硅钢资料

以试验室模拟CSP工艺生产的Fe-3Si热轧钢带为研究对象,采用正交试验及方差分析的方法,研究了取向硅钢初次再结晶退火工艺对高温退火后获得锋锐的高斯织构的影响。结果表明:取向硅钢两段式初次再结晶脱碳退火工艺参数加热段保温时间及加热温度是高温退火后获得锋锐高斯织构的主要影响因素,其可信度分别在90%和85%以上;在本试验条件下,通过正交试验获得的最佳退火工艺为:冷硬板经600℃保温3 min和850℃保温6 min。 Fe-3Si hot rolled strip was produced by simulating CSP technology in the laboratory.Orthogonal experiment and analysis of variance were carried out to investigate the influence of primary recrystallization on the sharp Goss texture of the oriented silicon steel.The results show that holding time of the heating section and the heating temperature for a sharp Goss texture of the samples annealed has important implications in this experiment conditions,the two-step decarburization annealing process... 

研究了卷取工艺对一种新型含铜无取向电工钢晶粒尺寸、织构演变、铁损和磁感应强度的影响。结果表明,试样织构组分主要为{111}、{112}、{100}和高斯织构,在550℃卷取、保温2～3h,{100}织构有增强趋势,磁感应强度较高,铁损较低。 The effects of coiling process on grain size,texture,core loss and magnetic induction of a new cold rolled non-oriented electrical steel with copper were investigated.The results show that there are mainly {111},{112},{100} and {110}<001> texture.Coiling at 550℃and keeping for 2～3 hours,the {100} texture is enhanced,magnetic induction is higher and core loss is lower. 

针对薄板坯连铸连轧流程结合\"获得抑制剂法\"所制备的低温高磁感取向硅钢,通过热力学计算研究了AlN与MnS在连铸与均热过程中的析出规律与行为。计算结果表明,连铸过程中AlN在凝固后的高温α相中便可能析出,而MnS仅可能在凝固后的α+γ两相区内析出。钢中AlN与MnS在均热过程中均处于部分固溶与部分析出的状态。后续高温渗氮处理后初次晶粒的异常长大并不明显,表明渗氮处理前钢中固有抑制剂的数量相对充足。 The precipitation behavior of MnS and AlN in low-temperature high magnetic induction grain-oriented silicon steel produced by thin slab casting and rolling process with\"acquired inhibitor method\"during continuous casting and soaking was studied by thermodynamic calculation.The calculated results show that AlN is likely to precipitate in ferrite after solidification.However,MnS can precipitate only in the two phase region of ferrite and austenite.Meanwhile,MnS and AlN in the steel can not be comp... 

通过观察冲剪边缘组织,测量冲剪边缘的显微硬度、残余应力的分布情况和磁性能的变化研究了冲剪加工对无取向硅钢50WW800边缘组织和磁性能的影响。对冲剪后硅钢片进行750℃退火,分析退火对组织和磁性能的影响。结果表明,硅钢片剪切边缘会存在0.4 mm的形变硬化层,边缘应力大,铁损增加。退火后变形减小,形变硬化层变小,残余应力大幅度减少,铁损减少。 The influence of punching process on cutting edge microstructure and magnetic properties of non-oriented silicon steel 50WW800was studied by observing microstructure and measuring microhardness near cutting edge.The residual stress distribution in the silicon steel tooth and magnetic properties were measured.Effect of annealing at 750 ℃ on microstructure and magnetic properties of the silicon steel was analyzed.The results show that a cut-edge hardening layer up to 0.4 mm is observed,residual st... 

结合工业化生产的高效硅钢,进行了RH精炼稀土处理试验研究。针对不同的稀土处理条件,观察了夹杂物的形貌和尺寸分布,探讨了稀土处理后钢中的夹杂物形成、变化规律。结果表明:试验条件下,最佳的稀土合金添加数量为0.6～0.9 kg/t。经过合适的稀土处理后,可以有效抑制尺寸相对较小的、不规则的AlN、MnS复合夹杂生成,促进钢中微细夹杂物的聚合、上浮,钢质纯净度得到明显提高。此时,钢中全氧含量最低,脱硫效果最佳,钢中的夹杂物主要是尺寸相对较大的、近似球形或者椭球形的稀土类夹杂。 Based on the industrial production of non-oriented silicon steel,the experiment on RE treatment during the RH refining process was studied.The morphology and the size distribution were observed for the steel specimens treated with different RE treatment conditions.Further more,the formation and change of inclusions of final steel sheets after RE treatment were discussed.The results show that the suitable RE added amount was 0.6～0.9 kg/t.After the suitable RE treatment,the formation of AlN and Mn... 

分析了电感耦合等离子体发射光谱法(ICP-AES)测定硅钢中铌的检测过程,讨论了该检测过程中不确定度的主要来源,建立了该方法的定量的数学模型,并根据这一模型计算出了检测结果的合成标准不确定度和扩展不确定度。 The measurement of niobium content in silicon steel by inductively coupled plasma atomic emission spectrometry(ICP-AES) was analyzed,by which the main factors affecting the uncertainty of the measurement were ascertained and the calculation formula was given.Finally,according to the formula the combined uncertainty and expanded uncertainty were obtained. 

