硅钢资料

试验了通过NaCl-KCl-NaF-SiO₂熔盐在电流密度50 mA/cm²、电沉积脉冲电流正反向比9:1和750⁸50℃60min电沉积下阴极（/mm）20×20×0.5的1.6Si无取向冷轧硅钢片断面层硅的分布,并通过计算得出Si的扩散系数。结果表明,电沉积温度由750℃提高至850℃时,试样中Si含量增加,扩散的深度由18μm提高到40μm;电沉积温度与Si在钢中的扩散系数近似符合Arrhenius指数关系。 The distribution of silicon at cross section of cathode（/mm） 20 × 20 × 0.5 sheet of 1.6Si non-oriented cold rolled silicon steel after electro-deposit treatment by NaCl-KCl-NaF-SiO₂ molten salt with current intensity 50 mA/cm²,electro-deposit pulse current positive-negative ratio 9:1 at 750 850 ℃ for 60 min has been tested and the diffusion coefficient of Si is obtained by calculation.Results show that with increasing electro-deposit temperature from 750 ℃ to 85... 

以取向电工钢成分为基础,制备了含C或Mn和S的4种实验钢。观察了接近平衡析出状态实验钢经60%冷轧后在600～1000℃范围再结晶退火过程中微观组织演变,统计分析了再结晶体积分数随退火时间的变化规律,进而计算了各实验钢静态再结晶的激活能。观察了高含C实验钢退火初期再结晶晶粒优先出现的部位。结果表明900～1000℃范围内各实验钢铁素体的化学成分相似,因而其再结晶激活能基本一致。在600～800℃范围内铁素体内会有阻碍再结晶进程的三次渗碳体析出,从而使再结晶激活能明显提高。高C含量实验钢中还会有从奥氏体转变而来的粗大珠光体或渗碳体,轧制过程中其附近形成的变形区会促进600～800℃加热时该区域附近率先发生再结晶形核、降低再结晶激活能。固溶的Mn、S元素可微弱提高再结晶激活能,但高Mn、S含量会改变粗渗碳体从奥氏体析出时的形态。 Four experimental steels based on grain oriented electrical steel containing C,or Mn and S were prepared.Microstructure evolution of the steels close to a state of equilibrium precipitation were observed during annealing processes at 600-1000 ℃after 60% cold rolling,the changes of recrystallization volume fraction were analyzed statistically as the annealing was prolonged,and the activation energy for static recrystallization of the steels were calculated.The locations,where the recrystallizatio... 

【作者】 吴清； ...

采用Nb对Fe-6.5%Si(质量分数)高硅钢进行微合金化处理,结果表明:Nb在高硅钢薄板制备过程中细晶效果明显.铸态、锻态和热轧态组织的晶粒分别细化了17.50%,24.51%和30.13%.铸态样品压缩强度由1365 MPa提高至1520 MPa,延伸率提高77.78%;温轧板试样室温拉伸强度由573 MPa提高至621 MPa,延伸率提高44.44%.利用XRD对厚度为0.30—1.68 mm的温轧板的板面织构演变过程进行跟踪测量,结果发现:初始织构以(011)〈100〉Goss织构为主,单道次变形量为26.2%的情况下,Goss织构完全转化为(100)〈011〉旋转立方织构,随后,在单道次变形为22.6%的情况下,旋转立方织构完全转化为{111}面织构,即纤维织构,并稳定保持至0.30 mm. Fe-6.5%Si（mass fraction） alloy possess perfect magnetic properties,though intermetallics of Fe₁₄Si₂ phase brought 6.5%Si leads to room temperature brittleness and hinder this significant materials industrialization.Nb was adopted into micro-alloying of Fe-6.5%Si high silicon steel. OM,thermal simulated test machine and XRD were employed to study the influence of Nb on high silicon steel in processing stages.Textures of warm-rolled high silicon steel strips were determined b... 

【作者】 朱凤泉； 黄生银； ...

采用火花源原子发射光谱分析测定电工钢中超低C,研究试样制备方法、Ar纯度和压力等条件对分析结果的影响,并对工作曲线进行了优化,实现了一次分析同时测定电工钢的多种元素,满足炉前和精炼在线分析的要求。 Ultra-low carbon in electrical steel is determined with spark-source atom emission spectrum.It is researched the influence of sample making method,purity of Ar,and pressure on analysis result.The work curve is optimized.The determination of many elements in electrical steel only in one analysis is realized.It meets demands of on-line analysis for blast furnace and refining. 

利用OM、SEM、TEM等实验方法研究了卷取工艺对一种新型含铜无取向电工钢晶粒度和析出相的影响。结果表明,该电工钢热轧带卷取后的晶粒尺寸为18～24μm,在卷取过程中,热轧带中有一定数量的第二相析出,经EDS能谱及选区电子衍射分析,这些析出相主要为AlN。随着卷取工艺的变化,该电工钢的晶粒度大小变化不明显,析出相的类型、尺寸大小不发生改变,体积分数发生一定的改变。 The effects of coiling process on grain size and precipitates of a new copper-bearing non-oriented electrical steel were investigated by OM,TEM and other experimental method.The results show that the grain size of hot-rolled bands after coiling is 18～24 μm.The second phases precipitate during coiling process.They are mainly AlN by EDS spectra and selected area electron diffraction.With the change of coiling process,the grain size of the electrical steel does not change significantly;the type and... 

