论文

无取向硅钢的磁性能主要取决于铁素体的晶粒尺寸、晶体织构和钢中的夹杂物。通过合适的化学成分设计以及采用适宜的夹杂物控制技术,可以获得最佳的夹杂物控制效果,使其纯净度大幅度提高或者无害,最终获得磁性能优良的高级别无取向硅钢。同时,为满足节能、环保、高效需求,无取向硅钢正朝着节能降耗、环境友好以及多功能、高效率、易加工等方向发展。 The magnetic properties of non-oriented silicon steel mainly depend on the grain size of ferrite,the crystallographic texture,and the inclusions in the steel.The optimum inclusion control effects can be obtained through a suitable chemical composition design and an appropriate inclusion control technique,and then the liquid steel will get be clean or the inclusion will get be harmless,finally the excellent magnetic property of the non-oriented silicon steel can be obtained.Meanwhile,in order to ... 

采用EBSD检测技术,分析了50W800无取向电工钢在重要生产工序间织构的演变以及织构沿带钢宽度方向上的差异性。结果表明:热轧板织构沿带钢宽度方向上的差异性主要体现在表层织构。带钢边部表层织构主要由旋转立方织构、α纤维织构以及少量的γ纤维织构组成,带钢宽度1/4处的表层织构主要存在高斯织构,带钢宽度1/2处的表层织构主要为(110)面织构以及少量的铜型织构。各处的带钢宽度1/4处和1/2处的织构类型基本一致,都以α纤维织构和旋转立方织构为主。冷轧后,各处的表层织构类型差异较小,均为γ纤维织构和α纤维织构。由板宽边部至中心处织构强度值逐渐降低。退火后,各处织构的组分基本一致,为较强的γ纤维织构和较弱的(100)面织构。各处织构强度值差异较小,变化趋势与冷轧板一致。 The texture of non-oriented electrical steel 50W800 was detected by EBSD technique.The evolution of the texture between important processes and the difference of texture along the width direction of strip were analyzed.The result shows that the difference along the width direction of strip of texture at the surface of hot rolled plate is most obvious.The texture at the surface of strip edge is primarily made of rotating cube texture,αfiber texture and weakγfiber texture.Goss texture is mainly co... 

通过对湿H2气氛下,相同退火温度、不同退火时间的CGO硅钢初次再结晶样品进行金相组织观察,并进行了EBSD微观织构分析,研究了CGO硅钢初次再结晶过程中的组织及再结晶织构演变行为。结果表明,在湿H2气氛下,820℃保温,CGO硅钢初次再结晶过程约在120 s时完成。随着退火时间的延长,γ面上{111}<112>织构含量逐渐减少,{111}<110>织构先减少后增多,随着再结晶的完成,部分{111}<112>取向晶粒向高斯{110}<001>取向转化的同时,也向{111}<110>取向转化,高斯{110}<001>织构含量逐渐增多。高斯取向晶粒较多是由{111}<112>取向晶粒转化而来,同时也证明了CGO硅钢高斯取向晶粒的二次再结晶异常长大生长机制为择优形核。 Microstructure development and texture evolution of conventional grain oriented silicon steel,which were annealed at same annealing temperature and different annealing time under wet H2 atmosphere,were investigated through metallographic observation and electron backscattered diffraction analyzing.The results show that the primary recrystallization finishes in 120 s at 820 ℃ under wet H2 atmosphere.With the extending of annealing time,{111}<112> texture decreases,{111}<110> texture d... 

以太钢热连轧厂的硅钢为研究对象,利用凸度仪测量热轧带钢出口凸度值,采用矩阵和失效模式的分析方法了解影响带钢凸度变化的主次因素。研究结果表明:通过有效控制轧制过程中的加热温度、时间及采用合理的辊型,硅钢凸度精度提高了4.34%左右。 In this paper,we take the hot-rolled silicon steelsheet of Taigang as the research symbol,exit profile was measured by convex instrument,the primary and secondary factors that affect the strip profile were measured by using matrix and failure mode analysis methed.The results indicate that convexity accuracy has significantly improved by nearly 4.34% through the effective control of the heating temperature,heating time and the use of correct roller type in the process of hot rolling. 

试验了通过NaCl-KCl-NaF-SiO₂熔盐在电流密度50 mA/cm²、电沉积脉冲电流正反向比9:1和750⁸50℃60min电沉积下阴极（/mm）20×20×0.5的1.6Si无取向冷轧硅钢片断面层硅的分布,并通过计算得出Si的扩散系数。结果表明,电沉积温度由750℃提高至850℃时,试样中Si含量增加,扩散的深度由18μm提高到40μm;电沉积温度与Si在钢中的扩散系数近似符合Arrhenius指数关系。 The distribution of silicon at cross section of cathode（/mm） 20 × 20 × 0.5 sheet of 1.6Si non-oriented cold rolled silicon steel after electro-deposit treatment by NaCl-KCl-NaF-SiO₂ molten salt with current intensity 50 mA/cm²,electro-deposit pulse current positive-negative ratio 9:1 at 750 850 ℃ for 60 min has been tested and the diffusion coefficient of Si is obtained by calculation.Results show that with increasing electro-deposit temperature from 750 ℃ to 85... 

