硅钢资料

借助OM、激光共聚焦显微镜、质谱仪和电解萃取等设备和方法，研究了添加微量稀土La（质量分数0.001 1%）的取向硅钢在轧制前采用不同加热保温时间对抑制剂固溶行为的影响。结果表明：当稀土取向硅钢在1 250℃分别保温10、20、30 min后，试验钢晶粒尺寸随保温时间延长有先快后慢的长大趋势；三种抑制剂元素Mn、Cu和Al均发生固溶，保温时间对Mn和Cu两种元素的固溶影响明显，固溶量分别由69.8%和43.7%增加至84.2%和85.2%；随着保温时间的延长，稀土取向硅钢中抑制剂的小尺寸未溶物逐渐减少直至消失，较大尺寸未溶物（300～600 nm）逐渐转变为小尺寸未溶物逐步溶入基体中，数量减少且未溶物的类型由复杂逐渐转变为单一。 In this paper the solid solution behavior of the inhibitor under various holding time in 0.001 1 %La oriented silicon steel during reheating had been investigated by using OM, LM, methods of electrolytic extraction and mass spectrometer. The results showed that grain size of the test steel increased significantly with the holding time prolonging when the rare earth oriented silicon steel was heated to1 250 ℃ and held for 10, 20 min and 30 min respectively, and the growth trend slowed down after ... 

通过对激光粒度分析仪测量硅钢级氧化镁(MgO)的分析条件进行优化,如分散介质、分散方式、样品预处理、仪器暗淡度等,探讨了硅钢级MgO粒度范围测量重现性较好的试验方法,满足硅钢生产过程控制对MgO粒度的要求。 The analysis condition of the laser particle size analyzer on grain oriented silicon-steel grade magnesium oxide is optimized,including the dispersion medium,dispersion methods,sample preparation,and instrument obscuration,etc.Therefore,particle size measurement with good reproducibility for silicon-steel magnesium oxide is discussed,which may meet the requirement of MgO particle size for silicon-steel process control. 

一种高磁感低铁损取向硅钢生产用表面涂层涂覆装置，包括：加工台，加工台上端固定连接支撑架，支撑架下端一侧固定连接伺服电机，伺服电机输出端固定连接第一齿轮，第一齿轮下端啮合连接第二齿轮，第二齿轮中部固定连接螺纹杆，螺纹杆上螺纹连接移动环，螺纹杆远离第二齿轮一侧转动连接支撑板，支撑板上端固定连接支撑架，移动环下端固定连接伸缩杆，支撑架下端前后部均固定连接连接框，本实用新型的有益效果是：通过设置的伺服电机、第一齿轮、第二齿轮、螺纹杆和移动环等结构，能够实现伸缩板带动硅钢板移动，从而能够完成自动化推料，减少工人劳力支出的同时，也能够避免工作人员手臂靠近涂层辊，从而避免安全事故的发生。

通过微观组织表征、高温拉伸和断口形貌分析,研究了钇(Y)元素对6.5%Si无取向硅钢组织、高温拉伸及断裂机制的影响。研究结果表明,添加Y元素可以在钢液中形成YS和YP的复合析出。YS和YP可以充当异质形核基底,提高形核率,细化凝固组织。热轧组织不均匀,由表层至芯部分别形成等轴晶、等轴晶/拉长晶和拉长晶的混合组织。退火后,热轧变形组织转变为等轴晶,含Y实验钢的退火组织得到明显细化。500℃时效处理后,含Y实验钢具备较低的有序度,300℃的拉伸断口呈现韧性断裂特征,断后伸长率达到20.2%。相反,无Y实验钢发生脆性断裂,断后伸长率仅为2.1%。研究结果证实,Y元素可以通过组织细化和降低有序度提高6.5%Si无取向硅钢的中温塑性。 The effects of yttrium(Y)on microstructure,elevated-temperature tensile properties and fracture mechanism of 6.5% Si non-oriented electrical steel were investigated by means of microstructure characterization,high-temperature tensile test and fracture analysis.The results showed that the doping of Y introduced composite Y-rich precipitates(YS/YP)in the melt.YS and YP precipitates were qualified for heterogeneous nucleation agents,which thus raised the nucleation rate and refined the solidificati... 

