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研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c... 
2013-01-28 141 5.8

根据本发明的一个实施例的双取向电工钢板,具有从{100}<001>起15°以内的取向的晶粒的分数为50至75%,并且具有从{100}<380>起15°以内的取向的晶粒的分数为50至75%。
2020-12-17 141 6.8

分析了影响脱碳效果和结晶行为的各种要素及其相互制约关系,提出了Hi-B连续退火工艺曲线,总结得出快速加热及合理稳态气氛是实现工艺制度的关键。结合实际工程,介绍了在连续退火炉设计中快速加热和气氛设计的考虑方法,并指出随着Hi-B产品的发展,如何改进这些方法将是连退工程研发的方向之一。 The factors which affect decarbonization and crystallization and the mutual restriction between them were analyzed.A complete continuous annealing process for Hi-B was put forward.As a result,the rapid heating and the proper steady atmosphere were two important factors.According to an actual project,the consider methods for designing rapid heating and proper steady atmosphere were introduced,and it is pointed that with the development of Hi-B technique,how to improve these techniques would be on... 
2011-02-28 141 5.8

本实用新型公开了一种高精度硅钢片加工用多向定位组件,包括底板、安装板、橡胶轮组一和橡胶轮组二,所述底板上端两侧对称设置有U型的所述安装板,所述安装板内底端中部安装有安装架二,所述安装架二上安装有所述橡胶轮组二。有益效果在于:本实用新型通过螺杆、调节套、安装架一、安装架二、橡胶轮组一、橡胶轮组二、弹簧以及连接柱的设计,能够实现高精度硅钢片在加工时的有效夹紧定位,避免了高精度硅钢片在加工时的晃动滑移,提高了高精度硅钢片的加工质量,通过电推杆、滑块以及滑槽的设计,能够根据高精度硅钢片的尺寸来调节安装板之间的间距,以满足也不同尺寸高精度硅钢片的加工需求,提高了定位组件使用的灵活性。
2021-07-02 141 6.8

从影响高牌号无取向硅钢退火工艺的主要参数入手,介绍高牌号无取向硅钢退火炉在加热、气氛控制、冷却、涂层烘烤方面的新技术,并展望无取向硅钢退火炉的发展方向。 Based on the technology parameters of high-grade non-oriented silicon steel annealing,the new technology of the annealing line,which includes heating,atmosphere control,cooling,coating baking,is introduced,and the development direction of non-oriented silicon steel annealing furnace is pointed out. 
2013-02-28 141 5.8

利用X-射线衍射织构分析和线形分析技术测定了交叉轧制双取向硅钢在制备工艺各阶段的织构及微结构,进而探讨了立方织构({100}<001>)的形成过程。通过对实验结果的分析可知,二次冷轧和交叉轧制工艺为立方织构提供了内能优势和有利的形变织构,而低温预退火工艺既强化了立方织构的内能优势,又为立方织构的异常长大提供了有利的组织保证,最终在抑制剂(AlN和MnS)的协同作用下,硅钢在二次再结晶退火后形成了强烈的立方织构。 The texture and substructure of the double oriented electrical steels produced by the cross rolling technology during the difference process has been measured by means of the X-ray texture and diffraction peak profile analysis technology,and research the formation mechanism of cube texture,{100}<001>.The results show that the dominances of inner energy and deformation texture were supplied by secondary cold rolling and the cross rolling technology and strengthened by pre-annealing at a low... 
2011-02-28 140 5.8

本发明公开了一种超高效变频空调压缩机用无取向硅钢薄带及其制造方法,属于无取向硅钢技术领域。本发明包括以下重量百分比的组分:C≤0.003%,Si:2.0%~2.5%,Mn:0.15%~0.5%,Als:0.3%~0.7%,Sn:0.05%~0.11%,S≤0.003%,P≤0.03%,B:0.002%~0.004%,Ca:0.003%~0.005%,N≤0.003%,Ti≤0.003%,其余为Fe及不可避免的杂质,且Mn/S比控制在20~60范围内,B/N比控制在0.7~1.5,Ca/S的比例≥1。为解决现有技术中存在的问题,本发明通过添加合金元素以及偏析元素,配合连铸、热轧、常化和连续退火等热处理工艺,以及优良的冷轧板形控制技术,实现0.30~0.35mm厚度薄规格的高效无取向硅钢产品,具备优异的磁性能和高屈强比的力学性能,满足高效变频空调压缩机电机磁性能和关节式定子高速冲裁对力学性能和板形的高标准要求。
2021-11-30 140 6.8