基于简化的取向硅钢片模型,系统地对不同的交流激励下的硅钢叠片内铁损、交链磁通和空气中指定位置的法向漏磁的分布进行了\"单片级\"的测量,并建立了相应的硅钢叠片级问题的三维有限元分析模型,进行了大规模的数值计算分析。模型实验和数值分析的结果表明垂直进入硅钢片的漏磁通和损耗呈现浅透入的特点,在硅钢片内引起的涡流损耗在总铁损中占据了\"举足轻重\"的份额。用电磁场有限元分析软件MagNet瞬态场时步法计算结果与测量结果相吻合,说明本文方法研究复杂的硅钢叠片问题的有效性。 The measurement and 3D finite element analysis of the iron loss,interlinkage flux inside the laminated silicon steel sheets and the magnetic flux densities at the specified positions are carried out based on a verifying silicon steel sheet model.The modeling results show that the leakage flux vertically through the silicon steel sheets has the peculiarity of shin effect,and the eddy current loss caused by the AC leakage flux is a significant component of the total iron loss.The calculated result... 

利用EBSD技术研究了电工钢中长轴平行于轧向的柱状晶样品在热轧和退火过程中组织和取向的演变规律,并与长轴平行于板法向的样品的已有研究结果进行对比。结果表明,无论柱状晶按何种方向排列,只要表面存在剪切力,热轧后都可形成剪切织构,同时中心形成轧制织构,主要包括旋转立方织构和{112}<1-10>。柱状晶造成的影响主要体现在板中心层,长轴平行于轧向排列的样品热轧时形成的粗大旋转立方晶粒要到脱碳退火后才能完全消除,但破坏了正常的不同取向晶粒间的取向差分布及尺寸均匀性,导致二次再结晶不完全及磁性能降低。 The evolution of microstructure and grain orientation in an electrical steel containing columnar grains with its long axis being parallel to the rolling direction of sheet was studied during hot rolling and annealing by EBSD technique.The results are compared with those of samples containing columnar grains being parallel to normal direction of sheet reported in the reference [3].It was shown that,whether the long axis of columnar grains was arranged in RD or ND,shear textures can be formed in t... 

高强无取向硅钢主要应用于高速电机，要求其具备高强度和优异磁性能，但目前无取向硅钢的磁性能和强度难以兼顾。因此，设计并制备了添加微量Cr的含Nb高强无取向硅钢，通过光学显微镜、EBSD、万能拉伸试验机、四探针测试仪和磁性能测量仪等研究了Cr对含Nb高强无取向硅钢微观组织、织构、力学性能及磁性能的影响。结果表明，添加质量分数为0.5%的Cr抑制了热轧组织的回复，使常化和退火组织再结晶减弱，常化和退火后有利织构面积分数增加，不利织构面积分数减小。添加质量分数为0.5%的Cr使含Nb无取向硅钢的屈服强度显著增大，磁感略升高，但对铁损几乎没有影响。Cr对屈服强度的影响一方面是由于Cr的固溶强化作用，另一方面Cr促进了Nb的析出而使Nb的析出强化效果增强；而Cr提高含Nb高强无取向硅钢的磁感主要是由于促进有利织构形成的同时抑制了不利织构的形成，使得织构因子增大；添加Cr使无取向硅钢的电阻率增加从而使铁损降低，同时Cr促进了Nb的析出，而这种富Nb析出相不仅抑制晶粒长大且会阻碍磁畴移动而使铁损增高，在两方面因素的综合作用下，添加质量分数为0.5%的Cr对含Nb高强无取向硅钢的铁损几乎没有影响。因此，... High strength non-oriented silicon steel is mainly used in high-speed motors, which requires good mechanical and magnetic properties. However, it is difficult for non-oriented silicon steel to obtain high strength and good magnetic properties at the same time. In this paper, the Cr-microalloyed Nb-containing high strength non-oriented silicon steel was designed and prepared. The effect of Cr on the microstructure, texture, mechanical properties and magnetic properties of Nb-containing high stren... 

通过金相分析和电子背散射衍射技术研究了一种新型含铜无取向电工钢在950℃退火不同时间(3～180s)空冷后的组织和织构取向的演变。结果表明:该钢在退火3s时的主要织构为α和γ线织构,{100}<110>织构最强;退火20s时织构以<111><112>、{111}<110>、{112}<110>、高斯织构和立方织构为主,随着退火时间的延长,高斯织构和立方织构强度呈减弱趋势;合理控制保温时间有利于提高{100}、{110}面织构的占有率。 Evolution of microstructure and texture oriented of a new non-oriented electrical steel during annealing at 950℃for different times(3-180) s and air cooling was studied by metallography and electron back-scattering diffraction analysis.The results show that after annealing for 3 s most of the texture oriented alongα-fibre andγ-fibre,the intensity of {100}〈110〉was the strongest.{111}〈112〉,{111}〈110〉,{112}〈110〉,Gauss texture and cube texture were the main texture after annealing for 20 s,with the ... 

从影响高牌号无取向硅钢退火工艺的主要参数入手,介绍高牌号无取向硅钢退火炉在加热、气氛控制、冷却、涂层烘烤方面的新技术,并展望无取向硅钢退火炉的发展方向。 Based on the technology parameters of high-grade non-oriented silicon steel annealing,the new technology of the annealing line,which includes heating,atmosphere control,cooling,coating baking,is introduced,and the development direction of non-oriented silicon steel annealing furnace is pointed out.