本发明提供能够制造磁特性与被膜密合性优异的电磁钢板的新颖并且得以改良的电磁钢板的制造方法。一种电磁钢板的制造方法，其特征在于，其包括以下工序：使电磁钢板与溶液相接触，所述电磁钢板以质量％计含有C：超过0％且0.10％以下、Si：2.5％以上且4.5％以下、Mn：0.01％以上且5.0％以下、S、Se及Te中的1种或2种以上的合计：超过0％且0.050％以下、酸可溶性Al：超过0％且5.0％以下、N：超过0％且0.015％以下、P：超过0％且1.0％以下、剩余部分由Fe及杂质构成，其中，上述溶液含有Cu、Hg、Ag、Pb、Cd、Co、Zn及Ni中的1种或2种以上，各元素的浓度合计为0.00001％以上且1.0000％以下。

本发明涉及取向硅钢技术领域，尤其涉及一种取向硅钢边浪的控制方法、装置、设备和存储介质，该方法包括：在将通过脱碳退火阶段的取向硅钢的带钢进行卷取过程中，在带钢的下端侧上刻上刻痕线，其中，下端侧为带钢与高温退火炉的承托底板接触的一侧，刻痕线平行于带钢轧制的方向；控制卷取后的带钢通过高温退火阶段和热拉伸平整阶段后至精整阶段时，沿着刻痕线，切除带刚的边浪；其中，边浪为在带钢的刻痕线至下端侧的边的部分。该控制方法可显著改善高温退火后取向硅钢边部浪形，有效降低精整切边量，提高取向硅钢的板形质量及成材率，降低生产成本。

本发明涉及取向硅钢技术领域，且公开了包括以下步骤：步骤一：冶炼，冶炼经转炉和RH精炼后得到钢水，在进行冶炼的过程中通入空气并设置总进气量100‑300Nl/min，且通入的空气中氧含量为20‑21％之间。该磁性优良的高磁感取向硅钢的气氛控制工艺，通过在不同的流程中，加入一定配比的氧气和氮气的含量，有效的提升每个阶段的气氛控制精度，从而得到最终的高磁感取向硅钢达到优良，避免了因气压、流量等因素影响最终高磁感取向硅钢磁力效果，炉渣中FeO含量减少，提高钢回收率和炉衬寿命，进而也起到降低生产成本的效果，且进行精确的气氛控制，使得在进行高磁感取向硅钢的冶炼中，使得冶炼的效果更好，使得冶炼出来的高磁感取向硅钢的磁性更加的优良。

本文介绍了无取向硅钢C6涂液的性能,研究了配水量、固化程度和涂层厚度等因素对无取向硅钢C6涂层性能的影响。结果表明,随着配水量的增加,完全固化所需的时间增加,涂液固体含量降低,涂层厚度减小;随着固化程度的提高,涂层硬度先增大然后趋于恒定,而柔韧性逐渐变差,在过固化后急剧恶化;涂层厚度对涂层的表面外观、附着性和绝缘层间电阻均有显著影响。 Based on the introduction about the performance of C6 varnish for non-oriented silicon steel sheets,effects of water amount,curing degree and coating thickness are discussed. Results show that with the increase of water amount,the time required to cure completely extends,and both the solid content of C6 varnish and the coating thickness decrease. As the curing degree increases,the hardness of the coating increases first and then tends to be constant,however the flexibility degenerates,especially... 

