钢厂
辉光放电发射光谱法测定硅钢薄板中微量硼元素
通过对辉光放电发射光谱参数的优化,以铁元素为内标来消除基体效应,建立了测定硅钢薄板中微量硼元素的方法。优化的实验参数为:放电电压1200 V,放电电流50 mA,预溅射时间40 s,积分时间10 s。校准曲线硼元素含量范围0.0001%~0.022%,相关系数大于0.999,测量结果与认定值一致,相对标准偏差小于10%。完全能够满足日常分析测试的要求。 A glow discharge optical emission spectrometry(GD-OES) method for determining trace boron element in silicon steel sheets were established through optimization of instrumental parameters and using Fe element as an internal standard to eliminate the matrix effect.The optimized instrumental parameters included discharge voltage,discharge current,pre-sputtering time and integration time,which are 1200 V,50 mA,40 s,and 10 s,respectively.The content of boron element that can be determined from the ca...
成品第二次退火工艺对高牌号无取向电工钢35W300组织和性能的影响
对高牌号无取向电工钢35W300的成品进行了第二次退火,对第二次退火后的成品性能、纵横向磁性能差异和组织变化进行了分析。结果表明,随着第二次退火温度的升高,晶粒长大,磁性能优化。铁损平均值下降0.087 5W/kg,磁感平均值升高0.008T。第二次退火温度为820℃的产品的磁性能能够满足用户使用要求。 The product of high grade non-oriented electrical steel 35W300 was annealed at the second time.Microstructure,the difference of magnetic properties in the vertical and horizontal and were studied.The results show that the grain grew up and magnetic properties optimized with the increase of annealing temperature for the second time.Iron loss average declines in 0.0875 W/kg,magnetic induction average increases 0.008 T.The magnetic properties can meet the requirements of users at the second anneali...
电工钢边缘降控制研究
以马鞍山钢铁集团公司电工钢板形优化控制研究项目为背景,系统地研究了热轧、冷连轧和单机架轧机在电工钢生产过程中的边缘降控制问题。通过现场数据采集、工况数值模拟计算和工业化大生产试验,设计出适用、合理的电工钢板形控制的辊型优化曲线,满足了不同工序、不同机型的板形控制策略要求,解决了电工钢板形质量问题,取得了显著的经济效益。 Based on the project of electric steel strip shape optimization control,problem of edge drop control was systematically studied in production of electric steel of hot-rolling mill,cold-rolling mill and single stand mill.Roll optimization contour was designed out in point and reasonable by collection of work condition data,numerical simulation and test of industrial production.The shape control system can meet with the different working steps and difference mills,and quality problem of electric s...
CN202110953170.1一种冷连轧法生产无取向高硅钢的方法
本发明涉及一种冷连轧法生产无取向高硅钢的方法,RH真空脱碳处理后,铝脱氧及部分铝合金化,合金化后大罐钢水净循环大于3次或大于5分钟;熔炼合格钢水至连铸开浇前静置时间大于二十分钟;控制过热度5~15℃;采用电磁搅拌,控制等轴晶比例45%以上;3)热轧工序板坯装炉温度大于750℃;常化使晶粒尺寸在90~110μm范围内;连续退火炉加热段温度设定950~1150℃,均热段温度设定900~1050℃,全氮气干气氛保护,控制晶粒尺寸120~170μm。生产全过程中的热履历参数控制,充分发挥设计的微合金元素功能,改变析出物的组成、大小、形态及分布。
CN202111069865.X一种改善高牌号无取向硅钢冷轧断带的控制方法
本发明涉及无取向硅钢技术领域,尤其涉及一种改善高牌号无取向硅钢冷轧断带的控制方法。按重量百分比计:[Si+Al]≥4.0%;Mn、S含量满足:S≤0.0015,[Mn]/[S]:200~400;1)热轧过程中使用保温罩,热轧轧制时投入边部加热,头尾100米内卷曲温度提高15~30℃;2)常化机组圆盘剪进行边部剪边前增加加热装置,剪切后增加毛刺打磨装置,采用煤气明火加热,保证钢板温度在韧脆转变温度以上;3)圆盘剪间隙满足关系式:ds=(0.15~0.45)d0ds:圆盘剪间隙,μm;d0:常化板板厚,mm;4)常化采用快速加热,控制钢带的预热段升温速度320~380℃/min,机组速度20~30m/min;5)常化工艺后,控制边部小于20μm的晶粒占比在5%以内。有效的减少了冷轧断带的发生,提高成材率1.30%以上,降低了生产成本。
CN202111440570.9一种超高效变频空调压缩机用无取向硅钢薄带及其制造方法
本发明公开了一种超高效变频空调压缩机用无取向硅钢薄带及其制造方法,属于无取向硅钢技术领域。本发明包括以下重量百分比的组分:C≤0.003%,Si:2.0%~2.5%,Mn:0.15%~0.5%,Als:0.3%~0.7%,Sn:0.05%~0.11%,S≤0.003%,P≤0.03%,B:0.002%~0.004%,Ca:0.003%~0.005%,N≤0.003%,Ti≤0.003%,其余为Fe及不可避免的杂质,且Mn/S比控制在20~60范围内,B/N比控制在0.7~1.5,Ca/S的比例≥1。为解决现有技术中存在的问题,本发明通过添加合金元素以及偏析元素,配合连铸、热轧、常化和连续退火等热处理工艺,以及优良的冷轧板形控制技术,实现0.30~0.35mm厚度薄规格的高效无取向硅钢产品,具备优异的磁性能和高屈强比的力学性能,满足高效变频空调压缩机电机磁性能和关节式定子高速冲裁对力学性能和板形的高标准要求。
CSP流程热轧板常化温度对冷轧无取向电工钢退火组织和磁性能的影响
研究了CSP工艺生产≤0.005%C-1.1%Si的2.2mm无取向电工钢热轧板在800~1000℃常化对0.5mm冷轧板840℃退火后组织和磁性能的影响。结果表明,热轧板常化温度升高,冷轧板退火后的再结晶晶粒增大,铁损降低,磁感增加;热轧板常化温度超过900℃,因第二相固溶而后弥散析出,退火后冷轧晶粒细化,铁损增加,因此该无取向电工钢热轧板最佳常化温度为900℃。 The effect of normalizing at 800-1000℃ of CSP produced plate(≤0.005%C-1.1%Si) on the microstructure and magnetic properties of downstream cold-rolled non-oriented electrical steel annealed at 840℃ was studied.Results show that with increasing normalizing temperature of hot-rolled material the recrystallized grain size of annealed sheet increases,iron loss reduced and magnetic induction increases.As normalizing temperature excesses 900℃,grain is refined and iron loss increases after annealing due...
