硅钢资料

系统研究了无取向硅钢用磷酸盐系涂层性能的影响因素。以氢氧化铝和磷酸为原料制备磷酸二氢铝,再添加适量的添加剂酒石酸铵、二氧化硅、环氧树脂,得到的涂液涂布于硅钢表面,并控制合适的烘干温度,通过耐盐雾实验考察各因素对涂液耐腐蚀性能的影响。实验结果表明,在磷酸与氢氧化铝物质的量比为3.4∶1、酒石酸铵用量为2%、二氧化硅用量为1%、环氧树脂用量为5%、烘干温度为300℃条件下,所得涂层材料的防(耐)腐蚀效果最佳。 The factors influencing the performance of phosphate anticorrosive coating for non-oriented silicon were systematically studied.Aluminum dihydrogen phosphate was prepared with aluminum hydroxide and phosphoric acid as raw materials.Then added the right amount of additives,such as ammonium tartrate,silicon dioxide,and epoxy resin to prepare the liquid coating,which was coated on the surface of the silicon steel,and finally controlled a suitable drying temperature.The influences of various factors... 

介绍了攀钢冶炼电工钢过程硫含量变化以及过程回硫、增硫情况,采取针对性措施,如:提高铁水装入量、转炉采用石英砂代替复合造渣剂造渣、RH脱硫等,降低钢中硫含量。结果表明:采取相应措施后,电工钢炼成率大幅提高,成品w[S]≤0.008%的比例由改进前的62%提高到92.4%,取得了明显的冶金效果。 The resulfurization and the change of sulphur content in production of electrical steel is analyzed.The targeted measures have been taken,such as increase the loaded quantity of liquid iron,quartz sand replaces the composite slagging agent in the converter and RH desulfurization to decrease the sulphur content of the steel.The result shows,after the measures have been taken,the finished product ratio of electrical steel increase a lot.The ratio of sulfur content of finished product no more than ... 

本发明涉及一种高性能取向硅钢冷轧工艺，具体涉及取向硅钢制造技术领域。本发明的冷轧工艺包括一次冷轧和二次冷轧，其中，取向硅钢热轧板厚度在2.0～3.0mm，一次冷轧轧制采用4或5道次轧制，轧至厚度0.60～0.62mm，轧制温度为100℃～105℃；二次冷轧轧制采用2道次，轧至厚度0.24～0.26mm，轧制温度为95℃～100℃。本发明通过对一次冷轧和二次冷轧中各道次的压下率、轧制张力、轧制速度、轧制温度进行优化设计，从而能够进一步优化织构，确保二次冷轧板高斯织构含量在0.8～1.5％，且轧制稳定性高，进而有效保证了所得取向硅钢的磁性能。

本发明涉及取向硅钢高温连续退火炉领域，尤其涉及一种取向硅钢高温连续退火炉隔离装置，包括安装在炉壳上的隔离炉门及设置在隔离炉门四周的密封井；隔离炉门顶部两侧安装有水冷却装置；水冷却装置上部设有隔离炉门动力牵引装置；密封井包括固定密封井和伸缩密封井，伸缩密封井位于固定密封井内部并与固定密封井滑动连接，伸缩密封井与固定密封井端部连接处设有密封装置。本发明可以确保隔离炉门升降过程中实现无缝全密封状态，提高密封效果，且采用伸缩密封井实际降低了密封井的高度，间接降低了水冷却装置连接管道上升至最高点的净空标高，与传统固定式密封井高度相比可以降低高度50％～80％，从而降低厂房净空标高，节省厂房基建投资。

本实用新型公开了一种取向硅钢喷涂用涂料的加工上料装置，包括底座，所述底座固定连接有立柱，所述立柱固定连接有搅拌桶，所述立柱上滑动连接有桶盖和电机支架，所述电机支架固定连接有电机，所述电机的输出端固定连接有搅拌杆，所述搅拌杆穿过桶盖并固定连接有搅拌叶片，所述电机支架与桶盖之间固定连接有弹簧，所述滑槽中位于电机支架和桶盖之间固定设有限位块，通过电机、搅拌杆、搅拌叶片之间的配合，使涂料在配制时能够混合均匀；通过电机支架、桶盖、弹簧和限位块之间的配合，使得在搅拌过程中，桶盖始终紧紧盖住搅拌桶，防止搅拌过程中涂料洒漏。

