硅钢资料

本发明公开了一种超薄取向硅钢用的半有机绝缘涂料。该半有机绝缘涂料，按质量百分比计，包括以下组分：10～25％磷酸盐，1～10％含有环氧基的硅烷耦合剂，0.2～2.0％有机硅烷，1～10％铬酐，1.5～6％二氧化硅粒子，0.3～5％碱，余量为水；其中二氧化硅粒子的粒径为100～300nm。该半有机绝缘涂料应用于超薄取向硅钢表面时，既提高了涂层与基体的附着性，又保证了涂层的绝缘性和耐热性，涂层附着性为A级，叠片系数大于0.96，可耐900℃高温，并且涂层较薄(小于1μm)时，钢板的绝缘电阻大于30Ω·cm2/片，绝缘性能优异，可满足超薄取向硅钢的应用需求。

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

本发明涉及取向硅钢技术领域，尤其涉及一种取向硅钢边浪的控制方法、装置、设备和存储介质，该方法包括：在将通过脱碳退火阶段的取向硅钢的带钢进行卷取过程中，在带钢的下端侧上刻上刻痕线，其中，下端侧为带钢与高温退火炉的承托底板接触的一侧，刻痕线平行于带钢轧制的方向；控制卷取后的带钢通过高温退火阶段和热拉伸平整阶段后至精整阶段时，沿着刻痕线，切除带刚的边浪；其中，边浪为在带钢的刻痕线至下端侧的边的部分。该控制方法可显著改善高温退火后取向硅钢边部浪形，有效降低精整切边量，提高取向硅钢的板形质量及成材率，降低生产成本。

借助电子背散射(EBSD)技术对AlN为主抑制剂的Hi-B取向硅钢常化工艺的中间冷却制度进行了研究。结果表明:常化后试样均发生了完全再结晶,在60℃/s冷速下组织最均匀;在合适的冷却制度下常化板表层保留了强的Goss织构,它深入到1/4厚度处,并且形成对Goss织构有利的强{554}<225>织构。 The intermediate cooling system of Hi-B oriented silicon steel with AlN main inhibitor in normalizing process was studied by means of electron back diffraction(EBSD) technique. The results show that:the specimens after normalizing are fully recrystallization, and the microstructure is most uniform under the intermediate cooling rate of 60℃/s; under suitable cooling system, normalized plate surface retains strong Goss texture, it penetrates into the 1/4 thickness of the plate and forming strong {... 

热卷箱位于热连轧带钢生产线粗轧与精轧机之间,是热连轧生产中比较理想的中间保温设备。由于取向硅钢变形温度区间较窄,在生产中易出现边裂现象,同时中间坯的边部温度难于得到保证,因此一般不采用热卷箱设备生产,限制了传统热连轧生产线产品开发的品种。通过合理优化热卷箱控制工艺参数,解决了某厂传统热连轧生产线用热卷箱生产取向硅钢的边部质量问题,成功地生产出取向硅钢带。 The hot coil-box is an ideal heat retaining apparatus for hot rolling,lined between roughing mill and finishing mill. But oriented silicon steel has a narrow deformation temperature range,so that the edge crack easily occurs and it is difficult to insure the temperature of the intermediate blank. Therefore,the hot coil-box is rarely used in producing oriented silicon steel,which restricts the product development of the traditional hot rolling line. The article reasonable optimized process parame... 

对无取向电工钢中的夹杂进行了系统的分析。利用小样电解,采取不同电解液,不同的分离方法对无取向电工钢中稳定和不稳定夹杂物进行了提取、分离和收集。利用扫描电镜(SEM)、X-射线衍射、ICP等对电解分离收集的夹杂物进行了定性和定量分析。 The inclusion analysis of the non-oriented electrical steel has been investigated.By using small sample electrolytic analysis,with different electrolytes and different separation ways,the stable inclusions and unstable inclusions was drew,separated,and collected.With utilizing the methods of SEM,X-ray and ICP,the qualitative and quantitative analysis of inclusions in the non-oriented electrical steel was obtained. 

本发明公开了一种硅钢冷轧吹扫辊，涉及硅钢加工设备领域，包括安装架、上轧辊和下轧辊、下调节机构、上调节机构以及吹扫机构；所述下调节机构包括调节支撑底板、楔形插块以及调节油缸；所述上调节机构包括顶升油缸、顶升杠杆和顶升连杆；所述吹扫机构包括吹扫连接座、吹扫管道和吹扫排管。本发明通过在上轧辊和下轧辊的出料端安装吹扫机构能够便于对出料的钢带表面进行吹扫清洁，能够有效提升钢带成品的表面质量；由于下轧辊在轧制过程中承受的重量较大，通过调节油缸带动下轧辊两侧的楔形插块来回移动的方式对下轧辊的高度进行微调，能够保证下轧辊在轧制过程中整体的稳定可靠性。

