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本发明公开了一种取向硅钢微观织构EBSD试样制样方法,包括:1)取样,采用线切割机制取向硅钢试样;2)制样,采用热镶嵌机镶制取向硅钢试样,按照常规方法进行粗磨、细磨、抛光、清洗、吹干;采用240目、400目、600目氧、800目、1000、2000目氧化铝砂纸对试样依次进行一次打磨处理;采用5.0um高效金刚石抛光剂对试样进行抛光处理;3)电解抛光,取向硅钢试样机械抛光后再进行电解抛光。
2021-02-04 144 6.8

通过实验室25 kg真空感应炉冶炼和锻轧研究了0.26%~0.95%Al含量对0.5 mm 2.2%Si无取向硅钢冷轧板组织、织构和磁性能的影响。试验结果表明,0.26%~0.81%Al含量时,随钢中Al含量的增加,成品退火钢板的晶粒尺寸增加同时铁损减少;当Al含量大于0.81%时,随Al含量增加,钢板的晶粒尺寸减小,同时铁损增加。Al含量对硅钢板磁感的影响没有明显的规律。2.2%Si无取向硅钢的合适Al含量为0.48%~0.81%。 The effect of 0.26%~0.95%Al content on structure,texture and magnetic performance of 0.5 mm cold rolled sheet of 2.2%Si non-oriented silicon steel has been studied by a 25 kg vacuum induction furnace smelting,and forging -rolling in laboratory.Results show that as 0.26%~0.81%Al,with increasing Al content in steel the grain size of annealed finished sheet increases while iron loss of sheet decreases,and as Al content in steel is more than 0.81%,the grain size of sheet decreases while iron loss in... 
2011-06-28 134 5.8

本实用新型实施例涉及一种硅钢片冲剪设备,该设备包括冲床、送料台、第一刀模、第二刀模和第三刀模;送料台用于传送待加工的硅钢条;第一刀模用于冲剪硅钢条以在硅钢条上形成预设形状的第一凹槽,第一凹槽处构成“工”字形硅钢片的一侧凹部;第二刀模用于冲剪硅钢条以在硅钢条上形成预设形状的第二凹槽,第二凹槽与所述第一凹槽相对应,第二凹槽处构成“工”字形硅钢片的另一侧凹部,第二刀模与硅钢条在硅钢条的横向方向上能够产生预设距离的相对位移;第三刀模用于沿硅钢条的横向方向剪断硅钢条。该设备能够采用硅钢片低成本、高效率地制造“工”字形硅钢片。
2021-04-14 130 6.8

采用硅钢自动测量装置及X射线衍射仪检测出样品在实验前后的磁性能参数和织构强度.结果表明:较低的电压、9 Hz、较长的处理时间以及退火温度为650℃有利于增高铁损降低比例;较低的电压、较高的频率以及退火温度为650℃有利于增加磁感应强度增高比例.最佳的提高磁性能的实验参数是:频率为9 Hz,电压为500 V,处理时间为6 min,退火温度为650℃.通过织构分析可以验证:取向硅钢磁感应强度的变化取决于{110}<001>晶粒取向度值,而{110}<001>取向度值可看成是一个反映总体平均偏离角大小情况的综合值. An automatic measurement system for silicon steel and an X-ray diffraction meter were used for measuring the magnetic property parameters and texture of ex-processed samples and processed samples.It is shown that under the condition of a lower voltage,9Hz,a longer processed time and an annealing temperature of 650℃,the decrease rate of iron loss can be increased;a lower voltage,a higher frequency and an annealing temperature of 650℃ are in favor of improving the increase rate of magnetic inducti... 
2011-08-28 129 5.8

采用\"热轧复合+冷轧减薄+退火\"方法成功制备了0.20mm厚的硅浓度梯度高硅钢薄带,并采用SEM和X射线衍射技术对制备过程中组织和织构演变进行了研究。热轧复合板微观组织呈明显层状分布,复合界面为紧密冶金结合且经过83%的大冷轧变形未开裂。热轧和冷轧复合板带中均形成强α和γ织构,再结晶退火后形成强γ织构。冷轧和退火织构沿板厚呈显著的梯度分布特征,其主要来自于复合界面两侧硅浓度和初始热轧织构的差异性以及冷变形的不均匀性。 Gradient high silicon steel thin sheets with thickness of 0.20 mm were successfully produced by the rolling and annealing method,including hot rolling bonding,cold rolling,and annealing.Microstructure and texture evolution was investigated by means of SEM and X-ray diffraction.Microstructure of hot-rolling-bonding shows obviously layered distribution,the composite interface was closely metallurgical bonding and no cracking appears even after 83%cold rolling.Strongαandγfibers develop in the hot a... 
2023-05-09 185 5.8

本发明涉及一种超纯净无取向冷轧硅钢中非金属夹杂物形貌的原位观察方法,包括如下步骤:制备无取向冷轧硅钢样品,将待测试面用打磨至1000#,使样品表面平整光滑,并进行机械抛光和表面清洗。对处理好的样品在电化学工作站上进行电化学腐蚀,电解液为:1~8wt%氯化物MCl溶液,余量为去离子水,通入CO2气体至饱和,加入适量NaHCO3和三乙醇胺作为稳定剂调节pH值将其稳定在6.0~6.5之间。电化学设定参数:开路:0.5~2h,动电位极化测试:扫描速率:0.1mV/S~1.0mV/S,测试区间:VS.SCE‑0.8V~0.2V,测试温度为:10~25℃。取不同区间内做完电化学腐蚀的样品用去离子水冲洗,吹干。通过扫描电子显微镜+能谱仪对非金属夹杂物的形貌进行原位观察和成分分析。
2021-06-11 146 6.8

