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研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c... 
2013-01-28 37 5.8

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%~100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 
2011-05-28 30 5.8

某厂对电工钢的轧制策略进行了优化,粗轧道次由“1+5”改为“1+3”。在优化后的生产过程中,每次变换钢种,烫辊材就会出现窄尺现象,而紧随其后的电工钢板则出现超宽现象。文中针对该问题,介绍了宽度设定模型和宽度自适应模型的原理,阐述了该问题出现的原因及解决方案,并通过对宽度自适应模型的应用研究及优化攻关,有效地解决了问题,大幅提升了实物质量,降低了宽度封锁率。 The rolling strategy of electrical steel was optimized in a factory,and the rough rolling pass was changed from “1+5”to“1+3”.Subsequently,the following problems were occurred in the production process:when the steel grade changed,the roasting roller steel before the electrical steel appeared the narrow width phenomenon,and then the electrical steel appeared the ultra-wide phenomenon.This paper introduced the principle of width setting model and width adaptive model,and expounded the causes and s... 
2022-02-28 33 5.8

本发明公开了一种改善取向硅钢内外圈和边部表面质量的方法及环形炉,在一次冷轧工序中,采用错边卷曲,卷曲张力按渐变张力进行控制且头尾的卷曲张力大、中部的卷曲张力小,MgO的涂覆量与卷曲张力同步变化且头尾的涂覆量少、中部的涂覆量多;在高温退火工序中,环形炉的底板上增设一层由若干扇形块绕中心均布形成的垫层,相邻扇形块之间存在空隙,环形炉的内罩内钢卷的上端加盖通风式的盖板,盖板底面的内圈间隙伸入钢卷孔、外圈间隙套在钢卷上、中间通过绕中心均布的导流槽支撑在钢卷端面上,导流槽呈螺旋状且入口与盖板内圈上的开口一一对应连通、出口延伸至盖板底面外圈内侧。本发明可显著减少表面缺陷,明显改善表面质量和磁性,操作容易。
2021-11-16 18 6.8

硅钢工业退火炉温度控制具有强耦合、纯滞后、多扰动等特点,它的控制方法代表着一类非线性系统控制的解决方法。以硅钢工业退火炉温度为控制对象,在双交叉限幅控制的基础上引入了智能学习系统,形成了基于智能学习系统的双交叉限幅控制方法来解决此类非线性系统的控制问题,并通过模块化的编程来实现其功能。结果表明:与传统的PID控制相比,该控制方法的控制精度、抗扰性等控制指标有明显提高,是解决此类非线性控制的一种有效方法。 The temperature control of silicon steel industrial annealing furnace has the features of strong coupling,pure lag,multidisturbance. The control method represents the solution of a class of nonlinear control systems. The control object is the temperature control of silicon steel industrial an-nealing furnace, the intelligent learning system based on Double Across Limit Control is introducedand used to solve control problem of this kind of nonlinear system, and the module programming isused to re... 
2014-05-28 12 5.8

本发明公开了一种高牌号硅钢的穿带激光焊接方法,包括:将焊缝中硅含量降低到Si焊<1.9%。采用激光+填丝焊接,填丝ER50‑6碳钢焊丝;根据焊缝截面积和激光焊接速度;激光填丝焊接时,激光线能量应足够大,达到填丝在熔池中充分混合,均匀分布,不至于填丝的成分浮在熔池的上半部分。采用此方法使焊缝组织从粗大铁素体变成细小、致密的无碳贝氏体,晶内沉淀相和晶间脆性相相对大幅减少,提高了焊缝韧性和成形性能,保证了高硅硅钢带的穿带焊接和连续生产。
2021-05-12 18 6.8

运用电子背散射衍射(EBSD)和X射线衍射(XRD)技术对硅钢热轧板的织构在板厚方向的分布进行了研究,并分析了两种织构测量方法的特点。EBSD技术能直观给出板厚方向的微观织构,XRD能得到钢板的宏观统计织构信息,结合两种技术的分析,能更直观更精确的研究不同织构在板厚方向的分布。 The texture distribution along the thickness of the silicon steel has been investigated by electron backscatter diffraction(EBSD) and X-ray diffraction(XRD) technique.The characteristics of two technique of texture analysis have been investigated.Combined the two techniques,the texture distribution along the thickness of the silicon steel could be realized distinctly and accurately. 
2011-02-28 39 5.8

