论文

某冷连轧机生产无取向硅钢板材时,其边缘降的长度合格率频繁超标。为满足用户的叠片厚度精度要求,这类产品必须以增大切边量的方式来保证交货质量,而这种方式又直接降低了金属收得率,提高了生产成本。基于此,以该产线现有设备特性为基础,详细分析其软、硬件功能模式,分别对辊形与反馈控制进行全面分析与优化改进。通过现场试验论证,充分明确依托辊形优化与反馈控制程序的改进能显著提高边缘降的控制水平,该技术的使用为生产现场的边缘降控制提供了合理的技术支撑。 A cold rolling mill production of non-oriented silicon steel sheet,the thickness difference of the edge( edge-drop) is usually exceed the preset standard value,In order to meet the accuracy requirements of the user flatness,these production must be trimed wider length to meet the delivery quality of the user need, which directly reduce the metal yield and increase the manufacturing cost. Therefor,the software and hardware of the production line has been analyzed, and the work roll shape and feed... 

观察了取向硅钢极薄带经冷轧至不同厚度,并经过不同工艺热处理后的显微组织及亚结构。结果表明:冷轧压下量越大,显微组织中位错密度越高,冷变形组织越多,等轴晶粒越少;增加冷轧压下量可以使试样的再结晶温度降低,当钢带厚度为0.08 mm时,在650℃退火时就能发生明显的再结晶。 Microstructure and substructure of the grain oriented ultra-thin silicon steel sheets is analyzed,which are rolled down to different thickness and treated with different heat treatment process.The result shows that there are higher dislocation density,more cold deformation structure and less equiaxed crystal grain in microstructure of the steel sheets with more cold rolled reduction.Increase of cold rolled reduction will decrease recrystallization temperature,and when thickness of the steel shee... 

绝缘涂层可以有效提高硅钢片的耐蚀、耐腐、磁、绝缘等性能，因此取向硅钢涂装绝缘涂层是取向硅钢生产过程中重要的一环。本文对取向硅钢含铬无机绝缘涂层以及氮化铬涂层的性能优缺点进行了介绍，并对国内无机含铬取向硅钢绝缘涂层及氮化铬涂层的研究现状进行了综述。最后对未来含铬无机绝缘涂层的研发方向进行了展望。 Insulation coating can effectively improve the corrosion resistance of silicon steel sheet, such as corrosion, magnetic, insulation performance, thus oriented silicon steel insulation coating is the important part of oriented silicon steel production process. In this paper, the inorganic insulation coating oriented silicon steel containing chromium and chromium nitride coating performance advantages and disadvantages are introduced.In addition, the research status of insulation coating and chrom... 

结合实际生产0.4%Si无取向硅钢，统计了不含Sn和0.025%Sn无取向硅钢的磁性能变化，利用金相显微镜、X射线衍射仪观察分析不同成分下试样的显微组织和微观织构。试验结果表明：Sn元素可以显著降低无取向硅钢的晶粒尺寸，0.025%Sn试样的平均晶粒尺寸比不含Sn减小28.4%;加入Sn元素后抑制了无取向硅钢中不利于磁性能的{111}面织构组分强度，提高了对磁性能有利的{100}面织构组分强度，0.025%Sn与不含Sn相比磁感均值从1.756 T提升至1.768 T,铁损均值从5.476 W/kg降低至5.204 W/kg,明显改善了无取向硅钢磁性能。 In this paper combined with the actual production of 0.4% Si non oriented silicon steel, the magnetic properties of non oriented silicon steel without Sn and 0.025% Sn were counted. The microstructure and microtexture of samples with different compositions were observed and analyzed by metallographic microscope and X-ray diffraction. The results show that: Sn can significantly reduce the grain size of non oriented silicon steel, and the average grain size of 0.025% Sn sample is 28.4% smaller tha... 

采用EBSD技术研究了有、无拉应力作用下无取向硅钢在晶粒长大过程中织构转变及晶界变化的规律。结果表明:在晶粒生长期间,无应力作用下的硅钢中,{111}〈112〉,{111}〈110〉织构组分强化,而{100}〈001〉织构组分弱化;与无拉应力作用下的情况相比,施加5MPa的拉应力时,{111}〈112〉,{111}〈110〉织构组分强化的速率下降,{100}〈001〉织构组分变化不明显。对于在晶粒生长期间持续变化的{111}〈112〉,{111}〈110〉和{100}〈001〉织构组分而言,虽然有、无拉应力作用下硅钢的{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率均下降,而{100}〈001〉织构组分的高取向差角度晶界频率则上升,但当有拉应力作用后,{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率下降的速率变小,{100}〈001〉织构组分的高取向差角度晶界频率上升的速率稍有变小。通过对无取向硅钢在晶粒长大过程中织构转变及晶界变化规律的研究,分析了合金原子在晶界的偏聚行为。 The rules of texture and grain boundary transformation in the nonoriented silicon steel under applied stress or without applied stress during grain growth were investigated by EBSD.The results show that the {111}〈112〉 and {111}〈110〉 components in the nonoriented silicon steel without stress are strengthened during grain growth whereas {100}〈001〉 component is weakened,but the growth rate of {111}〈112〉 and {111}〈110〉 component decreases,while the area fraction of {100}〈001〉 component doesn’t chang... 

