论文

对CSP流程生产的无取向电工钢M50W800不同尺寸样品的磁性能进行了测试和分析,结果表明:采用不同单片检测的磁性能结果与标准的Epstein方圈样品检测对比,存在明显的偏差;且同一尺寸的单片纵横向样品之间相比较,对应的磁性能差异性也较大。几种不同尺寸的单片样品,以320mm×30mm尺寸的纵横向平均值最接近标准Epstein方圈样的性能值,其铁损偏差最小。 The magnetic properties of M50W800 non-oriented electrical steel produced by CSP process were tested and analyzed with samples of different sizes,showing that significant deviation existed compared to that of Epstein square circle sample.In particular,obvious difference in magnetic properties also existed between longitudinal and transverse samples of the same size.For test samples of different sizes,the average magnetic properties of 320mm×30mm samples are the closest to that of Epstein square ... 

为了优化激光刻痕降低取向硅钢铁损的工艺,寻找刻痕速度、脉冲能量、扫描间距等重要刻痕参数的最佳匹配关系,提出了一种基于人工神经网络与遗传算法的优化模型,并利用这种模型对30Q130取向硅钢材料的刻痕工艺进行了优化实验,结果表明,这种模型稳定可靠,可以作为取向硅钢刻痕工艺优化的一种有效的措施。 A laser is often considered to scribe the grain-oriented silicon steel surfaces after cold-rolling and annealing to reduce the core loss.It is necessary to select the best scribing parameters to maximize the reduction in this process.This paper proposes an optimization method of genetic algorithm during laser scribing of 30Q130 steel,by developing an artificial neural network prediction model using a database form a designed orthogonal experiment.The objective is to determine the best combinatio... 

在实验室模拟CSP工艺条件下制备了取向硅钢,研究了二次冷轧中间退火工艺对组织和织构的影响。结果表明,中间退火温度对取向硅钢脱碳,高温退火组织及织构均产生明显影响。经940℃中间退火后,取向硅钢脱碳再结晶晶粒较850℃中间退火的多,且再经高温退火处理后,晶粒粗化,最大晶粒尺寸达4.8 mm;高斯织构组分密度达27.00,较850℃中间退火试样高。 Grain-oriented silicon steel was prepared by simulated CSP technology in laboratory. Effects of secondary cold-rolled intermediate annealing on microstructure and texture were studied. The results show that intermediate annealing has obvious effects on the microstructure and texture of the steels after decarburization annealing and high temperature annealing. After intermediate annealing at 940 ℃,recrystallized grain of decarburization annealed steel is more than that of intermediate annealed at... 

研究稀土Ce的添加对含Sn高磁感无取向电工钢磁性能及夹杂物的影响。对比分析了两种成分钢的磁性能以及各过程工艺条件下夹杂物种类和分布情况。结果表明,在含Sn高磁感无取向电工钢中加入稀土元素Ce可以粗化夹杂物,提高成品晶粒的均匀性,有效降低铁损;同时Ce的添加不影响Sn元素提高磁感的效果,磁感保持不变。 Effect of Ce on magnetic properties and inclusion of Sn-bearing high permeability non-oriented electrical steel was investigated. A comparative analysis of the magnetic properties and the types and distributions of inclusion in the two sheets with different composition shows that the addition of Ce to the Sn-bearing high permeability non-oriented electrical steel can coarse the inclusion,improve the homogeneity of the finished grain and effectively decrease the core loss. Also,the addition of Ce... 

【作者】 张正贵； 李战库； ...

采用热模拟方法及EBSD技术,研究Fe-3 wt%Si电工钢在不同温度下组织的动、静态再结晶及晶粒取向特征,特别是少量奥氏体对铁素体动、静态再结晶组织及取向的影响。结果表明,不同温度形变的组织主要分三类:形变长条铁素体、珠光体和等轴细小铁素体。长条形变铁素体内发生动态回复或连续式的动态再结晶,奥氏体周围的铁素体动态再结晶加速,部分以传统的不连续方式动态再结晶。铁素体、奥氏体都可发生静态再结晶。奥氏体的静态再结晶在1050℃以上明显,铁素体的静态再结晶随温度的升高逐渐进行,最显著的再结晶发生在1050℃。不同温度形变的样品,其形变晶粒取向主要以<111>和<100>为主,小等轴铁素体晶粒除与大形变铁素体取向相近外,出现了<110>取向及其它取向。 Static and dynamic recrystallization and grain orientations in a hot-compressed Fe-3 wt% Si electrical steels were studied at different temperatures using Gleeble simulator and EBSD technique,particularly focusing on the effect of small amount of austenite on ferritic microstructure and orientations.The results show that microstructure of the compressed steel,depending on deformation temperature,consisted of elongated and deformed ferrite,pearlite and fine equal-axed ferrite.The elongated ferrit... 

分析了太原钢铁(集团)有限公司第二炼钢厂80 t RH生产冷轧硅钢脱碳、脱硫原理及影响因素,认为通过合理控制RH到站钢水碳和氧含量、加大插入管内径、采用快速抽真空度等可提高脱碳效果。降低顶渣中FeO和MnO含量,保证脱硫剂加入后的循环时间可以提高RH脱硫率。 The present article analyzes the principle of decarburization and desulfurization in refining the cold rolled silicon steel in the 80 t RH in No.2 Steelmaking Plant of Taiyuan Iron & Steel(Group) Corp.,and its influencing factors.It’s determined that the decarburization effect can be achieved by properly controlling the cabon and oxygen contents in the hot metal coming into the RH station,enlarging the inner diameter of snorkel and adopting the fast evacuation method.In the meanwhile the des... 