本发明公开了一种控制无取向硅钢厚度稳定性的轧制工艺，涉及硅钢厚度控制方法领域。本发明通过降低硅钢精轧入口温度，并调节粗轧区域、精轧区域和卷取区域的生产参数，保证后续卷取工序的轧制稳定性及卷形质量，严格控制无取向硅钢的厚度稳定性。本发明提供的轧制工艺使硅钢的厚度命中率得到了明显提升，提升了后续冷轧工艺的轧制速度，轧制力波动减小，提高了产品质量。

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

本发明提出了一种控制磁畴结构来降低铁损的取向性电磁钢板的制造方法中，即使在实施了去应力退火的情况下，也能够保持铁损降低效果，并且在磁畴控制处理后磁通密度不会降低的方法。本发明的制造方法中，在取向性电磁钢板的表面，沿与钢板的轧制方向交叉的方向线状地照射周边比中心低的环状的强度分布的激光。

介绍了CSP工艺生产无取向电工钢各工序的设备特点、采用的工艺控制手段和电工钢产品质量情况,结合生产实践证明了马钢CSP工艺开发的无取向电工钢产品丰富了薄板坯连铸连轧的品种结构,发挥了薄板坯连铸连轧生产无取向电工钢性能均一、稳定的特点。 The equipment characteristic,the process control method and the quality of non-orientated silicon steel by CSP process were introduced.Combined with the production situation,it is proved that production of non-orientated silicon steel developed on Masteel CSP line would enrich product structure of thin slab continuous casting and rolling,and it exerts stable performance of non-orientated silicon steel. 

传统轧制法制备6.5wt.%高硅钢过程中温轧工艺具有显著不同于3 wt.%Si的电工钢的特点及组织织构特征,是开发新型基于织构优化的高硅钢的关键环节。采用EBSD技术对通过热轧、温轧、冷轧及退火工艺制备0.3mm厚的6.5wt.%Si电工钢板的组织和织构进行分析,重点研究温轧过程中的中间退火和大、小压下率组合以控制织构。结果表明,在热轧退火板是部分再结晶组织的情况下,一次性温轧或先小形变量、中间退火后再大形变量的工艺可得到更多的Goss晶粒;经过最终退火后Goss取向会发生偏转,形成部分黄铜取向,而{111}〈112〉取向的晶粒内形核生成近Goss取向的再结晶晶粒;大压下量轧制是最终组织中{111}取向晶粒较多的主要原因。 Warm rolling,a key process of developing new type high-Si electrical steel based on texture optimization,has significant different characteristics from 3wt% Si steel in conventional preparing process. 0. 3mm thickness 6. 5wt. % Si steel,obtained by a series of processes including hot and warm rolling,intermediate annealing and then cold rolling,was analyzed from microstructure and texture by EBSD,which are utilized mainly for investigating the intermediate annealing process and the combination o... 

研究的两种取向硅钢（%:No1-0.042C、3.16Si、0.009Al、0.07Mn、0.50Cu、0.015S、0.0084N和No2-0.040C、3.20Si、0.014Al、0.22Mn、0.49Cu、0.016S、0.008 2N）由50 kg真空感应炉冶炼,锻成（mm）350×120×35板坯,经1 250℃30 min加热,开轧温度1 100℃,5道次热轧成2.3 mm板,终轧温度950～1 000℃。实验结果表明,两热轧板沿板厚方向存在组织和织构的不均匀性,热轧板次表层为再结晶组织,有较强的Goss织构组分;中心层为形变组织,具有典型的形变织构。含0.22%Mn的No2钢次表层{110}〈001〉织构组分比含0.07%Mn的No1钢弱,中心层{001}〈110〉织构组分大大强于0.07%Mn No1钢,导致两者磁性能差异,0.22%Mn No2钢磁感应强度(B₈₀₀)和铁损(P_1.7/50)分别为1.87 T和1.24 W/kg,0.07%Mn No1钢分别为1.88 T和1.18 W/kg。 Studied both grain-oriented silicon steels（%:No1- 0.042C,3.16Si,0.009Al,0.07Mn,0.50Cu, 0.015S,0.0084N and No2-0.040C,3.20Si,0.014Al,0.22Mn,0.49Cu,0.016S,0.0082N） are melted by a 50 kg vacuum induction furnace,forged to（mm） 350×120×35 slab,heated at 1 250℃for 30 min,with beginning rolling temperature 1 100℃hot-rolled to 2.3 mm plate by 5 passes,finishing-rolled at 950～1000℃.Test results show that the structure and texture along thickness of both hot-rolled plates are inhomogeneous:the subsurface ... 

研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c...