硅钢资料

利用EBSD技术研究了电工钢中不同的柱状晶尺寸及退火工艺下{100}织构的演变规律。结果表明,初始晶粒尺寸的影响最显著。细小柱状晶热轧后经过常化处理,组织已均匀,但中心层有强{100}织构。粗大柱状晶中{100}织构的遗传性强,常化及中间退火后,中心层仍有粗大的以{100}取向为主的晶粒;脱碳退火后才能完成组织均匀化和织构梯度的弱化。常化时的升温速度也对织构演变存在影响,低的升温速度有利于{100}织构的保留,但升温速度的影响没有初始晶粒尺寸及退火次数的影响显著。细小柱状晶样品经过热轧及三次退火工艺适合制备取向电工钢。 Evolution of {100} texture of different columnar grains and annealing process was investigated in electrical steels with the help of EBSD technique.The results show that the effect of initial grain size is the strongest.The initial fine-grained specimen shows uniform microstructure after the normalizing process,while {100} grains appear preferentially in the central layer of sheets.The heredity of {100} texture in the initial coarse-grained specimen is more significant.{100} mainly-oriented coar... 

根据现场实际的生产控制情况,指出了热轧原料断面轮廓缺陷以一定的比列遗传给了冷轧带钢,分析了不同热轧原料断面轮廓对冷轧电工钢尺寸精度的具体影响,提出了相应的规律。并阐明了严格控制热轧原料断面轮廓形貌,对保证冷轧电工钢尺寸精度具有重大意义,对于中国现行的冷轧电工钢生产具有指导意义。 Based on the actual situation of production control,it was pointed out that the section profile defects of hot-rolled raw materials were geneticed to the cold-rolled strip.The specific impact analysis for the profile of different hot-rolled raw materials to the dimensional accuracy of cold-rolled silicon steel was analyzed.As a result, the corresponding orderliness are given;And the strict control to section profile of the hot-rolled material is of great significance to ensure the dimensional ac... 

2.9 mm热轧3%Si高牌号无取向硅钢板（/%:0.004 6C、3.04Si、0.32Mn、0.49Als、0.004S、0.013P、0.0042N）由CSP（Compact Strip Production紧凑式带材生产线）流程:120 t BOF-70 mm CC-热轧工艺生产。热轧终轧温度872℃,卷取温度683℃。铸坯及热轧板的组织和夹杂物的分析结果表明,铸坯组织为典型的贯穿柱状晶组织;热轧板边部为再结晶组织,中部为纤维组织带有少量再结晶晶粒;高牌号无取向硅钢的主要夹杂物为铸坯-Al₂O₃,AlN和Cu₂S+MnS;热轧板-Al₂O₃,AlN,AIN+MnS和Cu₂S+MnS。 The 2.9 mm hot rolled 3%Si high grade non-oriented silicon steel plate（/%:0.004 6C,3.04Si, 0.32Mn,0.49Als,0.004S,0.013P,0.004 2N） is produced by CSP（Compact Strip Production） flow sheet i.e.120 t BOF-70 mm CC-hot rolling process with end rolling at 872℃and coiling at 683℃.The analysis results on structure and inclusions in casting slab and hot rolled plate show that the structure of slab is typical trans-columnar crystal,the structure of hot rolled plate at edge is recrystallized grain and in ce... 

研究了退火温度和退火时间对电沉积硅钢试样中的断面层组织、硅在试样中的分布情况、织构分布和磁性能的影响。结果表明:退火温度为1000℃、退火时间为210 min时得到的试样晶粒分布均匀、硅在试样中分布均匀、硅平均浓度为6.3715%(接近6.5%)。试样的织构分析及磁性能检测的结果表明,在较高温度下延长退火时间可增加{100}和{110}面织构,降低铁损,所得试样的磁性能较为良好。 The effect of annealing temperature and time on the microstructure, distribution of silicon,texture and magnetism of the high silicon steel prepared by electrodeposition was investigated. The results showed that after annealing at 1000℃ for 210 min, the mean grain size of steel was about 190 μm with a uniform grain size distribution, and the silicon is also uniformly distributed on the entire cross section with an average Si concentration 6.3715%(close to 6.5%); With the increasing annealing tim... 

【作者】 胡志强； 张文康； ...

研究了硅钢铸坯再加热过程中夹杂物的析出行为。采用非水溶液电解提取+扫描电镜观察方法,观察了试样的显微组织,统计了夹杂物的尺寸、种类、数量、分布。结果表明,均热温度为1 523 K时,水淬试样的夹杂物尺寸绝大部分小于0.5μm,0.5～5.0μm的夹杂物数量很少,没有发现5.0μm以上的夹杂物。此外,均热时间为10、30、60、90、120、240 min时,对应试样中0.05～0.2μm的夹杂物数量分别为4.04×104、4.73×104、3.70×104、3.33×104、3.10×104、1.56×104个/mm3。绝大部分夹杂物以MnS、AlN、CuxS类为主,并以三类夹杂物中的两类复合或三类复合居多。三类复合夹杂物总量占每组试样夹杂物总量的90%或以上。随均热时间延长,典型的夹杂物组成会发生如下变化:MnS+AlN+CuxS MnS+AlN AlN。与此同时,MnS、AlN、CuxS三者复合比例从45.2%(均热10 min)降为9.7%(均热240 min)。 The methods of electrolysis extraction from nonaqueous solution and scanning electron microscope were adopted to study the precipitation behavior of non-metallic inclusions in Si steel slabs during reheating processes.The morphologies,chemical compositions,quantity and size distribution of non-metallic inclusions in these steel samples were analyzed.Results show that,when the soaking temperature is 1 523 K,almost all of the non-metallic inclusions are smaller than 0.5 μm,few are in the range of ... 