绝缘涂层可以有效提高硅钢片的耐蚀、耐腐、磁、绝缘等性能,因此取向硅钢涂装绝缘涂层是取向硅钢生产过程中重要的一环。本文对取向硅钢含铬无机绝缘涂层以及氮化铬涂层的性能优缺点进行了介绍,并对国内无机含铬取向硅钢绝缘涂层及氮化铬涂层的研究现状进行了综述。最后对未来含铬无机绝缘涂层的研发方向进行了展望。 Insulation coating can effectively improve the corrosion resistance of silicon steel sheet, such as corrosion, magnetic, insulation performance, thus oriented silicon steel insulation coating is the important part of oriented silicon steel production process. In this paper, the inorganic insulation coating oriented silicon steel containing chromium and chromium nitride coating performance advantages and disadvantages are introduced.In addition, the research status of insulation coating and chrom... 
2022-02-28 140 5.8

本发明的一种超低碳含钇取向硅钢及其制备方法,化学组成及质量百分比为Si:2.0~4.5%,C:≤0.003%,Y:0.001~0.1%,Mn:0.1~0.25%,Al:0.01~0.02%,Cu:0~0.3%,S:0.02~0.035%,N:0.009~0.011%,其余为Fe和不可避免的杂质元素。生产工艺为:连铸、铸坯加热、热轧、常化、冷轧、初次再结晶退火、二次再结晶退火。本发明采用超低碳的成分,取消了常规取向硅钢脱碳退火工艺,简化了生产流程。通过稀土微合金化解决了因超低碳成分导致的单向铁素体组织抑制剂析出困难的技术难题。本发明制备的含钇取向硅钢厚度为0.2~0.35mm,磁感应强度B8为1.85~1.94T,铁损P17/50为0.9~1.2W/kg,可以用于变压器的铁芯材料,制备流程更为简洁。
2021-12-02 140 6.8

对无取向硅钢炼钢全流程钢液增钛的原因进行了分析,认为铁水钛含量、转炉出钢温度、转炉下渣量、精炼渣TiO2含量、钢水罐及RH浸入管混钢种生产是影响钢液增钛的主要原因。通过采取低钛铁水冶炼,减少转炉下渣量,提高出钢温度,添加白灰改质精炼渣等措施,均能够降低钢液中的钛含量。 After analyzing the causes leading to increased content of titanium in molten nonoriented silicon steel during whole steelmaking process, it was concluded that such factors as content of titanium in hot metal, tapping temperature from converter, quantity of roughing slag entered into the ladle from converter, content of TiO2 in refining slag, molten steel ladle car,carrying out the steelmaking of different steel grades by the same ladle and same RH immersion tube were the main causes ... 
2022-01-28 140 5.8

本实用新型公开了一种硅钢片分流导料机构,属于硅钢片导料领域,包括传送带,所述传送带包括主带和副带,所述副带设置在主带的前面,所述主带横向设置,所述主带的后面设置有导流机构,所述导流机构包括电机、导流板和助力组件,所述主带的后面设置有安装架,所述安装架的顶部竖向固定连接有连接板,所述电机安装在连接板上,所述电机的输出轴与导流板的顶部固定套接,通过启动电机,电机带动导流板旋转,导流板在连接组件下带动助力组件旋转,使得主带上的物品被导流板进行阻挡,通过助力组件传送到副带上,避免了传送带方向单一,容易导致硅钢片对堆积的问题,从而减少硅钢片的损坏量,进而节约成本。
2021-12-15 140 6.8

采用低温板坯加热制备取向硅钢,通过透射电镜(TEM)观察并研究热轧板中的析出物,用ODF织构法研究热轧板距表面1/8、1/4和1/2处的织构分布。结果表明,热轧板中的析出物主要是密排六方AlN,AlN形貌呈规则长方形,AlN颗粒大小不等,分布密度低;热轧板中的织构沿板厚方向,由亚表层的{110}<001>织构向1/2中心层的α线织构变化,其中{110}<001>织构在热轧板距表面1/4层处最强。 The low temperature grain-oriented silicon steels were produced by acquired inhibitor method.The precipitates in hot rolling strip were observed and studied by transmission electron microscope,and the texture distribution in 1/8,1/4 and 1/2 layers of hot rolling strip were analyzed by ODF method.The results showed that the square shaped h-AlN is the main precipitates in hot rolling strip.The precipitates are varying in size and distribution.The texture of hot rolling strip in thick direction are... 
2011-04-28 139 5.8

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