通过热力学计算与模拟试验研究了含钒钛取向硅钢中氮化物析出相的析出规律与析出行为,并探讨了含钒钛元素的氮化物析出相作为薄板坯连铸连轧流程制备取向硅钢中辅助抑制剂的可行性.研究表明,在所冶炼的含钒钛取向硅钢的成分范围内,Ti N在钢液凝固末期便具备析出的热力学条件,而Al N与VN只可能在凝固后的α+γ或α+Fe3C两相区内析出.含钒钛取向硅钢中氮化物析出相以成分复杂的复合析出相为主,且随着钒钛加入量的增加,钢中抑制剂析出相总的分布密度由于含钒钛元素的氮化物析出相的增加而明显提高,使抑制剂抑制初次再结晶晶粒正常长大的能力得以加强,最终成品的磁感应强度值B8由1.857 T提升至1.898 T.同时,加入不高于0.007%的Ti与不高于0.005%的V不会影响中间脱碳退火工序的脱碳效果以及高温退火净化阶段硫、氮的脱除效果,其形成的含钒钛元素的纳米级氮化物析出相适合作为薄板坯连铸连轧流程制备取向硅钢的辅助抑制剂. The precipitation behavior of nitride precipitates in grain-oriented silicon steel containing vanadium and titanium elements produced by thin slab casting and rolling process was studied by thermodynamic calculation and simulation experiment. The feasibility of nitride precipitates containing V and Ti elements as auxiliary inhibitors was also investigated. It is found that Ti N is likely to precipitate at the final stage of solidification in the grain-oriented silicon steel,but VN and Al N can p... 

从取向硅钢生产路线的选择、工艺技术的改进和生产设备的改造三方面进行了生产取向硅钢的节能降耗技术改造.通过完善多元抑制剂配方生产低温取向硅钢,通过加抛丸的酸洗、带面超声波清洗、改进连续退火炉以及余热循环利用等技术改造,使2012年取向硅钢的产量与未进行技术改造前的2009年相比提高了2.5倍,产品磁性上升了一个半牌号,能耗下降了8.9%,成材率提高了6.4%,生产成本下降了22%,综合效益显著. Energy saving technological transformation was carried out in the production of grain oriented silicon steel from three aspects of the oriented silicon steel production process route selection,technology improvement and equipment renovation.Through the improvement of multiple inhibitor formulations for producing low-temperature grain-oriented silicon steel,and by adding the blasting pickling,the belt surface ultrasonic cleaning,improvement of continuous annealing furnace,waste heat recycling tec... 

对低温加热工艺生产的以AlN为主抑制剂的高磁感取向硅钢高温退火过程进行中断实验,借助电子背散射衍射技术对高温退火过程中高斯晶粒的演变进行了研究.在升温过程中高斯晶粒平均尺寸先减小再增大.800℃时取向分布函数图出现高斯织构组分,但强度很弱,高斯晶粒偏离角在10°以上;900℃时高斯晶粒平均生长速率超过其他晶粒;950~1000℃时高斯晶粒异常长大,偏离角3°~6°;在1000℃之前高斯取向晶粒相比于其他晶粒没有尺寸优势. The high-temperature annealing process of high permeability grain-oriented silicon steel with AlN as an inhibitor was studied by interrupting test.The evolution of Goss texture in this process was analyzed by electron back-scattered diffraction.It is found that the Goss grain size first decreases and then increases with the rise of temperature.Goss texture appears in the orientation distribution function at 800 ℃,but the intensity is very weak and the deviation angle is more than 10°.The average... 

利用加热炉模拟、动态再结晶以及热模拟等试验方法以及扫描电镜、金相显微镜等分析观察手段对无取向硅钢边裂的成因进行了探讨。结果表明,长时间加热使得板坯边部晶粒异常长大,晶界氧化并脱碳,轧制过程中边部温度过低,动态再结晶过程变弱,使得板坯边部延伸性能变差,是导致硅钢边裂的主要原因。建议通过适当降低铸坯加热温度、缩短保温时间、提高终轧温度来改善硅钢边裂缺陷。 The behaviors of high temperature oxidation,dynamic recrystallization,and hot ductility,microstructure evolution were investigated on the non-oriented electrical steel sheets to discuss the formation of edge crack.The key causes of cracking was found to be the coarse as-cast microstructure,grain boundary oxidation and decarburization in reheating furnace,as well as reduced temperature at strip edge region during hot rolling process resulting in reduced hot ductility and lack of enough dynamic re...