通过制备磷酸二氢铝硅钢涂层,研究了氧化锌对无铬涂层耐盐雾性能、电化学性能和附着性的影响。结果表明,硅钢表面涂层含有4.0%的氧化锌时,涂层具有最高的耐腐蚀性能和电化学性能,而且其致密表面最为平整,没有裂纹出现。 The effects of ZnO on the salt spray resistance property, electrochemical performance and adhesiveness of silicon steel insulating coating were studied. The results show that the best corrosion resistance and electrochemical properties can be obtained when the coating contains 4.0% oxide zinc, and the dense surface is smooth without cracks. 

聚焦无取向硅钢产品标准,从电磁性能、表面性能、机械性能以及尺寸公差与边部质量等维度对国际标准IEC、EN、JIS、ASTM以及国标GB进行了分析研究。分析得出,各类标准在电磁性能方面要求基本一致;ASTM标准的机械性能要求有别于其他几个标准。 In this paper,non-oriented silicon steel standards of EN,JIS,GB and ASTM were compared and analyzed. It is showed that,all types of standards in electromagnetic performance requirements are basically the same. Surface properties in ASTM standard are expressed in the most detailed. The mechanical properties requirements of the standards,except for ASTM,are basically the same. 

对高牌号无取向电工钢35W300的成品进行了第二次退火,对第二次退火后的成品性能、纵横向磁性能差异和组织变化进行了分析。结果表明,随着第二次退火温度的升高,晶粒长大,磁性能优化。铁损平均值下降0.087 5W/kg,磁感平均值升高0.008T。第二次退火温度为820℃的产品的磁性能能够满足用户使用要求。 The product of high grade non-oriented electrical steel 35W300 was annealed at the second time.Microstructure,the difference of magnetic properties in the vertical and horizontal and were studied.The results show that the grain grew up and magnetic properties optimized with the increase of annealing temperature for the second time.Iron loss average declines in 0.0875 W/kg,magnetic induction average increases 0.008 T.The magnetic properties can meet the requirements of users at the second anneali... 

【作者】 侯桂芹； 张颖； ...

【作者】 李波； 杨晓江； ...

利用XRD和EBSD研究了长轴分别平行于轧向(RD)、横向(TD)和轧面法向(ND)的柱状晶样品在热轧、冷轧及退火过程中的组织、织构演变规律,并分别从几何诱导和取向诱导两个方面分析了晶界的交互作用.结果表明,热轧时由表面摩擦剪切作用引起的组织和织构梯度直接影响并遗传给后续冷轧及退火样品.热轧后,不同样品的初始晶粒形状各向异性差异消失,形成相同的各向异性晶界组织,但晶体学各向异性发生改变,导致随后冷轧、退火组织及织构的变化均不同于直接冷轧的柱状晶样品.研究中特别关注了对磁性能有利的{100}取向区域与晶界的关系. Columnar grains show their special characteristics of morphological and crystallographic anisotropies, and thus markedly influence the microstructure and texture evolution during rolling and annealing process in electrical steel. The rolling and annealing microstructure and texture of three columnar grained samples with the long axes arranged along different directions were investigated by means of XRD and EBSD techniques, and the effects of columnar grain boundaries were analyzed from the view ... 

以质量分数为25%的丙烯酸乳液MC-102、15%Al(H2PO4)3溶液、0.01%H3BO3、0.01%Zn(Ac)2·2H2O和2%二乙二醇丁醚组分,在不同固化工艺下制备涂层。极化曲线和电导率测试发现300℃处理60 s得到的涂层具有良好的耐腐蚀性和绝缘性;水煮实验证明该涂层具有良好的耐水性;断口线扫描发现涂层具有良好的附着性。 A formula comprising MC-102 acrylic emulsion 25%,aluminium dihydrogen phosphate15%,boric acid 0. 01%,zinc acetate dihydrate 0. 01% and diethylene glycol monobutyl ether 2% was used to prepare coatings via different treatment process. The conductivity test and polarization curves revealed that a coating cured at 300 ℃ for 60 s showed good insulative and anticorrosive properties. The water boiling test indicated that the said coating had good water resistance. A cross section of the coating was in...