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研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%~100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 
2011-05-28 117 5.8

利用EBSD技术研究了电工钢中长轴平行于轧向的柱状晶样品在热轧和退火过程中组织和取向的演变规律,并与长轴平行于板法向的样品的已有研究结果进行对比。结果表明,无论柱状晶按何种方向排列,只要表面存在剪切力,热轧后都可形成剪切织构,同时中心形成轧制织构,主要包括旋转立方织构和{112}<1-10>。柱状晶造成的影响主要体现在板中心层,长轴平行于轧向排列的样品热轧时形成的粗大旋转立方晶粒要到脱碳退火后才能完全消除,但破坏了正常的不同取向晶粒间的取向差分布及尺寸均匀性,导致二次再结晶不完全及磁性能降低。 The evolution of microstructure and grain orientation in an electrical steel containing columnar grains with its long axis being parallel to the rolling direction of sheet was studied during hot rolling and annealing by EBSD technique.The results are compared with those of samples containing columnar grains being parallel to normal direction of sheet reported in the reference [3].It was shown that,whether the long axis of columnar grains was arranged in RD or ND,shear textures can be formed in t... 
2011-02-28 117 5.8

本实用新型公开了用于变压器铁芯硅钢片的叠片翻转支架,包括槽板,所述槽板内部卡装有转板,转板两侧对称安装有卡杆,槽板底部安装有风扇;所述转板另外两侧对称安装有放置槽,放置槽底部卡装有电磁铁,转板两侧皆设置有两组开关;在开关不受到压力时,此时开关所在电路处于通电状态,开关与电磁铁为电性连接,每个开关独立控制一组电磁铁,电磁铁处于工作状态,电磁铁正常运行产生的磁吸力,使得铁芯硅钢片固定在放置槽内,在使用机械臂取用铁芯硅钢片时,机械臂底部连接的触发条持续压迫开关,此时开关所在电路处于断路状态,开关所控制的相应电磁铁不产生磁力,机械臂可以较为容易的取用铁芯硅钢片。
2021-12-28 117 6.8

对CSP流程生产的高磁感无取向电工钢50W1300在偏离轧制方向不同角度处的磁性能进行了测试和分析。结果表明:在偏离轧向不同角度处,磁性能差异显著,尤其在α=60°时磁感最低;偏离轧制方向不同角度处的磁性能大小取决于织构类型、强度及分布状态;增强{100}<0vw>和α、η取向的有利织构组分,降低不利的γ取向织构组分,且使有利织构组分分布越漫散,磁各向异性越小。 Magnetic properties of high magnetic induction non-oriented electrical steel 50W1300 produced by CSP processes were investigated with different direction in relation to the rolling direction.The result shows that magnetic properties are significantly different in relation to the rolling direction,in particular,the minimum magnetic induction occurs at 60° in relation to the rolling direction.Magnetic properties of different directions in relation to rolling direction depend on type and distributi... 
2011-04-28 117 5.8

绝缘涂层可以有效提高硅钢片的耐蚀、耐腐、磁、绝缘等性能,因此取向硅钢涂装绝缘涂层是取向硅钢生产过程中重要的一环。本文对取向硅钢含铬无机绝缘涂层以及氮化铬涂层的性能优缺点进行了介绍,并对国内无机含铬取向硅钢绝缘涂层及氮化铬涂层的研究现状进行了综述。最后对未来含铬无机绝缘涂层的研发方向进行了展望。 Insulation coating can effectively improve the corrosion resistance of silicon steel sheet, such as corrosion, magnetic, insulation performance, thus oriented silicon steel insulation coating is the important part of oriented silicon steel production process. In this paper, the inorganic insulation coating oriented silicon steel containing chromium and chromium nitride coating performance advantages and disadvantages are introduced.In addition, the research status of insulation coating and chrom... 
2022-02-28 117 5.8

本发明属于涂料技术领域,具体涉及一种用于硅钢水性无机绝缘涂料的助剂及其制备方法,用于硅钢水性无机绝缘涂料的助剂,包括以下质量份配比的材料:磷酸二氢铝溶液10‑40份、氧化镁0.1‑5份、增稠剂0.01‑5份和水1‑80份。本发明还提供了上述助剂的制备方法,通过向磷酸二氢铝溶液中加入氧化镁悬浮液,得到铝镁混合液备用,然后在室温及搅拌条件下,向铝镁混合液中加入增稠剂预溶胶得到所需助剂,利用本申请的助剂制备了无机物料,结果表明,本发明提供的助剂适用于硅钢水性无机绝缘涂料,能改善涂料的稳定性,有效提高硅钢绝缘涂层的附着力和耐腐蚀性,改善硅钢涂层的综合性能。
2021-05-28 116 6.8

