硅钢资料

利用XRD和EBSD研究了长轴分别平行于轧向(RD)、横向(TD)和轧面法向(ND)的柱状晶样品在热轧、冷轧及退火过程中的组织、织构演变规律,并分别从几何诱导和取向诱导两个方面分析了晶界的交互作用.结果表明,热轧时由表面摩擦剪切作用引起的组织和织构梯度直接影响并遗传给后续冷轧及退火样品.热轧后,不同样品的初始晶粒形状各向异性差异消失,形成相同的各向异性晶界组织,但晶体学各向异性发生改变,导致随后冷轧、退火组织及织构的变化均不同于直接冷轧的柱状晶样品.研究中特别关注了对磁性能有利的{100}取向区域与晶界的关系. Columnar grains show their special characteristics of morphological and crystallographic anisotropies, and thus markedly influence the microstructure and texture evolution during rolling and annealing process in electrical steel. The rolling and annealing microstructure and texture of three columnar grained samples with the long axes arranged along different directions were investigated by means of XRD and EBSD techniques, and the effects of columnar grain boundaries were analyzed from the view ... 

以市场上购买的取向硅钢成品板为原料，经不同压下率冷轧至0.23～0.08 mm不等。借助X射线衍射仪(XRD)检测了冷轧后样品中的织构组分及其含量，利用电子背散射技术(EBSD)测量了试样的取向因子分布情况。观察了孪晶的形貌与晶体学特征，分析了硅钢超薄带的塑性变形行为。结果发现，在平面压缩应力下，{112}<111>滑移系的取向因子较大。随冷轧压下率的增加，Goss织构的含量逐渐减少，{212}<141>织构组分的含量先增加后减少，{111}<112>织构组分的含量逐渐增加，织构组分以{110}<001>→{212}<141>→{111}<112>顺序演变。冷轧后样品中出现了孪晶，其晶体取向为{001}<110>,冷轧过程中孪晶取向没有发生变化。 The commercial finished oriented silicon steel plate as the raw material were rolled to 0.23-0.08 mm. With the X-ray diffractometer(XRD), the texture components and their volume fractions in the cold-rolled samples were detected. And the orientation factor distribution of the cross-section of the samples was measured by the electron backscattering technique(EBSD). The morphology and crystallographic characteristics of twins were observed, and the plastic deformation behaviors of the ultra-thin o... 

本发明公开了一种半无机硅钢片漆及其制备方法和应用，其包括：聚酰胺酰亚胺清乳液、二氧化钛、二氧化硅、硫酸钡和氨基树脂，聚酰胺酰亚胺清乳液的制备：在保护气体保护下和回流状态下，使偏苯三酸酐与特定的复合双端氨基化合物在第一有机溶剂中反应，加入磷酸三丁酯、三乙胺，反应；向外蒸出第一有机溶剂，加入第二有机溶剂，加入直链烷基苯磺酸钠、脂肪醇聚氧乙烯醚硫酸钠和脂肪醇聚氧乙烯醚，混合，在搅拌条件下滴加水，滴加完之后，加入双马来酰亚胺进行封端，制成；该半无机硅钢片漆通过将各组分混合超声分散而制成，可在硅钢片中作为覆盖漆应用，且不仅可以采用水作为主体溶剂，环保型好，而且还兼具耐高温、高粘结强度、电气性能强等优点。

用还原分离-原子荧光光谱法分析了硅钢中的痕量汞.分析方法的不确定度主要来自测量重复性,样品溶液浓度,工作曲线变动性,标准溶液,移取、配制标准溶液,仪器变动性等.文章分别对上述构成合成不确定度大小的分量进行了计算讨论. Trace mercury in silicon steel and galvanized sheet was analyzed by adopting reduced separation-atomic fluorescence spectrometry.The uncertainty of the analysis method mainly comes from measurement repeatability,sample concentration,working curve volatility,standard solution,pipetting and preparation of standard solution,and instrument variability,etc.The essay conducted all calculations and discussions on the above components that determine uncertainty. 

本发明特别涉及一种控制边部翘皮的热轧电工钢的生产方法和生产系统，属于钢表面质量检测技术领域，方法包括：建立热轧电工钢边部翘皮的数据库，数据库包括翘皮类型及各翘皮类型的翘皮发生原因和翘皮发生的区域；对待质检的热轧电工钢表面进行识别，并对比数据库，获得待质检的热轧电工钢表面翘皮的翘皮类型；根据待质检的热轧电工钢表面翘皮的俏皮类型获得该类型翘皮的翘皮发生原因和翘皮发生的区域；根据翘皮发生原因和翘皮发生的区域，调整生产操作，用以减少热轧电工钢的边部翘皮；通过对边部翘皮进行准确分类及识别，能够准确的分辨出边部翘皮的产生原因，采取有针对性的措施防止缺陷扩大，最大程度的降低缺陷发生量，提高质量控制水平。

