硅钢资料

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

本发明涉及无取向硅钢生产技术领域，公开了一种改善含Cu高强度无取向硅钢冷轧质量的方法，包括如下步骤：A)含Cu高强度无取向硅钢热轧卷化学成分(wt,％)：Si：2.0～3.5％，Als≤1.5％，Cu：1～3％，其他为Fe,Als,Mn以及不可避免的杂质元素，对热轧卷进行常化酸洗处理，常化温度T常满足：T常≤1620‑(0.5Als+1.5Si+Cu)％×104，单位℃；B)将常化后的热轧卷在电磁感应加热炉内进行加热；C)在冷轧机组开卷机进行开卷，冷轧第一道次开卷温度T冷轧满足：1.5×(Si+Cu)％×103‑T室温≤T冷轧≤40+2×(Si+Cu)％×103，单位℃，式中，T室温为室温；D)按照4‑6道次冷轧到目标厚度。本发明改善含Cu高强度无取向硅钢冷轧质量的方法，在采用传统常化工艺路线，保证较高的强度和磁性水平前提下，改善冷轧质量，提高成品成材率。

一种适合冷连轧的高效变频压缩机用无取向硅钢，其化学成分及wt%为：C：≤0.0025%、Si：2.4~2.8%、Mn：0.35~0.65%、Al：0.5~0.8%、S：≤0.0020%、N：≤0.0025%、P：≤0.03%、Sb或Sn：0.03~0.08%；生产方法：冶炼浇注；对铸坯加热；粗轧；精轧；卷取；常化；经酸洗后冷连轧；退火；涂敷及精整。本发明产品性能既保证产品磁性能又提高生产效率、提高成材率和降低生产成本的效果，五机架连轧机只需要一次轧过即可，且连轧机相比单机架轧机减少了来回轧制的带头带尾切废量，因而可提高成材率，生产效率和成材率提高，自然降低生产成本。

本发明公开了一种适用于无取向硅钢极薄带表面涂覆的涂液，它由水溶性丙烯树脂、成膜助剂、耐盐雾助剂、流平剂、纳米氢氧化锆、消泡剂、水按质量比100:(2～8):(1～3):(1～5):(0～1):(0.1～0.5):(70～130)组成。将该涂液在无取向硅钢极薄带表面可表现出良好的涂覆性，经烘烤固化后形成的绝缘涂层表面透明光滑，附着性和绝缘性能优良，可有效提升无取向硅钢极薄带的综合性能，适合推广应用。

运用电子背散射衍射(EBSD)和X射线衍射(XRD)技术对硅钢热轧板的织构在板厚方向的分布进行了研究,并分析了两种织构测量方法的特点。EBSD技术能直观给出板厚方向的微观织构,XRD能得到钢板的宏观统计织构信息,结合两种技术的分析,能更直观更精确的研究不同织构在板厚方向的分布。 The texture distribution along the thickness of the silicon steel has been investigated by electron backscatter diffraction(EBSD) and X-ray diffraction(XRD) technique.The characteristics of two technique of texture analysis have been investigated.Combined the two techniques,the texture distribution along the thickness of the silicon steel could be realized distinctly and accurately. 

本发明公开了一种高磁感取向硅钢高效脱碳退火工艺，主要工艺流程为：炼钢连铸→热轧→酸洗常化→冷轧→脱碳和初次再结晶退火→渗氮处理(低温Hi‑B)→涂覆氧化镁隔离剂→高温退火→拉伸平整退火→涂覆绝缘涂层→精整，低温HiB不同于高温Hi‑B的工艺流程主要是在脱碳退火后增加了渗氮段。本发明在保证产品实物质量不低于现有水平(国内领先水平)的前提下，使Hi‑B钢退火效率达到世界领先，制造成本大幅降低。

本发明公开了一种高牌号硅钢的穿带激光焊接方法，包括：将焊缝中硅含量降低到Si焊＜1.9%。采用激光+填丝焊接，填丝ER50‑6碳钢焊丝；根据焊缝截面积和激光焊接速度；激光填丝焊接时，激光线能量应足够大，达到填丝在熔池中充分混合，均匀分布，不至于填丝的成分浮在熔池的上半部分。采用此方法使焊缝组织从粗大铁素体变成细小、致密的无碳贝氏体，晶内沉淀相和晶间脆性相相对大幅减少，提高了焊缝韧性和成形性能，保证了高硅硅钢带的穿带焊接和连续生产。

