硅钢资料

本发明涉及一种防止低温加热取向硅钢热轧边裂的方法，包括：1)控制取向硅钢铸坯进入加热炉前的表面温度；2)控制加热段各段炉气温度；3)二加热段采用加速加热；4)控制总加热时间；5)控制出炉温度；6)控制精轧道次及侧压量；7)控制精轧道次及终轧温度；8)精轧前对钢带边部进行加热补偿。本发明通过合理制定取向硅钢的加热温度、加热时间和轧制工艺制度，避免或消除了低温加热取向硅钢热轧边裂问题。

本文以热轧常化板为初始材料,采用二次冷轧法与三次冷轧法制备了0.1 mm厚的取向硅钢薄带,测定相应的磁性能,并通过EBSD取向成像技术检测了二次冷轧法与三次冷轧法各工艺过程中织构与组织演变规律。结果表明,采用最终冷轧压下率适中的三次冷轧法,能在冷轧至0.1 mm时保存较多的高斯晶核,使得高温退火后的磁性能明显优于二次冷轧法。最终冷轧压下率通过影响脱碳退火后样品中的{111}<112>织构组分及Goss晶粒数量对最终二次再结晶产生重要影响。 Grain-oriented silicon steel sheets with a thickness of 0. 1 mm were produced from hot-rolled and normalized sheets by two-step-rolling and three-step-rolling methods. Their magnetic properties were measured,and the textures were detected by EBSD technique. The results show that the three-step-rolling method,which has a moderate reduction rate of final cold rolling,can maintain more { 110} < 001 >nucleus,and thus obtaining better magnetic properties compared with the two-step-method. The f... 

取向硅钢热轧板中织构梯度对发展完善的二次再结晶十分关键,通过添加铜可以显著降低取向硅钢板坯加热温度,从而影响热轧板织构分布。利用X射线衍射仪,分析了实验室模拟薄板坯连铸连轧(TSCR)工艺的3种不同铜含量的取向硅钢热轧板织构。结果表明:不同铜含量热轧板表面到厚度1/4处均为弱的热轧织构,热轧板心部主要为{100}面织构;铜含量约在0.4%时,热轧板次表层的{110}<001>织构比例最高,而热轧板心部的{100}<110>织构比例最低;铜含量对热轧织构中{114}<110>和{001}<100>织构发展有显著影响。 The texture gradient in hot rolled grain oriented silicon steel strip is one of the essential factors to achieve a perfect secondary recrystallization.The addition of copper can significantly reduce the slab reheating temperature of grain oriented silicon steel,so as to impact the texture distribution in the hot rolled strip.The texture of hot rolled grain oriented silicon steel strip as-rolled by thin slab casting and rolling process(TSCR) in laboratory with three different copper contents was ... 

根据相关的取向电工钢典型专利技术,概述了日本高磁感低铁损取向电工钢低温板坯加热、抑制剂合理调节、关键成分Mn、C、Sn和Sb调节与利用、新型退火剂和绝缘溶液的制备及细化磁畴等生产工艺最新动态和进展情况,并提出了国内企业申请取向电工钢专利时应当借鉴之处。 According to related typical patent technology for grain-oriented electrical steel sheets,the recent trends and progress situation for production process of grain-oriented electrical steel sheets with high magnetic flux density and low core loss in Japan are summarized including low temperature slab heating,suitably regulating inhibitors,adjusting and utilizing key element Mn,C,Sn and Sb,manufacturing for new annealing agent and insulating solutions,and fining magnetic domain,and some suggestion... 

本发明公开了一种新能源汽车驱动电机用低铁损高强度无取向电工钢及其制造方法，所述无取向电工钢的化学成分及重量百分比包括C：0.001‑0.005％、Si：2.4‑3.0％、Mn：0.25‑0.5％、Al：0.70‑1.10％、P：≤0.02％、S：≤0.005％、0.015％≤Ce+Sn≤0.035％，余量为铁和不可避免的杂质，本发明通过加入Ce和Sn，净化钢质、微合金化提高无取向电工钢强度和磁性能，不需要添加固溶金属元素，且避免了高Si体系下的轧制困难问题，且不需要高温退火，解决了退火温度过高使晶粒异常长大，晶粒尺寸均匀性降低的问题，生产出的无取向电工钢具有较高强度的同时，还具有优良的磁性能。