一种取向硅钢极薄冷轧板钢带的焊接系统及方法，于该系统内设有焊轮及与焊轮电连接的焊接控制器；所述焊轮由前后呈直线布设的主焊轮、副焊轮构成；所述焊接控制器由分别与主焊轮电连接的第一焊接控制器、与副焊轮电连接的第二焊接控制器构成。所述焊接基于单排焊，仅使用一次焊接行程，通过设置的第一次焊接与第二次碾压焊接依次作业完成。本发明的一种取向硅钢极薄冷轧板钢带的焊接系统及方法，针对取向硅钢极薄钢带冷轧板焊接的问题，对传统电阻焊焊机拥有的碾压轮改造及建立的相应焊接工艺。平衡了热量积累与质量保证两者，解决了取向硅钢极薄钢带冷轧板焊接容易发生虚焊、爆焊和焊接时间长等问题。同时和传统电阻焊焊机相比焊接工艺窗口更大，焊接效率更高。

本发明公开了一种降低取向硅钢铁损的方法。本发明所述方法包括如下步骤：(1)将取向硅钢样品腐蚀，清理后，拍摄得到晶粒分布图；(2)计算平均晶粒大小S，确定刻痕间距；刻痕间距与晶粒大小S的关系为：S＜600mm2时，刻痕宽度为5.0mm；600≤S＜1000mm2时，刻痕宽度为4.5mm；1000≤S＜1400mm2时，刻痕宽度为4.0mm，S≥1400mm2时，刻痕宽度为3.5mm。本发明通过计算不同来料晶粒大小确定其刻痕间距的大小，通过对刻痕间距的调整，降低了取向硅钢的铁损。

结合实际生产0.4%Si无取向硅钢，统计了不含Sn和0.025%Sn无取向硅钢的磁性能变化，利用金相显微镜、X射线衍射仪观察分析不同成分下试样的显微组织和微观织构。试验结果表明：Sn元素可以显著降低无取向硅钢的晶粒尺寸，0.025%Sn试样的平均晶粒尺寸比不含Sn减小28.4%;加入Sn元素后抑制了无取向硅钢中不利于磁性能的{111}面织构组分强度，提高了对磁性能有利的{100}面织构组分强度，0.025%Sn与不含Sn相比磁感均值从1.756 T提升至1.768 T,铁损均值从5.476 W/kg降低至5.204 W/kg,明显改善了无取向硅钢磁性能。 In this paper combined with the actual production of 0.4% Si non oriented silicon steel, the magnetic properties of non oriented silicon steel without Sn and 0.025% Sn were counted. The microstructure and microtexture of samples with different compositions were observed and analyzed by metallographic microscope and X-ray diffraction. The results show that: Sn can significantly reduce the grain size of non oriented silicon steel, and the average grain size of 0.025% Sn sample is 28.4% smaller tha... 

介绍了硅钢氧化镁制备方法及高质量硅钢氧化镁制备技术的研究进展,并对利用我国丰富的卤水资源制备硅钢氧化镁进行了展望。 The preparation methods of silicon steel magnesium oxide and research progress of high quality silicon steel magnesium oxide preparation technology were introduced.The use of abundant brine resources in the preparation of silicon steel magnesium oxide was prospected. 

{100}织构因具有两个易磁化方向能够明显的提高磁性能,因此如何在表面获得具有{100}织构一直是无取向电工钢研究焦点。本文主要介绍了获得{100}织构的主要工艺方法及其基本原理,并结合实际生产过程对各工艺方法的优缺点进行了分析;一方面,优化无取向电工钢的成分,降低碳、锰元素含量以避免脱碳退火和真空退火,简化生产工艺;另一方面,调节升温速度、降温速度和退火气氛,使{100}晶面的表面能或弹性应变能最低,制备具有{100}织构柱状晶组织的无取向电工钢是今后的发展方向。 Because { 100} texture has two easy magnetization directions,which can significantly improve magnetization properfies,how to develop { 100} texture is a focus for researchers and manufactures. In the paper,main manufacturing processes and basic principle are introdued,and their advantages and disadvantages in practical production are analyzed. On the one hand,the production process can be simplified by optimizing chemical compositions,such as reducing the content of C and Mn,which can avoid deca... 

本实用新型公开了一种硅钢片焊接模具，包括底座，底座上均匀排布有多条滑槽，每条滑槽内连接有一根垂直设置的定位杆，定位杆底部穿过底座连接一气缸，气缸连接在底座底部。本实用新型结构设计合理巧妙，移动不同位置的定位杆，将定位杆与硅钢片贴合，不同滑槽内的定位杆之间相互错位，并利用气缸将硅钢片定位，这种结构不可以适用于各种形状的硅钢片，使用方便快捷。

针对攀钢高硫铁水冶炼现状,结合不同生产工艺路线,论述了攀钢近年来为实现低硫电工钢的生产,在铁水预处理、转炉冶炼、钢水精炼过程中硫控制技术的开发与应用,形成了低硫洁净钢生产工艺技术,实现了低硫电工钢的生产。低硫电工钢RH脱硫率可达到20%左右,成品[S]控制在0.006%左右。 According to the smelting situations of hot metal with high sulphur content at Panzhihua Steel,combined with different produce processes,technologies for controlling the sulfur content during hot metal pretreatment,converter smelting,and second refining are developed. Technologies in low-sulfur clean steelmaking are formed. Low-sulfur electric steel are produced. As for the desulfurization rate of lowsulfur electric steel can reach about 20%,and the content of [S] in products is controlled to ab...