为研究常化温度对热轧无取向硅钢组织与织构的影响,采用光学显微镜、背电子散射衍射技术研究了不同常化温度对其影响。结果表明,实验硅钢板在700～850℃温度下常化时,随常化温度的升高,晶粒尺寸增大,有利组分α织构增强,不利组分γ织构降低。对比研究了800℃和850℃常化热轧板CSL晶界分布图与取向差分布图,在本文研究条件下,Goss织构易在Σ=3,9的CSL晶界及晶粒取向差为30°～55°处形成。 The hot strips normalized at different temperatures were investigated by optical microscope and EBSD to study the effect of normalizing temperature on microstructure and texture of hot-rolled non-oriented silicon steel sheets.The results show that the grain size increases,the intensity of α-fibre texture increases,and the γ-fibre texture decreases when the hot strips are normalized at the 700-850 ℃.And CSL boundaries of Σ=3 and 15,and misorientation angles between 30° and 55° are more likely rel... 

通过对湿H2气氛下,相同退火温度、不同退火时间的CGO硅钢初次再结晶样品进行金相组织观察,并进行了EBSD微观织构分析,研究了CGO硅钢初次再结晶过程中的组织及再结晶织构演变行为。结果表明,在湿H2气氛下,820℃保温,CGO硅钢初次再结晶过程约在120 s时完成。随着退火时间的延长,γ面上{111}<112>织构含量逐渐减少,{111}<110>织构先减少后增多,随着再结晶的完成,部分{111}<112>取向晶粒向高斯{110}<001>取向转化的同时,也向{111}<110>取向转化,高斯{110}<001>织构含量逐渐增多。高斯取向晶粒较多是由{111}<112>取向晶粒转化而来,同时也证明了CGO硅钢高斯取向晶粒的二次再结晶异常长大生长机制为择优形核。 Microstructure development and texture evolution of conventional grain oriented silicon steel,which were annealed at same annealing temperature and different annealing time under wet H2 atmosphere,were investigated through metallographic observation and electron backscattered diffraction analyzing.The results show that the primary recrystallization finishes in 120 s at 820 ℃ under wet H2 atmosphere.With the extending of annealing time,{111}<112> texture decreases,{111}<110> texture d... 

对取向硅钢熔融态钢液进行处理,对比研究了不同脉冲参数的作用效果。结果表明,电脉冲对钢锭晶粒组织具有明显的细化作用,凝固组织等轴晶比例大幅上升。在脉冲电容、频率、处理时间和电压中,影响等轴晶比例的最显著性因素为脉冲频率;最优正交实验参数为:电容1 200μF,脉冲频率1 Hz,处理时间5 s,脉冲电压800 V;随着输入能量的增大,等轴晶率先增大后减小,脉冲输入能量为某值时,等轴晶率最大,通过经典形核理论和热力学对这一现象进行了解释。 Research on the influence of the electric pulse on the solidification structure of oriented silicon steel was preformed.Electric pulses in different parameters were applied to molten steel and results were compared.The result shows that solidification structure of oriented silicon steel can be improved by the electric pulse,and the equiaxed crystal ratio increases obviously.Among the four parameter factors of electric capacity,frequency,applied time and voltage,the most effective factor is frequ... 

通过在实验室条件下模拟薄板坯连铸连轧流程,并在以Cu2S为主抑制剂制造普通取向硅钢(CGO)的基础上,加入适量钒钛,研究了钒钛对取向硅钢组织与磁性能的影响。结果表明,适量钒钛使热轧板和脱碳退火板组织更好,尤其使脱碳退火板的晶粒更加细小和均匀;加入适量钒钛不但使热轧板表面高斯织构强度更高,更使脱碳退火板中有利于高斯织构发展的γ织构强度更高;适量钒钛能形成Cu2S+(V,Ti)N等复合析出物,起到辅助抑制剂作用,加强抑制能力。细小均匀的晶粒、强度更高的有利织构和更强的抑制能力使CGO钢磁性能更佳。 Effect of V and Ti on microstructure and magnetic properties of conventional grain-oriented silicon steel(CGO) were investigated under simulated thin slab continuous casting and rolling process in laboratory with Cu2 S as the dominant inhibitor. The results show that appropriate amount V and Ti make the microstructures of the hot rolled sheet and the decarburizing annealed sheet better,especially make the grains of the decarburizing annealed sheet more tiny and uniform. Adding appropriate V and ... 

通过制备磷酸二氢铝硅钢涂层,研究了氧化锌对无铬涂层耐盐雾性能、电化学性能和附着性的影响。结果表明,硅钢表面涂层含有4.0%的氧化锌时,涂层具有最高的耐腐蚀性能和电化学性能,而且其致密表面最为平整,没有裂纹出现。 The effects of ZnO on the salt spray resistance property, electrochemical performance and adhesiveness of silicon steel insulating coating were studied. The results show that the best corrosion resistance and electrochemical properties can be obtained when the coating contains 4.0% oxide zinc, and the dense surface is smooth without cracks. 

介绍了普通取向硅钢(CGO)和高磁感取向硅钢(Hi-B)铸坯高温加热两次冷轧、一次冷轧和铸坯低温加热两次冷轧、一次冷轧法4种成熟生产工艺的主要技术参数,取向硅钢理论研究(Goss晶核和抑制剂)和生产技术现状。取向钢的发展趋势为:提高(110)[001]晶粒取向度,降低取向硅钢铁损,发展铸坯低温加热(≤1 300℃)和薄板坯连铸连轧流程生产取向硅钢工艺。 Main technology parameters of four developed process:cast bloom higher temperature heating-double cold rolling or single cold rolling,lower temperature heating-double cold rolling or single rolling process for production of common grain oriented silicon steel(CGO) and high magnetic induction grain oriented silicon steel(Hi-B),theory research on grain oriented steel(Goss nucleus and inhibitor) and present situation of process are summarized in this paper.The development trend of grain oriented si...