本发明涉及一种转炉冶炼回炉高硅钢水的方法，转炉中兑入回炉高硅钢水，再兑入铁水至预定装入量，使转炉中的钢水硅含量≤1.0％；转炉采用双渣冶炼的方法，加入的造渣料包括活性石灰、白云石、轻烧白云石、烧结矿；吹炼时氧累达到83％‑85％时使用副枪测量TSC，按TSC测量数据吹炼至钢水目标成分和目标温度后提枪，出钢。本发明实现转炉冶炼回炉高硅钢水的稳定控制。降低钢厂经济损失，减少炼钢生产事故率。提高了炼钢生产作业率。

对应用动态加热进行短时温度退火的取向电工钢进行了二次再结晶研究。所进行研究的实验用取向电工钢是经过终冷轧和后续罩式退火后的一条工业化生产线生产的。研究结果表明,运用短时热处理条件可引起研究钢完全的异常晶粒长大。在实验室处理的材料的织构和金相组织与工业化生产的经过终退火而获得的相同的取向电工钢类似。但是,在实验室处理的取向电工钢的二次再结晶的矩阵中可观测到\"寄生\"晶粒。从磁性观点看,这些\"寄生\"晶粒含有不理想的{111}取向织构。 The present study was made to investigate secondary recrystallization in grain-oriented steels annealed at short time temperature exposures with application of dynamical heating.The investigated GO(Grain Oriented) steels for experiments were taken from one industrial line after final cold rolling reduction and subsequent box annealing.It was shown that application of short time heat treatment conditions could lead to complete abnormal grain growth in the investigated GO steel.The texture and mic... 

本发明提供了一种CSP流程生产高效冷轧无取向电工钢及生产方法，成分：C≤0.0030％、Si 1.00‑1.70％、Als≤0.0050％、Mn 0.10‑0.30％、Sn0.01‑0.3％、P≤0.050％、S≤0.0080％、N≤0.0030％、Nb≤0.0030％、V≤0.0030％、Ti≤0.0030％，其余为Fe以及不可避免的杂质。与现有技术相比，本发明CSP流程生产高效冷轧无取向电工钢的方法，通过控制钢中的化学成分，并采用合适的生产工艺，实现了表面质量优良，低铁损、高磁感、低制造成本且生产高效。

针对马钢无取向电工钢孔洞缺陷的分布规律及形貌特征,对缺陷样进行了显微分析,并利用生产实绩数据分析了该缺陷产生的原因。结合热轧生产过程,主要通过避免带钢撞击导卫以及降低导卫结瘤的产生等措施,可有效抑制热卷异物压入产生,从而降低冷轧工序孔洞的产生。 In viewing of the distribution and morphology characteristics of the hole defect of non-oriented electrical steel in Maanshan Iron and Steel Co.,Ltd.,the causes of the defect were analyzed by micro analysis of the defect sample and the production data.Combined with the production process of hot rolling,by avoiding the impact of strip steel on the guide and reducing the nodule formation on the guide,the pressing of foreign bodies in hot coiling could be effectively suppressed,thus reducing the fo... 

通过对辉光放电发射光谱法分析电工钢样品光谱行为的研究,分析其工作参数如:电压、电流、预溅射时间和积分时间对光谱强度和稳定性的影响,并以铁为内标元素,优化了工作参数。确定了直流辉光放电光谱法测定电工钢中碳、硅、锰、磷、硫、铬、镍、铜共8种元素的定量分析方法,并对该方法分析的精密度和准确度进行验证,结果表明,各元素的测定结果与认定值和其他方法测定值一致,测量元素结果RSD值小于2%。 Based on research on analyzing the spectrum behavior of the sample taken from the electrical steel by glow discharge optical emission spectrometry,the effect of its operational parameters such as current,voltage,pre-sputtering time and integrating time on the spectral intensity and spectral stability is analyzed.Taking the Fe as an element applied by internal standard method,these operational parameters are optimized,and therefore the quantitative analysis method for testing eight kinds of eleme... 

本发明涉及一种含磷高磁感无取向硅钢的生产方法，工艺路线：铁水脱硫－转炉冶炼－RH精炼－连铸－热轧－酸洗－冷轧－连续炉退火－涂层－性能检验－包装，具体步骤包括：1)将钢水冶炼至目标成分后采用连铸方式将钢水铸成坯；2)热轧板坯加热炉均热段板坯温度950～1050℃，终轧温度控制在780～830℃，卷取温度600～680℃；3)酸洗后冷轧，控制冷轧整体压下率80％以上，至成品厚度，增加剪切带组织；4)连续退火炉快速加热段温度设定1000～1150℃，增加有利织构组织形核；均热段温度设定750～830℃，全氮气干气氛保护，退火工艺速度110～150m/min，满足晶粒度8～4级。本发明在减少硅、铝、锰合金添加量的情况下，改善铁损提高磁感性能，提高机械性能。

【作者】 卢鹏； ...