利用场发射扫描电镜观察了以MnS为主要抑制剂的普通取向电工钢加工过程中第二相粒子的分布状态,统计了粒子面密度、平均尺寸以及相应的尺寸分布.结果显示,热轧加工造成了大量第二相粒子弥散、细小地析出,同时基体仍保持过饱和状态.冷轧变形会造成第二相粒子的回溶行为,而基体的过饱和状态会减弱回溶现象.中间退火与脱碳退火过程中会同时存在新粒子的形核及已析出粒子的粗化两个过程,而在最终二次再结晶升温阶段则以第二相粒子明显粗化为主. The distribution of second phase particles in conventional grain-oriented electrical steels during manufacturing processes with MnS as inhibitors was observed by field emission scanning electron microscopy,while the areal particle density,the average particle size and the corresponding size distribution were statistically determined.It is indicated that hot rolling leads to dispersive precipitation of a large amount of fine second phase particles and the matrix keeps a supersaturated state furth... 

对两种硅钢水溶性极厚绝缘涂层进行了不同温度的热老化实验。通过TG-DTA,GDS,FT-IR,SEM和光泽度仪等测试方法对老化的涂层进行分析表征,提出了评估硅钢水溶性极厚绝缘涂层热老化性能的合理温度区间,探讨了涂层热老化行为,并分析了两种涂层热老化性能的差异。结果表明,涂层附着性随着老化时间的延长逐渐下降。FT-IR表征结果显示,热老化过程中,涂料交联形成的化学键未发生断裂,交联剂氨基树脂的三嗪环被破坏是聚合物三维网络结构坍塌的主要原因。 Thermal aging expriments at different temperature were carried out on two types of water-soluble and extra-thick insulation coatings for non-oriented silicon steel,and a series of test methods such as glossmeters,TG-DTA,FT-IR,GDS,SEM were applied in analysis.For evaluating the thermal aging effect of this kind of insulation coating,the proper temperature range was proposed.The difference of aging performance between two coatings was been investigated and the related behaviors were been discussed... 

以试验室模拟CSP工艺生产的Fe-3Si热轧钢带为研究对象,采用正交试验及方差分析的方法,研究了取向硅钢初次再结晶退火工艺对高温退火后获得锋锐的高斯织构的影响。结果表明:取向硅钢两段式初次再结晶脱碳退火工艺参数加热段保温时间及加热温度是高温退火后获得锋锐高斯织构的主要影响因素,其可信度分别在90%和85%以上;在本试验条件下,通过正交试验获得的最佳退火工艺为:冷硬板经600℃保温3 min和850℃保温6 min。 Fe-3Si hot rolled strip was produced by simulating CSP technology in the laboratory.Orthogonal experiment and analysis of variance were carried out to investigate the influence of primary recrystallization on the sharp Goss texture of the oriented silicon steel.The results show that holding time of the heating section and the heating temperature for a sharp Goss texture of the samples annealed has important implications in this experiment conditions,the two-step decarburization annealing process... 

采用电解法和扫描电镜研究了300 t转炉-RH精炼钙处理对无取向硅钢板（%:≤0.005C、1.2～2.2Si、0.2～0.6Mn、≤0.20P、≤0.005S、0.2～0.6Al、0～0.01Ca）中夹杂物的影响。结果表明,钢中Al含量为0.25%和0.35%时,钢中溶解氧均小于1×10^-4%,钙处理后都会产生CaS夹杂物,尤其是含0.35%Al的钢水;钙处理可以有效减少钢中的夹杂物数量,尤其是0.5μm以下的微细夹杂物数量;钙处理后夹杂物的种类以AlN、CaS为主,同时还含有少量的氧化物夹杂物以及AlN-CaS复合夹杂物,尺寸主要为1.5～5.0μm。 The effect of 300 t converter-RH refining calcium treatment on inclusions in non-oriented silicon steel sheet （%:≤0.005C,1.2～2.2Si,0.2～0.6Mn,≤0.20P,≤0.005S,0.2～0.6A1,0～0.01Ca） has been studied by electrolysis and scanning electron microscope.Results show that with 0.25%and 0.35%Al content in steel,all the dissolved oxygen in liquid is less than 1×10^-4%,and the CaS inclusions are produced after calcium treatment,especial for the liquid containing 0.35%Al;the amount of inclusions in ste... 

借助光学显微镜、扫描电镜、交流磁性能测量仪和万能拉伸试验机研究了0.3 mm厚高强无取向电工钢冷轧板在780、820、860和900℃退火保温2 min后的组织、织构和性能。结果表明:在退火温度范围内,试验钢均发生了完全再结晶,得到等轴状的铁素体晶粒;随着退火温度的升高,平均晶粒尺寸从9.2μm增长到41.3μm,工频铁损和400 Hz高频铁损均先大幅减小后趋于平缓,磁感应强度先升高后降低。在820℃退火时,铁损P_1.5/50=5.51 W/kg,P_1.0/400=33.22 W/kg均处于较低值,磁感应强度B₅₀₀₀最大,为1.649 T。试验钢的屈服强度和抗拉强度均随退火温度的升高而降低,780℃退火时屈服强度为496 MPa, 900℃退火时降低至407 MPa。综合磁性能和力学性能考虑,试验钢的最佳退火温度是820℃。 Microstructure, texture and properties of 0.3 mm thick high strength non-oriented electrical steel cold rolled sheet annealed at 780 ℃, 820 ℃, 860 ℃ and 900 ℃ for 2 min were studied by means of optical microscope, scanning electron microscopy, AC magnetic property tester and universal tensile testing machine. The results show that in the annealing temperature range, complete recrystallization of the experimental steel occurs and equiaxed ferrite grains are obtained. With the increase of annealin...