钢厂
辉光放电发射光谱法测定硅钢薄板中微量硼元素
通过对辉光放电发射光谱参数的优化,以铁元素为内标来消除基体效应,建立了测定硅钢薄板中微量硼元素的方法。优化的实验参数为:放电电压1200 V,放电电流50 mA,预溅射时间40 s,积分时间10 s。校准曲线硼元素含量范围0.0001%~0.022%,相关系数大于0.999,测量结果与认定值一致,相对标准偏差小于10%。完全能够满足日常分析测试的要求。 A glow discharge optical emission spectrometry(GD-OES) method for determining trace boron element in silicon steel sheets were established through optimization of instrumental parameters and using Fe element as an internal standard to eliminate the matrix effect.The optimized instrumental parameters included discharge voltage,discharge current,pre-sputtering time and integration time,which are 1200 V,50 mA,40 s,and 10 s,respectively.The content of boron element that can be determined from the ca...
CN202111069865.X一种改善高牌号无取向硅钢冷轧断带的控制方法
本发明涉及无取向硅钢技术领域,尤其涉及一种改善高牌号无取向硅钢冷轧断带的控制方法。按重量百分比计:[Si+Al]≥4.0%;Mn、S含量满足:S≤0.0015,[Mn]/[S]:200~400;1)热轧过程中使用保温罩,热轧轧制时投入边部加热,头尾100米内卷曲温度提高15~30℃;2)常化机组圆盘剪进行边部剪边前增加加热装置,剪切后增加毛刺打磨装置,采用煤气明火加热,保证钢板温度在韧脆转变温度以上;3)圆盘剪间隙满足关系式:ds=(0.15~0.45)d0ds:圆盘剪间隙,μm;d0:常化板板厚,mm;4)常化采用快速加热,控制钢带的预热段升温速度320~380℃/min,机组速度20~30m/min;5)常化工艺后,控制边部小于20μm的晶粒占比在5%以内。有效的减少了冷轧断带的发生,提高成材率1.30%以上,降低了生产成本。
高效电机用无取向电工钢组织和析出物研究及产品开发
为开发高效电机用冷轧无取向电工钢,借助实验室薄板坯连铸连轧模拟设备及扫描电镜、透射电镜等检验手段研究了成分、组织、织构和析出物等对无取向电工钢磁性能的影响规律;结果表明:常化处理使组织均匀化并增加有利于磁性提高的织构组分;采用CSP流程开发的高效电机用无取向电工钢铁损平均值3.4 0 W/kg,磁感≥1.68 T。 In order to develop electrical steel for high efficiency motor,effect of components,microstructure,texture and precipitation on magnetic property of electrical steel are analyzed.From the result,normalizing treatment makes microstructure uniform and increases component of favorable texture.Iron loss of electrical steel developed by CSP line is 3.40W/kg and magnetic induction is more than 1.68T.
CN202111010835.1一种无取向电工钢清洗工艺
本发明公开了一种无取向电工钢清洗工艺,包括以下步骤:1)在脱脂剂箱体中添加脱脂剂溶剂,通过喷射泵将脱脂剂分别从上下两路管道喷出,经过流量控制电磁阀进入喷射梁,通过喷嘴喷洒在带钢表面;2)带钢轧制后温度为100~150℃,速度为600~1000m/min,带钢表面高温确保脱脂剂与带钢表面残留油脂反应充分,且在高速下喷射的脱脂剂与带钢相向而行,使带钢表面反应后残留硅泥、铁粉被迅速带走;3)喷射后的脱脂剂流入收集槽中,通过泵重新打入脱脂剂箱体中,实现脱脂剂的循环利用。其利用轧制时产生的高温及高速对带钢表面残留乳化液斑迹、铁粉、硅泥进行清洗,清洗彻底高效。
二次冷轧法与三次冷轧法制备取向硅钢薄带的织构转变规律
本文以热轧常化板为初始材料,采用二次冷轧法与三次冷轧法制备了0.1 mm厚的取向硅钢薄带,测定相应的磁性能,并通过EBSD取向成像技术检测了二次冷轧法与三次冷轧法各工艺过程中织构与组织演变规律。结果表明,采用最终冷轧压下率适中的三次冷轧法,能在冷轧至0.1 mm时保存较多的高斯晶核,使得高温退火后的磁性能明显优于二次冷轧法。最终冷轧压下率通过影响脱碳退火后样品中的{111}<112>织构组分及Goss晶粒数量对最终二次再结晶产生重要影响。 Grain-oriented silicon steel sheets with a thickness of 0. 1 mm were produced from hot-rolled and normalized sheets by two-step-rolling and three-step-rolling methods. Their magnetic properties were measured,and the textures were detected by EBSD technique. The results show that the three-step-rolling method,which has a moderate reduction rate of final cold rolling,can maintain more { 110} < 001 >nucleus,and thus obtaining better magnetic properties compared with the two-step-method. The f...
热轧工艺对TSCR流程生产取向硅钢组织和性能的影响
取向硅钢热轧板中组织、织构梯度对发展完善的二次再结晶十分关键,通过对2种不同热轧工艺生产取向硅钢的组织、织构进行研究,结果表明:采用后道次大压下热轧工艺时热轧板表层再结区晶粒平均尺寸增加,再结晶区厚度增加,高温退火后二次晶粒尺寸减小;采用后道次大压下热轧工艺热轧时,热轧板中平均等效应变高,热轧板厚度心部{100}〈011〉和{100}〈001〉位向取向强度降低,({111}~{113})〈110〉位向取向强度提高,高温退火后{110}〈001〉位向偏离角降低,磁性能提高。 The texture and microstructure gradient in hot rolled grain oriented silicon steel strip was one of the essential factors to achieve a perfect secondary recrystallization.The texture and microstructure of grain oriented silicon steel strip as-rolled with two different hot rolling parameters was investigated.The results show that with big reduction at the end rolling process,the intensity of {100}〈011〉 and {100}〈001〉 orientation reduces with({111}-{113})〈110〉 orientation intensity enhanced in hot...

