硅钢资料

采用低温板坯加热制备取向硅钢,通过透射电镜(TEM)观察并研究热轧板中的析出物,用ODF织构法研究热轧板距表面1/8、1/4和1/2处的织构分布。结果表明,热轧板中的析出物主要是密排六方AlN,AlN形貌呈规则长方形,AlN颗粒大小不等,分布密度低;热轧板中的织构沿板厚方向,由亚表层的{110}<001>织构向1/2中心层的α线织构变化,其中{110}<001>织构在热轧板距表面1/4层处最强。 The low temperature grain-oriented silicon steels were produced by acquired inhibitor method.The precipitates in hot rolling strip were observed and studied by transmission electron microscope,and the texture distribution in 1/8,1/4 and 1/2 layers of hot rolling strip were analyzed by ODF method.The results showed that the square shaped h-AlN is the main precipitates in hot rolling strip.The precipitates are varying in size and distribution.The texture of hot rolling strip in thick direction are... 

研究了CSP流程试制50W270高牌号无取向硅钢热轧→常化→冷轧→退火过程中织构的演变.利用电子背散射衍射技术对全流程织构进行测量和分析.发现热轧板织构在厚度方向上存在较大差异,表层主要为铜型、黄铜和高斯织构,1/4层存在微弱的高斯织构和旋转立方织构,中心层以γ纤维织构和旋转立方织构为主,还含有较弱的α纤维织构.与热轧板相比,常化板表层和1/4层织构变化不大,中心层旋转立方织构和α纤维织构增强.冷轧板各层均具有α纤维织构和γ纤维织构.与冷轧板相比,成品板各层中α纤维织构基本消失,还出现了立方织构和高斯织构. This article focuses on texture evolution in 50W270 high-brand non-oriented silicon steel produced by CSP in hot rolling,normalizing,cold rolling,and annealing processes.The texture in the whole process was measured and analyzed by electron back-scatter diffraction.It is found that the texture along the thickness direction in hot-rolled strips changes obviously;there are mainly copper,brass,and Goss textures in the surface layer;the 1/4 layer has weak Goss texture and rotating cube texture;γ-fib... 

本发明公开了一种冷轧取向硅钢EBSD用样品电解抛光制样方法，包括：S1.机械抛光，切取10mm*10mm规格试样用超声仪清洗，在不同粒度的砂纸上预磨后在金相试样抛光机上抛光至镜面；S2.电解抛光，利用struerslectropol‑5型电解抛光机对机械抛光好的试样进行电解抛光；S3.EBSD检测。本发明主要解决现有设备技术条件下如何得到高质量的EBSD检测技术样品的问题，适用于大批量冷轧取向硅钢的EBSD样品制备，发明本方法后实验过程简单快捷，节约了实验时间和成本。

研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c... 

在50Kg氧化镁坩埚真空感应炉上进行高硅电工钢的脱氧试验。结果表明,通过控制原料的成分、高真空下的碳氧反应和炉衬分解向钢液中的供氧,可使钢液的总氧含量≤15×10-6;在维持高温高真空条件下,当钢液中的反应达到一定程度后,延长精炼时间并不能降低钢液的总氧含量;完成精炼后加入硅钙合金沉淀脱氧可进一步降低钢液的总含氧量,但脱氧效果有限。 The test of high-silicon electric steel deoxidation has been carried out in 50Kg vacuum induction furnace with magnesium oxide crucible.Results show that the total oxygen could be ≤15×10-6in molten steel by controlling material components,carbon-oxygen reaction in high vacuum and oxygen contamination from crucible materials on molten steel;And when the reaction was carried through to a certain extent,total oxygen in molten steel could not be reduced by the extension of refining period in high va... 

采用电解法和扫描电镜研究了300 t转炉-RH精炼钙处理对无取向硅钢板（%:≤0.005C、1.2～2.2Si、0.2～0.6Mn、≤0.20P、≤0.005S、0.2～0.6Al、0～0.01Ca）中夹杂物的影响。结果表明,钢中Al含量为0.25%和0.35%时,钢中溶解氧均小于1×10^-4%,钙处理后都会产生CaS夹杂物,尤其是含0.35%Al的钢水;钙处理可以有效减少钢中的夹杂物数量,尤其是0.5μm以下的微细夹杂物数量;钙处理后夹杂物的种类以AlN、CaS为主,同时还含有少量的氧化物夹杂物以及AlN-CaS复合夹杂物,尺寸主要为1.5～5.0μm。 The effect of 300 t converter-RH refining calcium treatment on inclusions in non-oriented silicon steel sheet （%:≤0.005C,1.2～2.2Si,0.2～0.6Mn,≤0.20P,≤0.005S,0.2～0.6A1,0～0.01Ca） has been studied by electrolysis and scanning electron microscope.Results show that with 0.25%and 0.35%Al content in steel,all the dissolved oxygen in liquid is less than 1×10^-4%,and the CaS inclusions are produced after calcium treatment,especial for the liquid containing 0.35%Al;the amount of inclusions in ste... 

