硅钢资料

本发明公开了一种高热导率耐腐蚀电工钢自粘结涂料及制备方法，本发明的自粘结涂料包括以下质量百分比的组分：双酚A型环氧树脂25％～35％、酚醛环氧树脂4％～8％、异辛基磷酸酯0.2％～0.5％、丙二醇甲醚5％～10％、乳化剂5％～8％、二甲氨基乙氧基三恶硼杂八环1％～3％、铵封闭路易斯酸盐0.5％～2％、氮化硼纤维3％～12％、氧化铝纤维0.4％～1.0％、研磨助剂0.2％～0.3％、余量为纯水。该自粘结涂料一次固化后形成的活化态自粘结涂层显著提高对电工钢基材的耐腐蚀性，该自粘结涂层具有良好的热导率，一次固化与二次热压固化工艺条件操作难度显著降低。本发明的自粘结涂料制备方法操作简单，实施可行性高。

本发明公开了一种高效无取向硅钢极薄带的工业连续化生产方法，其包括异步轧制、脱脂、热处理、急速冷却、涂绝缘层、烘干烧结、卷取收集各工序；其中，异步轧制中的异步比为1:1.05～1:1.24；脱脂、热处理、急速冷却、涂绝缘层、烘干烧结、卷取收集工序为连续化生产工艺；热处理工序中，第一步为预热，预热温度为500℃～720℃，预热时间20秒～125秒；第二步为相变热处理，相变热处理温度为840℃～940℃，相变热处理时间100秒～600秒；急速冷却工序中，30秒内将钢带温度降温至350℃以下。优点在于:实现工业化连续生产无取向硅钢极薄带，有效提高产能，生产的无取向硅钢极薄带具备高磁感、低铁损等磁性能。

本发明涉及一种低耗高效硅钢常化酸洗工艺及酸洗设备，其有效利用常化炉出口余温作为加热带钢的介质，使带钢与低温的酸液接触表面发生强烈的物理化学反应，快速酸洗剥离表层粗大的氧化铁皮，降低酸洗系统的酸液温度，通过调控溶液氧化还原特性提高酸洗效率去除残留的铁橄榄石，节约了能耗，同时取消了高投资高运行成本的抛丸工艺，实现了低耗高效硅钢常化酸洗的目的。

试验研究了0.3 mm取向硅钢冷轧板(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005A1)的退火温度(760~880℃7 min)和退火时间(820℃3~9 min)对该钢的晶粒尺寸,再结晶和织构的影响。结果表明,最佳初次再结晶退火工艺为820℃5 min,该钢的平均晶粒尺寸为14.20μm,完全再结晶率为92%,不利{111}<110>结构含量为3.16%,有利织构{111}<112>,{012}<001>和高斯织构含量分别0.40%,4.73%和2.46%。 The effect of annealing temperature(at 760 ~ 880 X.for 7 min) and time(at 820℃ for 3~9 min) on grain size,recrystallization rate and texture of 0.3 mm cold-rolled sheet of oriented silicon steel(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005Al) has been tested and studied.Results show that with optimum recrystallized annealing at 820℃ for 5 min,the silicon steel average grain size is 14.20 fun,the complete recrystaUization rate is 92%,the unfavourable-texture {111}< 110 > content in steel is ... 

本实用新型公开了一种硅钢加热保温装置，包括安装板，所述安装板上表面固定连接有加热箱，所述加热箱背面通过固定板连接有多个伺服电机，所述伺服电机输出端固定连接有第一螺杆，所述第一螺杆远离伺服电机的一端贯穿加热箱并螺纹连接有置物板，所述加热箱内侧壁转动连接有多个第二螺杆，所述第一螺杆与相邻的第二螺杆之间通过锥轮组件相连接，所述第二螺杆外侧壁螺纹连接有螺纹块，所述螺纹块上表面通过连接组件连接有夹板。本实用新型，这种保温方式，操作简单，使硅钢在这个过程中，硅钢裸露在空气的时间短，能够起到较好的保温效果，避免因保温不当造成硅钢成品质量降低，从而有效的提高硅钢成品合格率。

本文对某厂硅钢DR510温度、成分及过程控制水平和成品的组织、力学性能进行了研究,并在此基础上提出了工艺优化方案,有一定的借鉴和推广价值。 In this paper,the critical process and the products quality,including temperature,composition and process controlling level,the organization and mechanical properties of the finished product,were studied.On the basis of that the optimized technical plan provided,and this control technology is worth using and spreading. 