提供一种可以制造具有优异特性的变压器的、兼顾低铁损和良好的磁致伸缩特性的方向性电磁钢板。本发明的方向性电磁钢板具有在与轧制方向交叉的方向上线状延伸的线状应变区域,线状应变区域具有在轧制方向上具有压缩应力的区域,在与该具有压缩应力的区域的轧制方向邻接的区域具有在轧制方向上具有拉伸应力的区域。
2020-12-23 116 6.8

从影响高牌号无取向硅钢退火工艺的主要参数入手,介绍高牌号无取向硅钢退火炉在加热、气氛控制、冷却、涂层烘烤方面的新技术,并展望无取向硅钢退火炉的发展方向。 Based on the technology parameters of high-grade non-oriented silicon steel annealing,the new technology of the annealing line,which includes heating,atmosphere control,cooling,coating baking,is introduced,and the development direction of non-oriented silicon steel annealing furnace is pointed out. 
2013-02-28 116 5.8

研究了冷轧大压下量,950℃退火时间对一种新型含铜无取向电工钢晶粒度和织构的影响。结果表明,大压下量冷轧,随压下量的增加,退火晶粒向γ线聚集,形成强{111}<112>织构。提高冷轧压下率,退火织构{111}<100>,{110}<001>强度减弱,增加退火时间,退火织构{111}<110>,{100}<001>,{110}<001>强度变弱。采用87.5%冷轧压下率和950℃退火60 s,有利织构{100},{110}占有率最大。 The effect of annealing(950 ℃) time with high cold rolling reduction on grain size and texture of a new non-oriented electrical steel containing copper was investigated.The results show that for high cold rolling reduction,most annealed grains are oriented along γ-fibre with increasing cold rolling reduction ratio and strong texture {111}<112> is formed.With increasing the cold rolling reduction ratio,the intensity of annealed texture {111}<110>,{011}<100> decreases.With increa... 
2011-01-28 116 5.8

本发明公开了一种控制无取向硅钢厚度稳定性的轧制工艺,涉及硅钢厚度控制方法领域。本发明通过降低硅钢精轧入口温度,并调节粗轧区域、精轧区域和卷取区域的生产参数,保证后续卷取工序的轧制稳定性及卷形质量,严格控制无取向硅钢的厚度稳定性。本发明提供的轧制工艺使硅钢的厚度命中率得到了明显提升,提升了后续冷轧工艺的轧制速度,轧制力波动减小,提高了产品质量。
2021-01-07 116 6.8

研究了常化对CSP流程生产的wSi=1.6%的无取向电工钢组织、织构和成品磁性能的影响。结果表明,经CSP流程生产,且在相同的冷轧及退火制度下,经1 000℃×2min常化处理的wSi=1.6%的无取向电工钢热轧板,其最终退火成品的铁损P15/50比不常化试样下降了10.5%,磁感B50比不常化试样提高了2.5%;常化使wSi=1.6%的无取向电工钢成品的平均晶粒尺寸增大,成品铁损P15/50相应减小;同时,常化使wSi=1.6%的无取向电工钢成品中高斯织构的强度增加,γ纤维织构的强度减弱,这有利于成品磁感B50的提高。 The effect of normalizing on microstructure,texture and magnetic properties of non-oriented electrical steel with wSi=1.6% produced by CSP process was investigated.The results show that,under the same cold rolling and annealing system,the iron loss(P15/50) of annealed samples whose hot bands has been normalized by 1 000 ℃×2 min process decreases by 10.5% and magnetic induction(B50) increases by 2.5% compared with the samples whose hot bands was not normalized.The average grain size of non-orient... 
2012-11-28 116 5.8

本发明公开了一种普通级稀土取向硅钢制备方法,通过添加稀土元素,利用第二相作用,对铸坯组织、热轧组织、初次再结晶晶粒和二次再结晶晶粒的影响,改善成品磁性能,即降低铁损,提高磁感。
2021-11-25 116 6.8

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