硅钢资料

本发明公开了一种提高超高磁感取向硅钢底层质量的退火隔离剂及其制备方法和应用。本发明所述退火隔离剂包括如下组分：MgO、TiO2、硼酸、Na2O、Sb2(SO4)3；以MgO质量为标准，其余各组分相对MgO的质量百分数为：TiO21.9～40％，硼酸0.05～0.1％，Na2O1～5％，Sb2(SO4)31～5％。本发明制备的退火隔离剂提高了超高磁感取向硅钢的成材率；提高了取向硅钢的底层附着性，降低了产品让步率；制备的超高磁感的取向硅钢可满足高容量变压器的使用要求。

【作者】 杨佳直； ...

介绍了烟气余热利用系统的工艺流程及控制思想,结合该系统在钢厂硅钢连续退火机组中的应用实践,估算出烟气余热利用系统每年可节约蒸汽5 040 t,经济效益良好,同时分析了该系统存在的问题及对策。 Introduced a method about the process and control of the application of waste heat system, which had been used into a silicon steel continuous annealing line and profiting a good economic benefit by saving a large number of steam every year, which has been estimated about 5 040 tons, and analyzed the problems and solutions existed in this system. 

对低温法生产的以AlN为主抑制剂的Hi-B取向硅钢高温退火过程进行了中断实验,借助EBSD及TEM技术对高温退火连续升温过程中织构与析出物的演变进行了研究。实验结果表明,800℃时ODF图出现高斯织构组分,但强度很弱,高斯晶粒偏离角在10°以上;950~1 000℃时高斯晶粒异常长大,偏离角3~6°;高温退火过程析出物主要有球形、规则立方形及不规则多面体形3种形貌,由于渗N的影响,Zener因子先增大再减小,并且析出物在高斯晶界前沿优先粗化。 The annealing process at high temperature of Hi-B silicon steel using low slab reheat temperature and with AlN as the inhibitor has been studied by interrupting test,and the evolution of texture and precipitates during continuous heating-up in the annealing process at high temperature was analyzed by EBSD and TEM. The results showed that Goss texture appears in ODF at 800 ℃,but the intensity of Goss texture was very weak and the deviation angle was more than10°. Goss grains grow abnormally durin... 

试验研究了0.3 mm取向硅钢冷轧板(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005A1)的退火温度(760~880℃7 min)和退火时间(820℃3~9 min)对该钢的晶粒尺寸,再结晶和织构的影响。结果表明,最佳初次再结晶退火工艺为820℃5 min,该钢的平均晶粒尺寸为14.20μm,完全再结晶率为92%,不利{111}<110>结构含量为3.16%,有利织构{111}<112>,{012}<001>和高斯织构含量分别0.40%,4.73%和2.46%。 The effect of annealing temperature(at 760 ~ 880 X.for 7 min) and time(at 820℃ for 3~9 min) on grain size,recrystallization rate and texture of 0.3 mm cold-rolled sheet of oriented silicon steel(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005Al) has been tested and studied.Results show that with optimum recrystallized annealing at 820℃ for 5 min,the silicon steel average grain size is 14.20 fun,the complete recrystaUization rate is 92%,the unfavourable-texture {111}< 110 > content in steel is ... 

通过热力学计算与模拟试验研究了含钒钛取向硅钢中氮化物析出相的析出规律与析出行为,并探讨了含钒钛元素的氮化物析出相作为薄板坯连铸连轧流程制备取向硅钢中辅助抑制剂的可行性.研究表明,在所冶炼的含钒钛取向硅钢的成分范围内,Ti N在钢液凝固末期便具备析出的热力学条件,而Al N与VN只可能在凝固后的α+γ或α+Fe3C两相区内析出.含钒钛取向硅钢中氮化物析出相以成分复杂的复合析出相为主,且随着钒钛加入量的增加,钢中抑制剂析出相总的分布密度由于含钒钛元素的氮化物析出相的增加而明显提高,使抑制剂抑制初次再结晶晶粒正常长大的能力得以加强,最终成品的磁感应强度值B8由1.857 T提升至1.898 T.同时,加入不高于0.007%的Ti与不高于0.005%的V不会影响中间脱碳退火工序的脱碳效果以及高温退火净化阶段硫、氮的脱除效果,其形成的含钒钛元素的纳米级氮化物析出相适合作为薄板坯连铸连轧流程制备取向硅钢的辅助抑制剂. The precipitation behavior of nitride precipitates in grain-oriented silicon steel containing vanadium and titanium elements produced by thin slab casting and rolling process was studied by thermodynamic calculation and simulation experiment. The feasibility of nitride precipitates containing V and Ti elements as auxiliary inhibitors was also investigated. It is found that Ti N is likely to precipitate at the final stage of solidification in the grain-oriented silicon steel,but VN and Al N can p... 