目的提高硅钢的磁性能。方法采用多弧离子镀技术,在普通取向硅钢薄板两面沉积高硅FeSi合金层制得高硅梯度硅钢,并进行热处理,观察其显微组织,测量磁性能。结果退火态高硅梯度硅钢表面的高硅FeSi合金层与基底结合紧密,均匀致密。高硅梯度硅钢中硅含量呈梯度分布,最表层硅质量分数为11.0%,随着深度增加,硅含量逐渐降低,在距表面20μm处硅质量分数仍能达到6.5%。沉积态高硅梯度硅钢的电阻率ρ、低频铁损P10/50、高频铁损P10/1k及磁感应强度B8分别为68.6μΩ·cm,0.82W/kg,83.3 W/kg和1.73 T,退火后分别为63.1μΩ·cm,0.44 W/kg,54.38 W/kg和1.89 T。结论由于表层高硅FeSi合金层的存在,梯度高硅钢的低频磁学性能良好,但高频损耗需进一步改善。 Objective To improve the magnetic properties of silicon steel. Methods FeSi alloy coatings with high-silicon content were deposited on the surface of common grain-oriented silicon steel by cathodic arc plasma evaporation,and then a kind of high silicon gradient steel was prepared. The morphologies,content and magnetic properties of the samples were tested. Results FeSi alloy coatings were featured with compact microstructures and excellent adhesive quality with the substrates. The silicon conten... 
2014-03-28 27 5.8

本发明提供了一种提高无取向硅钢铁损均匀性的方法,所述方法包括,对无取向硅钢板坯进行加热和粗轧,获得中间坯;将所述中间坯精轧后以620‑750℃的温度进行卷取,获得热轧卷;将所述热轧卷进行酸洗和冷轧,获得冷轧卷;对所述冷轧卷升温至900‑960℃的温度保温50‑90s的时间,进行退火,获得铁损均匀性良好的无取向硅钢。本发明提供的方法,其铁损P1.0/50为1.379‑2.721W/kg,P1.5/50为2.751‑5.438W/kg,B5000为1.706‑1.741T,在线P1.0/50极差为0.062‑0.188W/kg,无取向硅钢的铁损更均匀。
2021-03-18 12 6.8

本发明公开了一种高硅钢的冷轧生产工艺。该生产工艺属于机械制造技术领域,其中的处理工序的加热工序通过电磁感应加热装置加热,待处理钢经过加热工序的速度为30‑200mpm,加热工序的加热温度为70‑120℃。本发明具有生产效率高和生产质量高的特点,特别是在加热工序中对待处理钢采用电磁感应加热装置进行加热,使其可以快速有效地提升温度,以满足高硅钢的冷轧生产工艺要求,减少断带事故,具有很好的实用性和创新性。
2021-09-26 16 6.8

本发明公开了一种高磁感取向硅钢高效脱碳退火工艺,主要工艺流程为:炼钢连铸→热轧→酸洗常化→冷轧→脱碳和初次再结晶退火→渗氮处理(低温Hi‑B)→涂覆氧化镁隔离剂→高温退火→拉伸平整退火→涂覆绝缘涂层→精整,低温HiB不同于高温Hi‑B的工艺流程主要是在脱碳退火后增加了渗氮段。本发明在保证产品实物质量不低于现有水平(国内领先水平)的前提下,使Hi‑B钢退火效率达到世界领先,制造成本大幅降低。
2021-09-26 19 6.8

本发明提出一种预判取向硅钢冷轧脆断发生的方法,将酸洗带头20‑30cm进行剪切取样,在取到的样板上面注明工作侧和传动侧;将取好的样板送至焊缝检测冲压机处,通过冲压机对样板进行冲压,根据不同钢带厚度,设定不同冲孔机压力,对样板进行冲压后,通过观察裂纹形貌,预判常化卷在冷轧轧制过程中是否会发生脆断,本发明使带钢在冷轧前能够制定相应的对策措施,从而降低冷轧断带所产生的损失。
2021-03-05 17 6.8

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