晶界和{100}柱状晶在硅钢生产过程中对织构的遗传和演变有关键作用,因此本文利用晶体塑性有限元方法进行立方和旋转立方取向双晶在晶界不同位向时晶体取向演变的全场模拟。模拟显示,三种晶界位向下,晶界都具有诱发晶内产生S形状形变不均匀和缓解局部形变不均匀区取向转动的特点,立方和旋转立方取向双晶在带有剪切作用的轧制条件下都显示明显的取向稳定性。GB⊥RD(表示晶界垂直于轧向)晶界位向时,旋转立方取向晶粒优先在晶界中心位置发生取向转动,而立方取向则优先在远离晶界的端部发生取向转动。GB⊥TD(表示晶界垂直于横向)的晶界位向下,其晶界阻碍作用最小,双晶内产生的取向漫散度大,织构强度较低;除绕TD转动外,也具有复杂的绕RD、ND的取向转动。GB⊥ND(表示晶界垂直于法向)的晶界位向下,取向转动与GB⊥RD时相近,但有少量取向绕ND转动。 Grain boundaries and initial{100}columnar grains play a key role in the inheritance and evolution of texture in the production of electrical steels.In this paper,the crystal plasticity finite element method was used to simulate the grain orientation evolution of cube and rotated-cube oriented bicrystals when grain boundary was set to different orientations.It was shown that the grain boundary in three grain boundary orientations demonstrated the characteristics of inducing Sshape deformation inh... 

本文以热轧常化板为初始材料,采用二次冷轧法与三次冷轧法制备了0.1 mm厚的取向硅钢薄带,测定相应的磁性能,并通过EBSD取向成像技术检测了二次冷轧法与三次冷轧法各工艺过程中织构与组织演变规律。结果表明,采用最终冷轧压下率适中的三次冷轧法,能在冷轧至0.1 mm时保存较多的高斯晶核,使得高温退火后的磁性能明显优于二次冷轧法。最终冷轧压下率通过影响脱碳退火后样品中的{111}<112>织构组分及Goss晶粒数量对最终二次再结晶产生重要影响。 Grain-oriented silicon steel sheets with a thickness of 0. 1 mm were produced from hot-rolled and normalized sheets by two-step-rolling and three-step-rolling methods. Their magnetic properties were measured,and the textures were detected by EBSD technique. The results show that the three-step-rolling method,which has a moderate reduction rate of final cold rolling,can maintain more { 110} < 001 >nucleus,and thus obtaining better magnetic properties compared with the two-step-method. The f... 

【作者】 侯桂芹； 张颖； ...

在实验室模拟CSP工艺条件下制备了取向硅钢,研究了二次冷轧中间退火工艺对组织和织构的影响。结果表明,中间退火温度对取向硅钢脱碳,高温退火组织及织构均产生明显影响。经940℃中间退火后,取向硅钢脱碳再结晶晶粒较850℃中间退火的多,且再经高温退火处理后,晶粒粗化,最大晶粒尺寸达4.8 mm;高斯织构组分密度达27.00,较850℃中间退火试样高。 Grain-oriented silicon steel was prepared by simulated CSP technology in laboratory. Effects of secondary cold-rolled intermediate annealing on microstructure and texture were studied. The results show that intermediate annealing has obvious effects on the microstructure and texture of the steels after decarburization annealing and high temperature annealing. After intermediate annealing at 940 ℃,recrystallized grain of decarburization annealed steel is more than that of intermediate annealed at... 

分别采用传统冷轧轧制液和纳米TiO₂的冷轧轧制液,对无取向硅钢板进行了四辊冷轧实验.重点研究两种冷轧轧制液的轧制润滑性能和对轧后硅钢薄带表面质量和耐蚀性能的影响.通过场发射电子显微镜和能谱仪对使用两种轧制液轧后得到的硅钢薄带表面形貌和成分进行了分析.给出了轧制液中TiO₂纳米粒子在轧制过程中的抗磨减摩机理.在轧制载荷较高时,纳米TiO₂轧制液具有优良的轧制润滑性能并能显著改善轧后硅钢薄带的表面质量.同时在高载荷作用下,TiO₂纳米粒子被压入硅钢薄带基体,形成一个滑动系来支撑载荷,从而使润滑膜的耐磨性提高. Non-oriented silicon steel strips were rolled on a four-high cold rolling mill lubricated by a traditional cold rolling liquid and a nano-TiO₂ cold rolling liquid,with emphasis on studying the rolling lubrication performance of both the liquids and their effect on the surface quality and corrosion resisting property of the silicon steel strips.The surface micrograph and composition of the silicon steel strips after being rolled with both the liquids were characterized by field emissio... 

为提高无取向硅钢导磁性能,研究了不同剪切方式对无取向硅钢剪切处磁畴结构的影响。利用纳米磁流体观测无取向硅钢剪切后边部磁畴结构。结果表明,硅钢无论在机械剪切还是线切割后的边部磁畴都会发生不同程度的改变:线切割对边部磁畴结构改变较小,边部磁畴分布均匀且连续,在距边缘0～20μm范围内出现磁畴宽度变小现象;机械剪切对磁畴的改变较为严重,剪切处磁畴零乱且不连续,在距边缘20μm处仍难以观察到完整的磁畴结构。 The effects of different shearing modes on magnetic domain structure of cold rolled non-oriented silicon steel are studied in this paper.The magnetic domain of cold rolled non-oriented silicon steel is observed by nanometer magnetic fluid pattern method.The results show that the edge magnetic domain structure will be changed by mechanical shear and wire-electrode cutting,the variation of edge magnetic domain structure wire-electrode cutting edge is very small,the magnetic domain structure is wel...