论文

利用XRD和EBSD研究了长轴分别平行于轧向(RD)、横向(TD)和轧面法向(ND)的柱状晶样品在热轧、冷轧及退火过程中的组织、织构演变规律,并分别从几何诱导和取向诱导两个方面分析了晶界的交互作用.结果表明,热轧时由表面摩擦剪切作用引起的组织和织构梯度直接影响并遗传给后续冷轧及退火样品.热轧后,不同样品的初始晶粒形状各向异性差异消失,形成相同的各向异性晶界组织,但晶体学各向异性发生改变,导致随后冷轧、退火组织及织构的变化均不同于直接冷轧的柱状晶样品.研究中特别关注了对磁性能有利的{100}取向区域与晶界的关系. Columnar grains show their special characteristics of morphological and crystallographic anisotropies, and thus markedly influence the microstructure and texture evolution during rolling and annealing process in electrical steel. The rolling and annealing microstructure and texture of three columnar grained samples with the long axes arranged along different directions were investigated by means of XRD and EBSD techniques, and the effects of columnar grain boundaries were analyzed from the view ... 

介绍了攀钢冶炼电工钢过程硫含量变化以及过程回硫、增硫情况,采取针对性措施,如:提高铁水装入量、转炉采用石英砂代替复合造渣剂造渣、RH脱硫等,降低钢中硫含量。结果表明:采取相应措施后,电工钢炼成率大幅提高,成品w[S]≤0.008%的比例由改进前的62%提高到92.4%,取得了明显的冶金效果。 The resulfurization and the change of sulphur content in production of electrical steel is analyzed.The targeted measures have been taken,such as increase the loaded quantity of liquid iron,quartz sand replaces the composite slagging agent in the converter and RH desulfurization to decrease the sulphur content of the steel.The result shows,after the measures have been taken,the finished product ratio of electrical steel increase a lot.The ratio of sulfur content of finished product no more than ... 

采用传统的轧制和退火工艺制备了0.30mm厚的6.5%(质量分数)Si高硅电工钢薄板,采用X射线衍射技术对退火过程中的再结晶织构进行了研究。冷轧高硅钢薄板700℃退火形成以{111}〈112〉为峰值的γ织构(〈111〉∥ND)和以{001}〈210〉为峰值的{001}织构;而900℃以上温度退火则形成强{001}〈210〉织构。进一步的研究表明是在晶粒长大过程中{001}〈210〉发展成为主要再结晶织构组分。 High silicon steel thin sheets with thickness of 0.3mm were successfully produced by conventional rolling and annealing methods.Recrystallization texture was investigated by means of X-ray diffraction.It is found that recrystallization texture is mainly composed of γ fiber(〈111〉∥ND)with peak at {111}〈112〉 and {001} fiber with peak at {001}〈210〉 after annealing at 700℃,while strong {001}〈210〉 component dominates recrystallization texture after annealing above 900℃.It is during grain growth that {... 

采用Nb对Fe-6.5%Si(质量分数)高硅钢进行微合金化处理,结果表明:Nb在高硅钢薄板制备过程中细晶效果明显.铸态、锻态和热轧态组织的晶粒分别细化了17.50%,24.51%和30.13%.铸态样品压缩强度由1365 MPa提高至1520 MPa,延伸率提高77.78%;温轧板试样室温拉伸强度由573 MPa提高至621 MPa,延伸率提高44.44%.利用XRD对厚度为0.30—1.68 mm的温轧板的板面织构演变过程进行跟踪测量,结果发现:初始织构以(011)〈100〉Goss织构为主,单道次变形量为26.2%的情况下,Goss织构完全转化为(100)〈011〉旋转立方织构,随后,在单道次变形为22.6%的情况下,旋转立方织构完全转化为{111}面织构,即纤维织构,并稳定保持至0.30 mm. Fe-6.5%Si（mass fraction） alloy possess perfect magnetic properties,though intermetallics of Fe₁₄Si₂ phase brought 6.5%Si leads to room temperature brittleness and hinder this significant materials industrialization.Nb was adopted into micro-alloying of Fe-6.5%Si high silicon steel. OM,thermal simulated test machine and XRD were employed to study the influence of Nb on high silicon steel in processing stages.Textures of warm-rolled high silicon steel strips were determined b... 

为开发高效电机用冷轧无取向电工钢,借助实验室薄板坯连铸连轧模拟设备及扫描电镜、透射电镜等检验手段研究了成分、组织、织构和析出物等对无取向电工钢磁性能的影响规律;结果表明:常化处理使组织均匀化并增加有利于磁性提高的织构组分;采用CSP流程开发的高效电机用无取向电工钢铁损平均值3.4 0 W/kg,磁感≥1.68 T。 In order to develop electrical steel for high efficiency motor,effect of components,microstructure,texture and precipitation on magnetic property of electrical steel are analyzed.From the result,normalizing treatment makes microstructure uniform and increases component of favorable texture.Iron loss of electrical steel developed by CSP line is 3.40W/kg and magnetic induction is more than 1.68T. 

