硅钢资料

6.5%Si硅钢具有优异的磁学性能和广泛的应用前景。本文综述了6.5%Si硅钢的物理、机械及磁学特性,讨论了传统轧制、温轧、薄带连铸、快速凝固、CVD、粉末轧制等不同制备工艺的关键技术及特点,概括了6.5%Si硅钢在高效节能电机、汽车马达及磁屏蔽等领域中的主要应用,介绍了硅钢的制备技术取得的研究进展,并指出了其广阔的发展前景。 6.5% Si silicon steel has good magnetic properties and wide applications.In this paper physical and mechanical magnetic properties were summarized,and key technology and characteristic of several preparation methods,such as traditional rolling,warm rolling,thin strip continuous casting,rapid solidification,CVD and powder rolling,were discussed.Main applications of 6.5% Si steel in the fields of high-efficiency electrical motors,automobile motors,transformer cores and magnetic shielding were gene... 

利用光学显微镜、TEM和EBSD研究了退火温度对双辊连铸无取向硅钢再结晶组织的影响。结果表明,900℃退火后组织分布不均匀,有大量带状组织,平均晶粒尺寸29.5μm。提高退火温度,晶粒尺寸增大,组织均匀化程度增加,1050℃退火时,带状组织基本消失,平均晶粒尺寸42.2μm。 Effect of annealing temperature on recrystallization microstructure of non-oriented electrical steel produced by twin-roll casting process was investigated using OM,TEM and EBSD.The results show that the recrystallization microstructure is uneven because of many banded grains existing,average grain size is 29.5 μm.With annealing temperature increasing,the recrystallization grain size increases,microstructure becomes more homogeneous.When 1050 ℃ annealing,the banded structure almost disappear and... 

【作者】 吴玉美； 陆晔； ...

研究了取向硅钢制备过程中常见的两种冷轧工艺,主要研究了一阶段冷轧与两阶段冷轧+中间退火工艺对初次再结晶组织及织构的影响.结果表明:采用两阶段冷轧+中间退火工艺制备以Cu2S为主抑制剂的取向硅钢,其初次再结晶平均晶粒尺寸为18.1μm,高斯晶粒的体积分数为0.6%,迁移性强的重位点阵晶界(Σ5+Σ9)和高能晶界(20°~45°取向偏差角)所占比例分别为1.8%和50.4%.与一阶段冷轧工艺相比,其初次再结晶晶粒较细,且高斯晶核与特征晶界所占的比例较高,有利于高斯晶粒发生二次再结晶. Two common cold-rolling processes of grain oriented silicon steel and the effects of the single stage cold rolling and tw o-stage cold rolling w ith intermediate annealing processes on the primary recrystallization microstructure and texture w ere investigated. The results revealed that for the grain oriented silicon steel prepared under the tw o-stage cold rolling process w ith intermediate annealing w ith Cu 2 S as the main inhibitor,the average grain size of the primary recrystallization micr... 

利用电子探针面分析、状态分析及电子背散射衍射相分析技术研究硅钢高温氧化铁皮的显微结构。电子探针面分析可以直观的看出元素的分布状态,初步判断氧化铁皮的结构,而状态分析可以准确表征常规氧化铁皮中铁元素的状态,对于合金元素富集区域则通过电子背散射衍射相分析技术来标定。结果表明,高温氧化铁皮的结构主要有4层,即最外层为厚度约为10μm的Fe2O3相,次外层为Fe3O4相,中间层为FeO相上分布有颗粒状的Fe3O4相,最内层为FeO相和Si元素富集的Fe2SiO4相。其中Fe2SiO4层的分布特征与加热温度密切相关:1 100℃时,Fe2SiO4相呈颗粒状,弥散分布在FeO层;1 200℃时,Fe2SiO4相呈液态,侵入基体和疏松的FeO层,且沿着FeO晶界呈网状分布。 The microstructure of high temperature oxide scale on silicon steel was characterized by electron probe microanalyzer(EPMA)mapping analysis,state analysis and electron backscatter diffraction(EBSD)phase analysis.The element distribution and the initial structure of the oxide scale could be detected by EPMA mapping analysis apparently.And the state of iron in the conventional oxide scales could be determined by state analysis.Meanwhile,the alloy-rich region could be identified by EBSD phase analy... 

利用OM、TEM与EDS技术,对Fe-3.2%Si低温取向硅钢热轧板进行不同常化冷却工艺处理后的显微组织、析出相及最终产品的磁性能进行分析,并与热轧板的组织和析出相进行对比。结果表明,常化板较热轧板的表层组织均匀,基体中再结晶比例增加,带状组织变窄;常化板中析出物的数量明显比热轧板的多,析出物主要有AlN、MnS及复合析出的(Cu,Mn)S等。在常化温度1120℃、保温3 min的条件下,采用二段式冷却较空冷、淬沸水、淬常温水的冷却工艺,常化板表层显微组织更均匀,沿板厚方向的显微组织的不均匀性显著,取向硅钢的磁性能最高;常化后采用二段式冷却工艺析出的细小析出物数量最多,且弥散分布在基体中,抑制剂的抑制效果最好,对成品获得高磁性最有利。 Microstructure, precipitate and magnetic characteristic of final products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy(OM), transmission electron microscopy(TEM), and energy dispersive spectrometry(EDS). The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are nar... 

【作者】 陶永根； ...