试验了通过NaCl-KCl-NaF-SiO2熔盐在电流密度50 mA/cm2、电沉积脉冲电流正反向比9:1和750850℃60min电沉积下阴极(/mm)20×20×0.5的1.6Si无取向冷轧硅钢片断面层硅的分布,并通过计算得出Si的扩散系数。结果表明,电沉积温度由750℃提高至850℃时,试样中Si含量增加,扩散的深度由18μm提高到40μm;电沉积温度与Si在钢中的扩散系数近似符合Arrhenius指数关系。 The distribution of silicon at cross section of cathode(/mm) 20 × 20 × 0.5 sheet of 1.6Si non-oriented cold rolled silicon steel after electro-deposit treatment by NaCl-KCl-NaF-SiO2 molten salt with current intensity 50 mA/cm2,electro-deposit pulse current positive-negative ratio 9:1 at 750 850 ℃ for 60 min has been tested and the diffusion coefficient of Si is obtained by calculation.Results show that with increasing electro-deposit temperature from 750 ℃ to 85... 
2014-06-28 155 5.8

一种无取向电磁钢板用热轧钢板,其以质量%计,含有C:0.0010~0.0050%、Si:1.90%~3.50%、Al:0.10%~3.00%、Mn:0.05~2.00%、P:0.100%以下、S:0.005%以下、N:0.0040%以下、B:0.0060%以下、Sn:0~0.50%、Sb:0~0.50%、Cu:0~0.50%、REM:0~0.0400%、Ca:0~0.0400%及Mg:0~0.0400%,剩余部分为Fe及杂质;该无取向电磁钢板用热轧钢板的特征在于,在无取向电磁钢板用热轧钢板的板宽方向端部中,板厚中心部(t/2位置)的加工组织的硬度HD为Hv220以下。
2021-02-19 116 6.8

利用OM,TEM,EDS与XRD技术,对Fe-3.15%Si低温取向硅钢热轧板不同常化处理后的显微组织、析出相及最终产品的磁性能进行了分析研究,并对热轧板和常化板经过冷轧后的冷轧板织构进行了对比分析.结果表明,采用1120℃保温3 min二段式冷却的常化处理工艺,常化板表层显微组织均匀,沿板厚方向的显微组织的不均匀性显著,对后续过程中形成高取向的Goss织构最有利,取向硅钢的磁性能最高;采用二段式冷却的常化冷却工艺最优,在此冷却工艺下析出的细小的析出物数量最多,且弥散分布在基体中,抑制剂的抑制效果最好,对成品获得高磁性最有利;热轧板、常化板经过冷轧后的冷轧板织构均主要由{111}〈110〉和{111}〈112〉织构组成,但常化板较热轧板冷轧后的冷轧板γ取向线织构密度明显增高,由此可以证实常化处理有助于取向硅钢最终获得高取向的Goss织构. The decreasing of slab heating temperature for grain-oriented silicon steel will reduce the amount of precipitates in hot rolled plate,and be disadvantage to the formation of ultimate Goss texture.The aim of normalizing is to control and adjust the amount,size and distribution of precipitates.Microstructures,precipitates and magnetic characteristics of finished products with different normalizing technologies for Fe-3.15%Si low temperature hot rolled grain-oriented silicon steel are researched,a... 
2013-05-28 126 5.8

1.本外观设计产品的名称:硅钢片。;2.本外观设计产品的用途:多片硅钢片用来共同组成马达的转子的其中一个部件。;3.本外观设计产品的设计要点:在于本外观设计产品的形状。;4.最能表明设计要点的图片或照片:立体图。;
2020-12-16 129 6.8

为了更好的解决电力系统防污闪涂料RTV-Ⅰ长期应用暴露出来的问题以及目前RTV-Ⅱ防污闪涂料存在的一些不足,结合具体实际需求,在电力系统外绝缘领域,应用新型防污闪硬质涂层——防污闪纳米硅钢涂层,并对分别喷涂了防污闪纳米硅钢涂层以及RTV涂料的绝缘子进行对比运行情况研究分析。研究结果表明,防污闪纳米硅钢涂层是一种同时具有优异憎水性迁移性能和自洁性能的新型涂层,具有良好的应用前景。 In order to solve the problem exposed of anti-pollution flashover coating RTV-Ⅰwhich has been used long-term in power system,as well as to better solve some shortcomings of the current anti-pollution flashover coating RTV-Ⅱ,in this paper,a new anti-pollution flashover hard coating — anti-pollution flashover nanometer silicon hard coating(NSHC) is applied in the field of power system insulation for the specific practical needs.At the same time insulators which are separately sprayed by the NSHC a... 
2013-05-28 98 5.8

对高磁感取向硅钢冷轧板分别进行800、950、1050和1120℃不脱碳的预退火处理,在800℃预退火,成品的磁性能较好。织构分析的结果表明,随着预退火温度升高,初次再结晶后有利织构组分{111}<112>与不利织构组分(118)[110]的比值f(111)/f(118)逐渐降低,初次再结晶织构的变化是成品磁性的影响因素之一。 Preliminary annealing process at different temperatures for cold-rolled strips of a high permeability grain-oriented silicon steel was investigated to study the effect of the annealing temperature on microstructure and magnetic performance of the steel.Results show that the magnetic performances of the products annealed at 800 ℃ are best.Analysis of primary recrystallization texture indicates that with rising temperature,f(111)/f(118) which is the ratio of the favorable component {111}<112>... 
2013-03-28 129 5.8

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