本实用新型涉及硅钢片生产技术领域，特别涉及一种电机硅钢片冲槽生产线，包括支架，支架下方依次设有:毛坯料垛，毛坯料垛由待冲毛坯片堆成，待冲毛坯片中心具有通孔；理片机；定子冲槽机，定子冲槽机用于在毛坯片上冲裁形成已冲毛坯片，已冲毛坯片包括定子片和转子坯片；第一液压升降机，第一液压升降机用于承载定子片；转子冲槽机，转子冲槽机用于冲裁转子坯片从而形成转子片；第二液压升降机，第二液压升降机用于承载冲裁得到的转子片；输送装置，输送装置用于输送待冲毛坯片、已冲毛坯片、转子坯片或转子片，本实用新型提出一种适用范围广、运行效率高、结构简单、价格适宜的电机硅钢片冲槽自动线。

本发明公开了叠片装置，以及采用该叠片装置的硅钢片收料设备，包括分料装置和本发明第一方面实施例的叠片装置，分料装置包括有分料件、上分料传送带和下分料传送带，上分料传送带的一端和下分料传送带的一端与分料件连接，分料件用于将硅钢片分别输送至上分料传送带和下分料传送带，本发明第一方面实施例的叠片装置，叠片装置的数量为两个，两个叠片装置上下平行设置，并且分别与上分料传送带和下分料传送带的远离分料件的一端连接。根据本发明的叠片装置，以及采用该叠片装置的硅钢片收料设备，可实现硅钢片的自动叠片，提高生产效率。

提供能够稳定地制造磁特性优异且钢卷长度方向的铁损的偏差少的取向性电磁钢板的取向性电磁钢板的制造方法。本发明是一种取向性电磁钢板的制造方法，包括如下工序：对钢坯进行热轧，根据情况实施退火，然后通过1次冷轧或夹有中间退火的2次以上的冷轧来制成具有最终板厚的冷轧板，接着对上述具有最终板厚的冷轧板进行脱碳退火，然后实施二次再结晶退火；在最终的冷轧之前，将钢板以100℃/s以上的升温速度加热到100℃～350℃的加热温度，上述钢板从达到加热温度到进入最终的冷轧的第1道次的时间为5秒以内。

根据相关的取向电工钢典型专利技术,概述了日本高磁感低铁损取向电工钢低温板坯加热、抑制剂合理调节、关键成分Mn、C、Sn和Sb调节与利用、新型退火剂和绝缘溶液的制备及细化磁畴等生产工艺最新动态和进展情况,并提出了国内企业申请取向电工钢专利时应当借鉴之处。 According to related typical patent technology for grain-oriented electrical steel sheets,the recent trends and progress situation for production process of grain-oriented electrical steel sheets with high magnetic flux density and low core loss in Japan are summarized including low temperature slab heating,suitably regulating inhibitors,adjusting and utilizing key element Mn,C,Sn and Sb,manufacturing for new annealing agent and insulating solutions,and fining magnetic domain,and some suggestion... 

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

一种低温高磁感取向硅钢的热轧方法：经转炉冶炼并浇注成坯；对铸坯加热后进行粗轧：首先确定粗轧减宽量；根据所确定的粗轧减宽量进行粗轧；进行精轧；常规进行下工序。本发明采用低温板坯加热技术，降低了板坯烧损和修炉负担，且边裂发生率比现有技术的不低于18%的基础上能降低5%以上，由此节约资源及降低能耗。