两炉次无取向硅钢XG800WR（/%:0.003～0.004C、0.71～0.75Si、0.32～0.33Mn、0.004～0.007S、0.016P）的炼钢流程为铁水预处理（KR）-210 t顶底复吹转炉-钢包吹氩-RH脱碳精炼-230mm×1220 mm板坯连铸。53 t中间包钢水过热度为25～30℃,钢包到中间包采用长水口全程吹氩保护浇铸,中间包至结晶器采用浸入式水口浇铸。结果表明,在RH、中间包、结晶器过程中钢中总氧以及夹杂物数量和尺寸均明显降低;但在钢包到中间包过程T[O]、[N]和钢中夹杂物数量增加,说明长水口浇铸过程存在二次氧化。连铸坯中T[O]、[N]平均他分别为11×10^-6和30×10^-6,显微夹杂物数量平均为4个/mm²。铸坯中的显微夹杂物主要为3～5μm的AlN,同时存在少量的MnS、Al₂O₃·AlN和Al₂O₃·MgO·MnS。 The steelmaking flow sheet for two heats non-oriented silicon steel XG800WR（/%:0.003～0.004C. 0.71～0.75Si,0.32～0.33Mn,0.004～0.007S,0.016P） is hot metal pretreatment（KR）-210 t top and bottom combined blown converter-ladle argon blowing-RH decarburization refining-230 mm×1 220 mm slab casting.The superheating extent of liquid in 53 t tundish is 25～30℃,whole casting is shielded by blowing argon with long nozzle from ladle to tundish and the submerged nozzle is adopted in casting from tundish to mold... 

以水氯镁石为原料,采用氨法沉镁-煅烧-添加剂的方法制备硅钢级氧化镁。考察了反应温度、反应pH值、陈化时间对中间体氢氧化镁纯度及转化率的影响;研究了煅烧温度和煅烧时间对氧化镁水化率的影响及添加剂的量对氧化镁悬浮性能的影响。控制实验条件为:反应温度55℃,pH值为9.5,陈化时间2h,煅烧温度1050℃,煅烧时间2h,添加剂量为0.8%,制得氧化镁的纯度为98.99%、水化率为2.92%、悬浮性能为3mm/h,达到硅钢级氧化镁的要求。 Using bischofite as raw material,the preparation of magnesium oxide with silico-steel grade was studied.The effects of reaction temperature,reaction pH value and aging time on the intermediate magnesium hydroxide purity and conversion rate were studied.Calcinations temperature,calcinations time relationship to the hydration rate of MgO and amount of additive to the suspension performance of MgO were investigated.The results indicated that the optimum technological conditions were as follows:reac... 

为了优化激光刻痕降低取向硅钢铁损的工艺,寻找刻痕速度、脉冲能量、扫描间距等重要刻痕参数的最佳匹配关系,提出了一种基于人工神经网络与遗传算法的优化模型,并利用这种模型对30Q130取向硅钢材料的刻痕工艺进行了优化实验,结果表明,这种模型稳定可靠,可以作为取向硅钢刻痕工艺优化的一种有效的措施。 A laser is often considered to scribe the grain-oriented silicon steel surfaces after cold-rolling and annealing to reduce the core loss.It is necessary to select the best scribing parameters to maximize the reduction in this process.This paper proposes an optimization method of genetic algorithm during laser scribing of 30Q130 steel,by developing an artificial neural network prediction model using a database form a designed orthogonal experiment.The objective is to determine the best combinatio... 

常化快冷是生产高牌号无取向硅钢和高磁感取向硅钢不可缺少的一个工艺环节,气-雾冷却则是实现常化快冷的关键方式之一。介绍了国内自主设计建设的常化酸洗机组气雾冷却系统的技术特性,并对其特点进行了系统分析,最后给出该系统在设计、运行参数的选择上若干注意事项,对气-雾冷却系统设计和使用具有一定的指导作用。 The normalizing rapid cooling is a indispensable process to high grade non-oriented silicon steel and high magnetic induction oriented silicon steel’ s production. The fog cooling is a key ways of coming true the normalizing rapid cooling. This paper introduces the technical features of the fog cooling system in normalizing pickling line which is the domestic independent design and construction. Meanwhile,the fog cooling system’s characteristic is analyzed systematacially. In the end,this paper ... 

通过固溶度积公式计算及热模拟实验,对不同热装和加热温度条件下的无取向硅钢铸坯中析出相进行了研究.在低于950℃热装时,铸坯中AlN的析出量和尺寸不再变化,但MnS和AlN-MnS的数量及平均尺寸随着热装温度降低而进一步增加,并在温度低于600℃时达到最大值后保持不变.与1200℃相比,1100℃加热的铸坯中AlN、MnS的总固溶量相对更少.相比850℃热装,600℃热装再加热到1100℃的铸坯中AlN和MnS的总固溶量更少,且AlN和MnS尺寸更大.合适的热装温度和加热温度分别为600℃和1100℃. Based on solubility product calculation and thermal simulation experiments,precipitated phases in continuous casting slabs of non-oriented silicon steel were systematically studied at different hot charging and heating temperatures.When the hot charging temperature is below 950 ℃,the content and size of AlN remain unchanged,but the quantity and size of MnS and AlN-MnS increase when the hot charging temperature decreases,reach maximum and remain unchanged when the hot charging temperature is belo...