硅钢资料

组织和织构是影响无取向硅钢性能的重要因素。为改善产品性能，研究了冷轧压下率（71.7%～87.0%）对高牌号无取向硅钢组织、织构、磁性能和力学性能的影响。结果表明，随冷轧压下率的增加，退火晶粒平均尺寸先减小后增大；高斯和立方织构强度减弱，γ纤维织构增强，α纤维织构转变为较强的α^*（{h, 1, 1}〈1/h, 1, 2〉）织构，并随冷轧压下率的增加而增强，同时其峰值逐渐向{111}面移动；工频铁损P_1.5/50、高频铁损P_1.0/400和磁极化强度J₅₀₀₀同时降低，屈服强度变化不大，表面硬度逐渐增加。当冷轧压下率由84.7%增至87.0%、厚度减至0.30 mm时，高频铁损降幅是工频铁损的11倍，表面硬度增幅变大。以上研究成果对硅钢减薄后织构及组织的优化提供了很好的指导。 Microstructure and texture are critical factors on non-oriented silicon steel properties. In order to improve product properties, this paper studied the effect of cold rolling reduction rate（71.7%-87.0%） on microstructure, texture, magnetic properties and mechanical properties of high-grade non-oriented silicon steel. The results show that with the increase of cold rolling reduction rate, the average size of annealing grain decreases first and then increases. The intensity of Goss and λ fiber te... 

取向硅钢利用析出物作为抑制剂,抑制初次再结晶晶粒的长大,抑制剂是取向硅钢发生二次再结晶的基本条件之一。文中通过低温板坯加热技术制备取向硅钢,采用透射电镜(TEM)观察并研究了高温退火阶段抑制剂的演化过程。结果表明,渗氮后形成的非晶态Si3N4析出物不稳定,在700～750℃退火升温阶段转化为(Al,Si)N;(Al,Si)N颗粒在800℃发生团聚,随后长大并粗化;(Al,Si)N是低温取向硅钢主要抑制剂,随退火温度的升高,(Al,Si)N抑制力大幅下降。 Precipitates as inhibitor are used to inhibit the grain growth of primary recrystallization in grain-oriented silicon steel,and inhibitor is one of the basic conditions for occurring of secondary recrystallization.The grain-oriented silicon steel was produced by low temperature slab heating and nitriding technique.The evolution of inhibitor was observed by transmission electron microscopy.The results show that Si3N4 particles are precipitated after nitriding,and Si3N4 particles are amorphous and... 

针对宝钢集团、日本新日铁住金和JFE公司公开的相关专利等资料,总结了国内外高强度无取向电工钢的研究进展,分析了不同电工钢的化学成分、生产工艺及产品性能,指出固溶强化、细晶强化、析出强化、位错强化都有可能被用来提高无取向电工钢的强度,并阐述了四种强化方式的优缺点;指出在高强度无取向电工钢的研发过程中,需根据其具体用途确定目标性能,再采用合适的强化手段,最终实现力学性能、磁性能和生产性能之间的平衡。 The research progress of high strength non-oriented electrical steels at home and abroad is summarized according to related patents brought into the public by Baosteel,Nippon Steel & Sumitomo Metal corporation and JFE corporation.The characteristics of chemical composition,production technology and properties of products in the patents are analyzed.Each of solution strengthening method,fine-grain strengthening method, precipitation strengthening method or dislocations strengthening method ma... 

依据GB/T 15616—2008《金属及合金的电子探针定量分析方法》,采用电子探针波谱仪对某W600硅钢中的硅含量进行了定量测定,对影响其定量测定结果的不确定度分量进行了分析,并对不确定度的各个分量进行了计算和合成,最后给出了硅钢中硅含量测定结果的不确定度报告:该硅钢中的硅含量(质量分数)为1.50%,扩展不确定度U=0.20%,取包含因子k=2。 According to GB/T 15616-2008\"Quantitative Method for Electron Prohe Microanalysis of Metals and Alloys\",the quantitative results of Si content in some W600 silicon steel was measured hy EPMA-WDS.The uncertainty components which might affect the measurement results were considered,calculated and synthesized. Finally the uncertainty result for the quantitative value of Si content in the silicon steel was got.The mass content of Si was 1.50%,and expanded uncertainty U=0.20%under the condition of co... 

结合扫描电镜和大样电解研究了CSP流程W800牌号无取向电工钢表面线状缺陷中夹杂物成分及来源，采用SPSS软件回归分析了生产过程各因素对表面线状缺陷的影响。研究表明：稳态浇铸过程铸坯中大型夹杂物含量为5.39 mg/10 kg。引起无取向电工钢表面线状缺陷的大型夹杂物主要为脱氧产物、镁铝尖晶石和钢包顶渣，主要类型为Al₂O₃、MgO-Al₂O₃、CaO-Al₂O₃-MgO和CaO-Al₂O₃-SiO₂。非稳态浇铸过程钢水洁净度明显降低，热轧板表面线状缺陷比例上升。影响表面线状缺陷的主要因素为RH出站时顶渣的w（CaO）/w（Al₂O₃）、RH脱氧结束氧位及中间包最低吨位。 Combining scanning electron microscopy and large sample electrolysis, the composition and source of inclusions in the surface linear defects of W800 grade non-oriented electrical steel in the CSP process were studied. SPSS software was used to regress and analyze the main factors which affected the surface linear defects in the steelmaking process. Research shows that the content of large inclusions in the steady state casting process is 5.39 mg/10 kg. The large inclusions which cause linear def... 