本发明涉及一种冷连轧法生产无取向高硅钢的方法，RH真空脱碳处理后，铝脱氧及部分铝合金化，合金化后大罐钢水净循环大于3次或大于5分钟；熔炼合格钢水至连铸开浇前静置时间大于二十分钟；控制过热度5～15℃；采用电磁搅拌，控制等轴晶比例45％以上；3)热轧工序板坯装炉温度大于750℃；常化使晶粒尺寸在90～110μm范围内；连续退火炉加热段温度设定950～1150℃，均热段温度设定900～1050℃，全氮气干气氛保护，控制晶粒尺寸120～170μm。生产全过程中的热履历参数控制，充分发挥设计的微合金元素功能，改变析出物的组成、大小、形态及分布。

研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c... 

对应用动态加热进行短时温度退火的取向电工钢进行了二次再结晶研究。所进行研究的实验用取向电工钢是经过终冷轧和后续罩式退火后的一条工业化生产线生产的。研究结果表明,运用短时热处理条件可引起研究钢完全的异常晶粒长大。在实验室处理的材料的织构和金相组织与工业化生产的经过终退火而获得的相同的取向电工钢类似。但是,在实验室处理的取向电工钢的二次再结晶的矩阵中可观测到\"寄生\"晶粒。从磁性观点看,这些\"寄生\"晶粒含有不理想的{111}取向织构。 The present study was made to investigate secondary recrystallization in grain-oriented steels annealed at short time temperature exposures with application of dynamical heating.The investigated GO(Grain Oriented) steels for experiments were taken from one industrial line after final cold rolling reduction and subsequent box annealing.It was shown that application of short time heat treatment conditions could lead to complete abnormal grain growth in the investigated GO steel.The texture and mic... 

对商用50W330型无取向硅钢成品在930℃下保温2 h固溶并以不同方式冷却处理,利用磁性检测仪检测分析了处理前后的磁感和铁损变化,应用光学显微镜、扫描电子显微镜、X射线衍射仪观测分析了显微组织结构的演变。考察了平均晶粒尺寸、织构组分比及第二相粒子状态对磁性能的影响规律,结果表明:固溶处理前后平均晶粒尺寸的变化对硅钢磁性能的影响非常显著;当平均晶粒尺寸相差不大时,织构组分比[Goss+{100}]/{111}越大,磁感会越高;固溶处理会将细小弥散的第二相粒子重新回溶到基体中,减小了其对磁畴壁的钉扎作用,铁损随之下降。 The commercial 50W330 non-oriented silicon steel samples were heat treated at 930℃ for 2 h and cooled in different ways,then the iron loss and the magnetic induction of the samples before and after solution treatment were measured with a magnetic detector.The evolution of microstructural texture was analyzed by optical microscopy,scanning electron microscopy and X-ray diffractometry.The effects of average grain size,texture composition ratio and the second phase particles on the magnetic propert... 

【作者】 朱传芳； 潘恒韬； ...

变压器D21硅钢铁芯片采用冲压工艺生产。首先对其工艺进行了分析,确定了冲压方案。对产品进行了排样设计,计算了冲压力,确定了压力中心。然后,设计了单工序落料模具,完成了模具装配图。 D21 silicon steel chips for transformer are produced by stamping.First,its stamping process was analyzed and the scheme of the stamping process was determined.The product layout was designed,the punching pressure was calculated,the pressure center was determined.Then,the blanking die with single procedure was designed,the die assembly drawing was completed.