边即可进行冷轧，使产品成材率能比现有技术提高2~4%；且由于铸坯加热温度的降低使能耗也随之降低。

通过对激光粒度分析仪测量硅钢级氧化镁(MgO)的分析条件进行优化,如分散介质、分散方式、样品预处理、仪器暗淡度等,探讨了硅钢级MgO粒度范围测量重现性较好的试验方法,满足硅钢生产过程控制对MgO粒度的要求。 The analysis condition of the laser particle size analyzer on grain oriented silicon-steel grade magnesium oxide is optimized,including the dispersion medium,dispersion methods,sample preparation,and instrument obscuration,etc.Therefore,particle size measurement with good reproducibility for silicon-steel magnesium oxide is discussed,which may meet the requirement of MgO particle size for silicon-steel process control. 

【作者】 姚昌国； ...

目的提高硅钢的磁性能。方法采用多弧离子镀技术,在普通取向硅钢薄板两面沉积高硅FeSi合金层制得高硅梯度硅钢,并进行热处理,观察其显微组织,测量磁性能。结果退火态高硅梯度硅钢表面的高硅FeSi合金层与基底结合紧密,均匀致密。高硅梯度硅钢中硅含量呈梯度分布,最表层硅质量分数为11.0%,随着深度增加,硅含量逐渐降低,在距表面20μm处硅质量分数仍能达到6.5%。沉积态高硅梯度硅钢的电阻率ρ、低频铁损P10/50、高频铁损P10/1k及磁感应强度B8分别为68.6μΩ·cm,0.82W/kg,83.3 W/kg和1.73 T,退火后分别为63.1μΩ·cm,0.44 W/kg,54.38 W/kg和1.89 T。结论由于表层高硅FeSi合金层的存在,梯度高硅钢的低频磁学性能良好,但高频损耗需进一步改善。 Objective To improve the magnetic properties of silicon steel. Methods FeSi alloy coatings with high-silicon content were deposited on the surface of common grain-oriented silicon steel by cathodic arc plasma evaporation,and then a kind of high silicon gradient steel was prepared. The morphologies,content and magnetic properties of the samples were tested. Results FeSi alloy coatings were featured with compact microstructures and excellent adhesive quality with the substrates. The silicon conten... 

本发明实施例公开了一种硅钢稀酸废水零排放处理方法和系统，所述方法包括：获得稀酸废水；对所述稀酸废水中的含硅固体杂质进行分离与回收，以获得稀酸废水净化液和含硅脱水泥饼；将所述稀酸废水净化液进行两级电吸附分盐处理，利用直流电场将稀酸废水中氯化亚铁组份浓缩分离，以获得分盐浓水和分盐淡水；将所述分盐浓水与酸再生工艺耦合，以获得再生盐酸；将所述分盐淡水调质再生处理，以获得铁系絮凝剂和再生工业净化水。所述硅钢稀酸废水零排放处理方法和系统，可以较低成本和能耗实现硅钢稀酸性废水全回用，真正实现废水零排放；可回收稀酸废水中的铁素和稀盐酸，不产生固体废物，可彻底实现废弃物资源化利用。

本发明公开了一种精确控制高磁感取向硅钢板坯Als含量的方法，转炉出钢20～40秒时，定量加入金属铝，加入量按0.15～0.35kg/吨钢；转炉出钢及合金加入后，底吹搅拌均匀3～5min后，加入一定量金属铝后再底吹搅拌均匀3～5min后将钢水吊运至RH开始精炼处理，铝加入量按[WAls目标+(0.009～0.0120％)]范围控制；钢水在RH精炼过程经过2～3次酸溶铝的成分微调后结束精炼，精炼结束Als按[WAls目标+(0.0030～0.0045％)]目标范围控制；RH精炼结束样酸溶铝检测结果出来后，在连铸开浇前，在钢包内补加铝线使钢液中Als在[WAls目标+Δ浇注Als损]目标范围内；连铸进行氩气环流保护浇注，其中氩气环流流量控制在6～12m3/h；浇注成合格板坯后按正常工艺进行热轧及后工序生产。

【作者】 谌剑； ...

本发明公开了一种适用于无取向硅钢极薄带表面涂覆的涂液，它由水溶性丙烯树脂、成膜助剂、耐盐雾助剂、流平剂、纳米氢氧化锆、消泡剂、水按质量比100:(2～8):(1～3):(1～5):(0～1):(0.1～0.5):(70～130)组成。将该涂液在无取向硅钢极薄带表面可表现出良好的涂覆性，经烘烤固化后形成的绝缘涂层表面透明光滑，附着性和绝缘性能优良，可有效提升无取向硅钢极薄带的综合性能，适合推广应用。

电动汽车电机在高速旋转时承受离心力和电磁力的作用,在进行电机转子设计时,既要考虑电磁性能,还要考虑机械性能。对电机转子受力情况进行了综述,分析了转子用电工钢疲劳性能参数的重要性,详细阐述了试样抛光、表面处理、试样的对中和安装对测试结果的影响。 The motor of electric vehicle bears big force for high speed rotors,mainly including centrifugal and electromagnetic forces.The magnetic and mechanical aspects of the electrical steel are crucial to machine design.In this paper,the forces applied on the motor were summarized and importance of fatigue properties was analyzed.The influence of specimen polish,surface treatment,alignment and installation on fatigue testing result were represented in detail. 

研究了铝和铬元素在无取向电工钢晶粒长大过程中对织构及晶界变化的影响规律。试验结果表明:电工钢在晶粒长大过程中的主要织构组分均为{111}<112>。在晶粒生长期间,不加铝的1号试样中,{111}<112>、{111}<110>织构组分强化,而{100}<001>织构组分弱化;与1号试样相比,在加入0.2%的铝(质量分数,下同)的2号试样中,{111}<112>、{111}<110>织构组分强化(增加)的速率下降,{100}<001>织构组分变化不明显,甚至稍有增加。在含铝的试样中再加入0.3 5%的铬之后(3号试样),{111}<112>{、111}<110>和{100}<001>织构组分的变化规律与1号试样相似,但当电工钢中加入0.72%的铬之后(4号试样),上述3种织构组分的变化规律与2号试样相似。对于在晶粒生长期间持续变化的3种织构组分而言,1号试样的{1 1 1}<112>和{111}<110>织构组分的高(低)取向差角度晶界频率下降(... The effect rule of Aluminm and Chromium on texture and grain boundary transformation in the nonoriented electrical steel during grain growth was investigated.The experimental result shows that the main texture component is {111}<112> in the electrical steel.The {111}<112> and {111}<110> components in specimen 1 without Alumium were strengthened during grain growth whereas {100}<001> component was weakened.But the growth rate of {111}<112> and {111}<110> compon...