从影响高牌号无取向硅钢退火工艺的主要参数入手,介绍高牌号无取向硅钢退火炉在加热、气氛控制、冷却、涂层烘烤方面的新技术,并展望无取向硅钢退火炉的发展方向。 Based on the technology parameters of high-grade non-oriented silicon steel annealing,the new technology of the annealing line,which includes heating,atmosphere control,cooling,coating baking,is introduced,and the development direction of non-oriented silicon steel annealing furnace is pointed out. 

本发明提供能够制造磁特性与被膜密合性优异的电磁钢板的新颖并且得以改良的电磁钢板的制造方法。一种电磁钢板的制造方法，其特征在于，其包括以下工序：使电磁钢板与溶液相接触，所述电磁钢板以质量％计含有C：超过0％且0.10％以下、Si：2.5％以上且4.5％以下、Mn：0.01％以上且5.0％以下、S、Se及Te中的1种或2种以上的合计：超过0％且0.050％以下、酸可溶性Al：超过0％且5.0％以下、N：超过0％且0.015％以下、P：超过0％且1.0％以下、剩余部分由Fe及杂质构成，其中，上述溶液含有Cu、Hg、Ag、Pb、Cd、Co、Zn及Ni中的1种或2种以上，各元素的浓度合计为0.00001％以上且1.0000％以下。

采用中、厚板坯生产技术对取向硅钢进行了研制和开发,对热轧及后工序样品进行了金相组织观察和EBSD分析,探讨了两种组织及织构的差异性,研究结果表明:除高温退火样品外,中板坯生产的取向硅钢各工序样品平均晶粒尺寸大;厚板坯生产的取向硅钢热轧和常化样品亚表层Goss织构强;中板坯和厚板坯的脱碳退火板织构没有明显区别。中板坯生产的取向硅钢成本低,产品磁性能和质量与厚板坯相当。 Grain oriented silicon steel was researched and developed by medium thickness slab and thick slab.Microstructures observation and EBSD analysis to the samples of hot rolling and following processes were carried out,respectively.The differences between the two kinds of microstructures and textures were discussed.The results show that the average grain sizes of every process samples are larger except that of high temperature annealing samples of grain oriented silicon steel produced by medium thic... 

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

本实用新型涉及一种硅钢片横剪线用转运系统，包括一暂存组件，所述暂存组件包括一暂存支架，在暂存支架上安装有若干存放条料卷用的凸台；一转运组件，包括一转运底座，该转运底座由第一水平移动机构驱动进行往复移动，在转运底座上安装有一转运支架，所述转运支架由一旋转机构驱动进行转动，且转运支架由第二水平移动机构驱动进行水平移动，在转运支架上安装有一转运托架，所述转运托架由一升降机构驱动上下升降。本实用新型的优点在于：通过暂存组件与转运组件之间的相互配合，实现了条料卷的竖直存放，方便了后续人员选用所需宽度的条料卷，也实现了条料卷的自动流转，有效的降低了人工劳动强度，对于人力资源的消耗也减少了。

本发明公开了一种超高效变频空调压缩机用无取向硅钢薄带及其制造方法，属于无取向硅钢技术领域。本发明包括以下重量百分比的组分：C≤0.003％，Si：2.0％～2.5％，Mn：0.15％～0.5％，Als：0.3％～0.7％，Sn：0.05％～0.11％，S≤0.003％，P≤0.03％，B：0.002％～0.004％，Ca：0.003％～0.005％，N≤0.003％，Ti≤0.003％，其余为Fe及不可避免的杂质，且Mn/S比控制在20～60范围内，B/N比控制在0.7～1.5，Ca/S的比例≥1。为解决现有技术中存在的问题，本发明通过添加合金元素以及偏析元素，配合连铸、热轧、常化和连续退火等热处理工艺，以及优良的冷轧板形控制技术，实现0.30～0.35mm厚度薄规格的高效无取向硅钢产品，具备优异的磁性能和高屈强比的力学性能，满足高效变频空调压缩机电机磁性能和关节式定子高速冲裁对力学性能和板形的高标准要求。