利用本钢技术中心试验厂技术手段,并与北京钢铁研究院合作,试制了用作家电用电机、微电机、小电机或部分中型电机铁芯的冷轧无取向电工钢。试制钢硅含量小于0.5%,钢板表面平滑,公称厚度0.5mm,且厚度均匀偏差小,性能测定结果表明,产品的磁性能、力学性能满足其使用要求。 BX STEELTechnology Center pilot plant using technical means,and with Beijing Iron and Steel Research Institute,trial cold rolled non-oriented electrical steel that has been used as appliance motor core,micro motor core,small motor core,or part of the medium-sized motor core。Trial steel of silicon content is less than 0.5%,steel plate surface is smooth,the nominal thickness of 0.5mm,and the thickness deviation is small,performance measurement results show that the magnetic properties,mechanical p... 

【作者】 李波； 杨晓江； ...

【作者】 马芳； 张春红； ...

冷轧无取向硅钢（/%:0.003C,2.35Si,0.22Mn,0.011P,0.002S,0.36A1,0.003 0N）经890℃或940℃3 min常化的2.3 mm热轧板冷轧成0.35 mm薄板。研究了常化温度和800⁹20℃3 min退火对该钢高频（400Hz）磁性能和抗拉强度的影响。结果表明,830⁹20℃退火时高频铁损P_10/400值最低,随退火温度增加,晶粒尺寸增大,钢的抗拉强度降低;该钢的最佳热处理工艺为常化温度940℃,退火温度830℃,其抗拉强度R_m、高频铁损P_10/400和磁感应强度J₅₀分别为565 MPa,21.5 W/kg和1.69 T。 The cold-rolled non-oriented silicon steel（/%:0.003C,2.35Si,0.22Mn,0.011P,0.002S,0.36A1,0.003 0N） is cold-rolled to 0.35 mm sheet from 2.3 mm hot-rolled plate normalized at 890 ℃ or 940℃ for 3 min.The effect of normalizing temperature and annealing process at 800 ⁹20 °C for 3 min on high frequency（400 Hz） magnetic properties and tensile strength of the steel has been tested and studied.Results show that with annealing at 830 920 ℃the high frequency iron loss value P_10... 

取向硅钢利用析出物作为抑制剂,抑制初次再结晶晶粒的长大,抑制剂是取向硅钢发生二次再结晶的基本条件之一。文中通过低温板坯加热技术制备取向硅钢,采用透射电镜(TEM)观察并研究了高温退火阶段抑制剂的演化过程。结果表明,渗氮后形成的非晶态Si3N4析出物不稳定,在700～750℃退火升温阶段转化为(Al,Si)N;(Al,Si)N颗粒在800℃发生团聚,随后长大并粗化;(Al,Si)N是低温取向硅钢主要抑制剂,随退火温度的升高,(Al,Si)N抑制力大幅下降。 Precipitates as inhibitor are used to inhibit the grain growth of primary recrystallization in grain-oriented silicon steel,and inhibitor is one of the basic conditions for occurring of secondary recrystallization.The grain-oriented silicon steel was produced by low temperature slab heating and nitriding technique.The evolution of inhibitor was observed by transmission electron microscopy.The results show that Si3N4 particles are precipitated after nitriding,and Si3N4 particles are amorphous and... 

【作者】 张煜； 朱国辉； ...

试验研究了退火温度(850~950℃)和时间(5~18 min)对2.3 mm热轧硅钢板(/%:0.036C,3.15Si,0.21Mn,0.005P,0.007S,0.032A1)6道次轧制的0.35 mm冷轧板组织和织构的影响。结果表明,退火温度越高,晶粒平均尺寸越大,900℃5 min退火时平均晶粒尺寸41.39μm,试样织构主要集中在γ取向线上的{111}<112>织构组分和{111}<110>织构组分;900℃18 min退火时平均晶粒尺寸为48.08μm,试样的{111}面织构和{112}面织构密度都明显减弱,{001}面织构增强,磁性能较优。 The effect of annealing temperature(850 ~950 ℃) and holding time(5 ~ 18 min) on structure and texture of 0.35 mm sheet by 6 passes cold-rolling from 2.3 mm hot-rolled plate of silicon steel(/%:0.036 C,3.15 Si,0.21 Mn,0.005 P,0.007 S,0.032A1) has been tested and studied.Results show that the higher the annealing temperature the coarser the average grain size;As annealing at 900 ℃ for 5 min the average grain size of steel sheet is 41.39 μm,and the texture in sample is mainly concentrated in y orie...