硅钢工业退火炉温度控制具有强耦合、纯滞后、多扰动等特点,它的控制方法代表着一类非线性系统控制的解决方法。以硅钢工业退火炉温度为控制对象,在双交叉限幅控制的基础上引入了智能学习系统,形成了基于智能学习系统的双交叉限幅控制方法来解决此类非线性系统的控制问题,并通过模块化的编程来实现其功能。结果表明:与传统的PID控制相比,该控制方法的控制精度、抗扰性等控制指标有明显提高,是解决此类非线性控制的一种有效方法。 The temperature control of silicon steel industrial annealing furnace has the features of strong coupling,pure lag,multidisturbance. The control method represents the solution of a class of nonlinear control systems. The control object is the temperature control of silicon steel industrial an-nealing furnace, the intelligent learning system based on Double Across Limit Control is introducedand used to solve control problem of this kind of nonlinear system, and the module programming isused to re... 

采用X-射线衍射分析技术测定了取向硅钢热轧板在不同压下率下不同厚度处的织构。结果表明,在压下率低于80%的情况下,几乎所有试样的不同厚度处的织构均为旋转立方织构类型{100}<011>,但不同压下率、不同厚度处的织构强度存在很大差异;在压下率大于80%的情况下,不同试样的不同厚度处的织构类型发生了变化,其织构类型为旋转立方织构或高斯织构{011}<100>,且当织构类型为旋转立方织构时,织构强度存在很大差异,而当织构类型为高斯织构时,织构强度差异相对较小。 The texture of the grain oriented silicon steel hot rolled plate at different compressibility has been measured.The experimental results have shown that the texture of all samples at different thickness is {100}<011> when the compressibility is below 80%,and its intensity at different compressibility and thickness is difference.The texture of all samples at different thickness is variable when the compressibility is above 80%,it is {100}<011> or {011}<100>,and the intensity of ... 

本发明公开了一种改善取向硅钢内外圈和边部表面质量的方法及环形炉，在一次冷轧工序中，采用错边卷曲，卷曲张力按渐变张力进行控制且头尾的卷曲张力大、中部的卷曲张力小，MgO的涂覆量与卷曲张力同步变化且头尾的涂覆量少、中部的涂覆量多；在高温退火工序中，环形炉的底板上增设一层由若干扇形块绕中心均布形成的垫层，相邻扇形块之间存在空隙，环形炉的内罩内钢卷的上端加盖通风式的盖板，盖板底面的内圈间隙伸入钢卷孔、外圈间隙套在钢卷上、中间通过绕中心均布的导流槽支撑在钢卷端面上，导流槽呈螺旋状且入口与盖板内圈上的开口一一对应连通、出口延伸至盖板底面外圈内侧。本发明可显著减少表面缺陷，明显改善表面质量和磁性，操作容易。

阐述了电工钢在\"双碳\"中的作用,强调了电工钢的生产工艺技术及在减少碳排放、降低能耗中的作用,对下游能效升级带来明显的节能及降碳成果。同时,分析了2021年电工钢的生产运行情况,介绍了电工钢的未来发展,并针对如何减少碳排放以及生产更多的更低铁损、更高磁感的电工钢谈了几点启示。 The effects of electrical steels on carbon peak and carbon neutralization were expounded,especially on the achievements of obvious energy saving and carbon reduction to the downstream energy efficiency upgrading bringing from the production technology of electrical steels and their effects to reducing carbon emission and energy consumption.Meanwhile the production situation of electrical steels in 2021 was analyzed,and the future development of electrical steels was introduced,and some advices w... 

在50Kg氧化镁坩埚真空感应炉上进行高硅电工钢的脱氧试验。结果表明,通过控制原料的成分、高真空下的碳氧反应和炉衬分解向钢液中的供氧,可使钢液的总氧含量≤15×10-6;在维持高温高真空条件下,当钢液中的反应达到一定程度后,延长精炼时间并不能降低钢液的总氧含量;完成精炼后加入硅钙合金沉淀脱氧可进一步降低钢液的总含氧量,但脱氧效果有限。 The test of high-silicon electric steel deoxidation has been carried out in 50Kg vacuum induction furnace with magnesium oxide crucible.Results show that the total oxygen could be ≤15×10-6in molten steel by controlling material components,carbon-oxygen reaction in high vacuum and oxygen contamination from crucible materials on molten steel;And when the reaction was carried through to a certain extent,total oxygen in molten steel could not be reduced by the extension of refining period in high va...