分析了高转矩和高转速条件下高效驱动马达铁芯材料对无取向硅钢磁性能要求,讨论了无取向硅钢的高磁通密度和低铁损对电机转矩和效率的影响,介绍了国内外高磁感无取向硅钢发展情况。在生产工艺上,提高钢质纯净度,弱化夹杂物和第二相粒子对畴壁移动和再结晶晶粒长大的钉扎作用,添加微量晶界和带钢表面的偏析元素促使有利织构发展等技术可提高无取向硅钢的磁通密度。 The requirements of high efficient drive motor core materials under the conditions of high torque and high speed were analyzed.The effects of high magnetic flux density of non-oriented silicon steel on the torque and efficiency of the motor were discussed.The development of non-oriented silicon steel with high magnetic was introduced.The magnetic flux density of non-oriented silicon steel sheet can be obviously improved by some production technologies,such as purification steel,weakening the pin... 

介绍了电工钢生产线连退机组的表面处理工艺,特别是电解清洗系统的工作机理、设备构造、生产工艺及各种影响因素。 This paper introduces the technology of surface treatment of continuous annealing unit in electrical steel production line,in particular the working mechanism,structure of equipment,production techniques and various influence factors of the electrolytic cleaning system. 

采用自主研发的脉冲磁场退火装置，在取向硅钢脱碳退火过程中分别施加不同强度的磁场，并采用光学显微镜和X射线衍射仪研究了脉冲磁场脱碳退火后试样的显微组织和宏观织构。结果表明，脱碳退火过程中施加脉冲磁场后取向硅钢的平均晶粒尺寸均增加，当磁场强度为40 mT时，平均晶粒尺寸最大，为13.06μm。此外，取向硅钢试样的立方织构{001}<100>强度减弱，高斯织构{110}<001>和{111}<112>织构增强，有利于获得更好的成品织构和磁性能。 Self-developed pulsed magnetic field annealing device was used to apply magnetic field of different intensities during decarburization annealing of an oriented silicon steel, and microstructure and macro-texture of the specimens after decarburization annealing in a pulsed magnetic field were studied by using optical microscope and X-ray diffractometer. The results show that the average grain size of the oriented silicon steel increases with the application of pulsed magnetic field during decarbu... 

介绍了一种适用于超大晶粒取向硅钢的高斯晶粒取向偏离角的X射线衍射测量方法，提出了将试探法和探测器扫描法相结合的方式进行测量。结果表明：该方法可以同时获得准确的实际衍射角度和取向偏离角度，试样制备方式简单，对设备的要求低且测量结果准确。 This paper introduces a X-ray diffraction measurement method of Gaussian grain orientation deviation angle for ultra-large grain oriented silicon steel, and puts forward a method of combining the test method with the detector scanning. The results show that this method can obtain accurate actual diffraction angle and orientation deviation angle at the same time. The sample preparation method is simple, the requirements for equipment are low, and the measurement results are accurate. 

利用背散射衍射技术(EBSD)和XRD,研究了两段式脱碳退火工艺对取向硅钢纵截面初次再结晶的微区取向、取向差分布、特殊晶界(CSL)及高温退火试样高斯织构。分析了初次再结晶晶界特征对取向硅钢高温退火后宏观织构的影响。结果表明:初次再结晶的纵截面基体中Σ3和Σ5晶界使得高斯晶粒有着较高的迁移率,在高温退火时借助20o～45°的大角度晶界的界面能吞并周围{111}<112>晶粒迅速长大,形成密度水平较高的高斯织构。 Micro area orientation of primary recrystallization,the misorientation distribution,special boundaries under different two-stage decarburization annealing and the Goss texture under high temperature annealing the longitudinal section of grain-oriented silicon steel were detected by electron back scattering diffraction(EBSD) and X-ray diffraction(XRD).The effect of primary recrystallization grain boundary on macrotexture after high temperature annealing was analyzed.The results show that the Σ3 a... 

利用OM、TEM与EDS技术,对Fe-3.2%Si低温取向硅钢热轧板进行不同常化冷却工艺处理后的显微组织、析出相及最终产品的磁性能进行分析,并与热轧板的组织和析出相进行对比。结果表明,常化板较热轧板的表层组织均匀,基体中再结晶比例增加,带状组织变窄;常化板中析出物的数量明显比热轧板的多,析出物主要有AlN、MnS及复合析出的(Cu,Mn)S等。在常化温度1120℃、保温3 min的条件下,采用二段式冷却较空冷、淬沸水、淬常温水的冷却工艺,常化板表层显微组织更均匀,沿板厚方向的显微组织的不均匀性显著,取向硅钢的磁性能最高;常化后采用二段式冷却工艺析出的细小析出物数量最多,且弥散分布在基体中,抑制剂的抑制效果最好,对成品获得高磁性最有利。 Microstructure, precipitate and magnetic characteristic of final products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy(OM), transmission electron microscopy(TEM), and energy dispersive spectrometry(EDS). The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are nar... 

基于简化的取向硅钢片模型,系统地对不同的交流激励下的硅钢叠片内铁损、交链磁通和空气中指定位置的法向漏磁的分布进行了\"单片级\"的测量,并建立了相应的硅钢叠片级问题的三维有限元分析模型,进行了大规模的数值计算分析。模型实验和数值分析的结果表明垂直进入硅钢片的漏磁通和损耗呈现浅透入的特点,在硅钢片内引起的涡流损耗在总铁损中占据了\"举足轻重\"的份额。用电磁场有限元分析软件MagNet瞬态场时步法计算结果与测量结果相吻合,说明本文方法研究复杂的硅钢叠片问题的有效性。 The measurement and 3D finite element analysis of the iron loss,interlinkage flux inside the laminated silicon steel sheets and the magnetic flux densities at the specified positions are carried out based on a verifying silicon steel sheet model.The modeling results show that the leakage flux vertically through the silicon steel sheets has the peculiarity of shin effect,and the eddy current loss caused by the AC leakage flux is a significant component of the total iron loss.The calculated result...