运用电子背散射衍射(EBSD)技术,研究了50W600无取向硅钢在热轧→冷轧→退火工序间织构的演变。结果表明:由于热轧板沿板厚方向的应力场和温度场存在差异,导致热轧板不同层织构类型和强度存在差异;热轧板表层主要存在铜型、黄铜和高斯织构,1/4层织构主要为α纤维织构和较弱的高斯织构,中心层织构较单一,主要为α纤维织构;和热轧板相比,冷轧板各层织构差异较小,为典型的轧制织构(α纤维织构和γ纤维织构);退火板各层都表现为γ纤维织构增强、α纤维织构减弱,旋转立方织构基本消失。 The texture evolution of 50W600non-oriented silicon steel in hot rolling,cold rolling and annealing process was investigated by electron back-scatter diffraction(EBSD)technology.Results show that the hot rolled plate texture types and intensities along thickness direction were different because of the different stress fields and temperature fields.The major texture types in the surface of hot rolled plate were copper,brass and Gauss texture.The texture was composed ofαfibre texture and weaker Ga... 

本发明提供一种能够有效地抑制去应力退火中的渗碳、氮化的，实施了耐热型的磁畴细化处理的取向性电磁钢板。该取向性电磁钢板在一侧面具有多个槽，在所述钢板的表面至少具备镁橄榄石被膜，该多个槽是朝向横切轧制方向的方向线状地延伸且在该轧制方向隔着间隔地并列，并且，形成于所述槽的底部的所述镁橄榄石被膜厚度的平均值为0.45μm以上，并且该厚度的标准偏差σ为0.34μm以下。

取向硅钢常化工序主要采用现场实测带钢温度的方式测定冷却速率，并通过稳定冷却水温、调整冷却水量及喷梁运行数量等方式保证合理的冷却速率，给常化工艺设计和生产带来诸多不便。通过对常化工艺水冷过程带钢的传热分析求解，在建立带钢水冷温度模型的基础上，研究了不同冷却工艺参数对带钢温度及冷却速率的影响规律以及冷却工艺的交互作用结果。结果表明：模型计算结果能够较好地反映取向硅钢在常化水冷过程中的温度及冷却速率的变化，其计算误差为0.80%～4.11%;在特定取向硅钢厚度规格和常化工艺下，随着常化冷却水量及有效冷却长度的增加，带钢水冷温度及冷却速率与呈非线性变化；常化水冷工艺主要通过调控带钢与冷却水之间热交换量和交换时间实现对带钢温度的控制，实际生产中需综合考虑机组速度、冷却水量及有效冷却长度之间的交互作用，选定喷梁投入数量和冷却水量以获得稳定的冷却速率。 The cooling rate of normalization process mainly determined by measuring the grain oriented silicon steel strip temperature on site, and ensures the cooling rate by stabilizing the cooling water temperature, adjusting the cooling water volume and the operation quantity of spray beam, which brings inconvenience to the normalization process design and production. Based on the heat transfer of strip in the water cooling section of normalization process, the water cooling temperature model for the n... 

本实用新型公开了一种硅钢片二次搭接夹具，包括底座、位于底座顶部的调节板以及位于调节板顶部一端的固定杆，所述底座包括设置在底座内部顶端中间位置处的活动槽。本实用新型通过连接块将第一夹钳与第二液压缸的输出端相连接，通过第一夹钳和第二夹钳对硅钢片进行固定，将焊条焊接在一组硅钢片上，伺服电机带动调节杆发生转动，调节杆外侧的外螺纹和活动块内部的螺纹孔相互配合，可使活动块在活动槽内部发生活动，通过活动块带动调节板发生前后移动，从而使对硅钢片进行前后一端，通过滑轨使调节板的移动更加稳定，使两组硅钢片相对齐，通过固定块使第一液压缸带动调节架左右移动，使焊条与两组硅钢片紧密接触，实现二次搭接。

运用EBSD和光学显微镜,研究了0.25%~0.45%Cu对无取向电工钢热轧板显微组织,成品板显微组织、织构和磁性能的影响。实验结果表明:卷取过程中Cu元素在热轧板表层的偏聚作用显著阻碍了热轧板表层再结晶晶粒长大,导致热轧板表层晶粒尺寸随着Cu含量增加而逐渐较小,但热轧板中间晶粒尺寸变化不大。同时发现Cu元素能够明显改善织构类型,使有利织构组分增加,不利织构组分减少,同时减弱织构强度。从实验结果可知0.35%Cu能够显著改善电工钢的磁性能,铁损P15/50最低达到4.1 W/kg,磁感B50最高值达到1.8 T。 Effects of high content Cu on microstructure of hot rolled plates and microstructure,texture and magnetic properties of annealed finish product plates of non-oriented electrical steel were examined by means of EBSD technique and optical microscope. The results show that surface segregation of Cu significantly hindered recrystallized grain growth of surface layer in hot rolled plate during the coiling,as a result,the surface grain sizes of the hot-rohed plates decrease with the increase of Cu con...