以太钢热连轧厂的硅钢为研究对象,利用凸度仪测量热轧带钢出口凸度值,采用矩阵和失效模式的分析方法了解影响带钢凸度变化的主次因素。研究结果表明:通过有效控制轧制过程中的加热温度、时间及采用合理的辊型,硅钢凸度精度提高了4.34%左右。 In this paper,we take the hot-rolled silicon steelsheet of Taigang as the research symbol,exit profile was measured by convex instrument,the primary and secondary factors that affect the strip profile were measured by using matrix and failure mode analysis methed.The results indicate that convexity accuracy has significantly improved by nearly 4.34% through the effective control of the heating temperature,heating time and the use of correct roller type in the process of hot rolling. 

研究了退火温度和退火时间对电沉积硅钢试样中的断面层组织、硅在试样中的分布情况、织构分布和磁性能的影响。结果表明:退火温度为1000℃、退火时间为210 min时得到的试样晶粒分布均匀、硅在试样中分布均匀、硅平均浓度为6.3715%(接近6.5%)。试样的织构分析及磁性能检测的结果表明,在较高温度下延长退火时间可增加{100}和{110}面织构,降低铁损,所得试样的磁性能较为良好。 The effect of annealing temperature and time on the microstructure, distribution of silicon,texture and magnetism of the high silicon steel prepared by electrodeposition was investigated. The results showed that after annealing at 1000℃ for 210 min, the mean grain size of steel was about 190 μm with a uniform grain size distribution, and the silicon is also uniformly distributed on the entire cross section with an average Si concentration 6.3715%(close to 6.5%); With the increasing annealing tim... 

研究了锰含量对w(Si)=1.8%Si无取向电工钢组织和性能的影响。结果表明,钢中锰含量从0.3%增加到1.2%时,由于α_γ相变的产生,铸坯低倍组织、热轧板金相组织及成品织构等均发生了不同程度的变化,对成品表面质量及磁性能产生了明显的影响。 The effects of manganese content on structure and properties of w(Si)=1.8% non-oriented electrical steels have been studied.Results show that with increasing manganese content to 1.2% from 0.3%,macrostructure of continuous casting slab,hot rolled band metallurgical structure and finished product texture vary in some extent because of the occurrence of α-γ phase transformation,the surface quality and magnetic properties of finished product are affected greatly. 

利用EBSD技术对CGO硅钢热轧、中间退火、脱碳退火及二次再结晶退火组织及织构进行分析,研究了CGO硅钢各阶段加工制备过程中高斯{110}<001>晶粒的形状、尺寸及分布特点,分析了高斯取向晶粒在各工序过程中的遗传继承性特点。结果表明,CGO硅钢热轧板的次表层存在Goss取向晶粒,历经一次冷轧及中间退火后Goss取向晶粒基本消失,一次再结晶之后Goss织构仍不是主要织构,主要织构为{111}<110>和{111}<112>,说明Goss取向晶粒在二次再结晶退火前数量及尺寸上并不占优势,二次再结晶过程中Goss取向晶粒异常长大形成锋锐Goss织构。{111}<110>和{111}<112>织构组分的强度在一次冷轧中不断增加,{111}<112>织构组分的强度在二次冷轧后达到最大而{111}<110>织构组分是在初次再结晶后变强。 Grain shape,size and distribution of { 110} < 001 > Goss grains in CGO steel and the hereditary characteristics of Goss orientated grains during each processing period were investigated,based on the analysis of the microstructure and texture of the CGO silicon steel during hot rolling,intermediate annealing,decarburizing annealing and secondary recrystallization annealing by means of EBSD. The results show that Goss orientated grains exist in the subsurface of the hot rolled plate,and Goss... 

用还原分离-原子荧光光谱法分析了硅钢中的痕量汞.分析方法的不确定度主要来自测量重复性,样品溶液浓度,工作曲线变动性,标准溶液,移取、配制标准溶液,仪器变动性等.文章分别对上述构成合成不确定度大小的分量进行了计算讨论. Trace mercury in silicon steel and galvanized sheet was analyzed by adopting reduced separation-atomic fluorescence spectrometry.The uncertainty of the analysis method mainly comes from measurement repeatability,sample concentration,working curve volatility,standard solution,pipetting and preparation of standard solution,and instrument variability,etc.The essay conducted all calculations and discussions on the above components that determine uncertainty. 

借助光学显微镜、扫描电镜、交流磁性能测量仪和万能拉伸试验机研究了0.3 mm厚高强无取向电工钢冷轧板在780、820、860和900℃退火保温2 min后的组织、织构和性能。结果表明:在退火温度范围内,试验钢均发生了完全再结晶,得到等轴状的铁素体晶粒;随着退火温度的升高,平均晶粒尺寸从9.2μm增长到41.3μm,工频铁损和400 Hz高频铁损均先大幅减小后趋于平缓,磁感应强度先升高后降低。在820℃退火时,铁损P_1.5/50=5.51 W/kg,P_1.0/400=33.22 W/kg均处于较低值,磁感应强度B₅₀₀₀最大,为1.649 T。试验钢的屈服强度和抗拉强度均随退火温度的升高而降低,780℃退火时屈服强度为496 MPa, 900℃退火时降低至407 MPa。综合磁性能和力学性能考虑,试验钢的最佳退火温度是820℃。 Microstructure, texture and properties of 0.3 mm thick high strength non-oriented electrical steel cold rolled sheet annealed at 780 ℃, 820 ℃, 860 ℃ and 900 ℃ for 2 min were studied by means of optical microscope, scanning electron microscopy, AC magnetic property tester and universal tensile testing machine. The results show that in the annealing temperature range, complete recrystallization of the experimental steel occurs and equiaxed ferrite grains are obtained. With the increase of annealin... 

【作者】 马芳； 张春红； ...