在动态热处理条件下对取向电工钢二次再结晶的研究
对应用动态加热进行短时温度退火的取向电工钢进行了二次再结晶研究。所进行研究的实验用取向电工钢是经过终冷轧和后续罩式退火后的一条工业化生产线生产的。研究结果表明,运用短时热处理条件可引起研究钢完全的异常晶粒长大。在实验室处理的材料的织构和金相组织与工业化生产的经过终退火而获得的相同的取向电工钢类似。但是,在实验室处理的取向电工钢的二次再结晶的矩阵中可观测到\"寄生\"晶粒。从磁性观点看,这些\"寄生\"晶粒含有不理想的{111}取向织构。 The present study was made to investigate secondary recrystallization in grain-oriented steels annealed at short time temperature exposures with application of dynamical heating.The investigated GO(Grain Oriented) steels for experiments were taken from one industrial line after final cold rolling reduction and subsequent box annealing.It was shown that application of short time heat treatment conditions could lead to complete abnormal grain growth in the investigated GO steel.The texture and mic...
热轧工艺对TSCR流程生产取向硅钢组织和性能的影响
取向硅钢热轧板中组织、织构梯度对发展完善的二次再结晶十分关键,通过对2种不同热轧工艺生产取向硅钢的组织、织构进行研究,结果表明:采用后道次大压下热轧工艺时热轧板表层再结区晶粒平均尺寸增加,再结晶区厚度增加,高温退火后二次晶粒尺寸减小;采用后道次大压下热轧工艺热轧时,热轧板中平均等效应变高,热轧板厚度心部{100}〈011〉和{100}〈001〉位向取向强度降低,({111}~{113})〈110〉位向取向强度提高,高温退火后{110}〈001〉位向偏离角降低,磁性能提高。 The texture and microstructure gradient in hot rolled grain oriented silicon steel strip was one of the essential factors to achieve a perfect secondary recrystallization.The texture and microstructure of grain oriented silicon steel strip as-rolled with two different hot rolling parameters was investigated.The results show that with big reduction at the end rolling process,the intensity of {100}〈011〉 and {100}〈001〉 orientation reduces with({111}-{113})〈110〉 orientation intensity enhanced in hot...
冷轧无取向硅钢冶炼过程炉渣分析
对冷轧无取向硅钢在冶炼过程中各个工序的顶渣进行了检测,分析了顶渣变化原因,并得出结论:硅钢生产宜采用复吹转炉,以降低吹炼终点渣中TFe含量,进而减轻对精炼的压力;使用低S、低Al2O3含量中间包覆盖剂;RH脱氧及合金化顺序采用先加硅铁后加铝;首罐宜经LF提温并降低渣中TFe。 The top-surface slag used for the various production processes in smelting coldrolled non-oriented electrical steel is tested and based on tested results the cause of the top surface slag change is analyzed.So it is concluded that the combined blown converter is more suitable to be used for smelting electrical steel in order to reduce the content of TFe in slag at blow end point and then much better results can be achieved during the period of refining.Secondly the tundish flux contenting low co...
CN202111200887.5一种改善表面麻点缺陷的薄规格中低牌号无取向硅钢及其生产方法
本发明提供一种改善表面麻点缺陷的薄规格中低牌号无取向硅钢及其生产方法,成分C≤0.0025%,1.2≤Si≤1.65%,0.25%≤Mn≤0.35%,0.06%≤P≤0.11%,0.1%≤Als≤0.2%,S≤0.0025%、N≤0.0025%,Ti≤0.0025%,其余为Fe及不可避免的杂质。与现有技术相比,本发明采用较低氢气浓度,防止炉内氧化铁皮还原,减轻碳套辊的腐蚀程度,减少碳套辊结瘤率,改善带钢表面质量;采用合理合金成分设计,提高带钢的力学强度,降低碳套辊结瘤对带钢表面的影响程度,改善带钢表面质量。产品厚度为0.35mm,板面麻点发生率降低,无手感,且辊身周长周期范围内麻点个数≤5个。

