钢厂
退火温度对3.1%Si无取向硅钢组织织构与磁性能的影响
研究了退火温度对3.1%Si无取向硅钢组织和磁性能的影响规律。结果表明:退火温度从940℃提高至1 000℃,平均晶粒尺寸由98μm增加到145μm,铁损P1.5/50从2.576 W/kg降低至2.408W/kg。随着退火温度的升高,γ不利织构组分强度逐渐降低,{111}〈112〉织构组分强度降低约16%,磁感B50逐渐升高,磁性能水平提高。 The effects of annealing temperature on microstructure and texture and magnetic properties of 3.1%Si non-oriented silicon steel were investigated in this paper.The results showed that,when the annealing temperature increased from 940℃ to 1 000℃,the average grain size of metallographic structure increased from 98μm to 145μm,the iron loss value P1.5/50 decreased from2.576 W/kg to 2.408 W/kg.And as the annealing temperature increased,the strength of the unfavorable texture componentγgrad...
无取向硅钢晶粒长大过程中应力对织构和晶界变化的影响
采用EBSD技术研究了有、无拉应力作用下无取向硅钢在晶粒长大过程中织构转变及晶界变化的规律。结果表明:在晶粒生长期间,无应力作用下的硅钢中,{111}〈112〉,{111}〈110〉织构组分强化,而{100}〈001〉织构组分弱化;与无拉应力作用下的情况相比,施加5MPa的拉应力时,{111}〈112〉,{111}〈110〉织构组分强化的速率下降,{100}〈001〉织构组分变化不明显。对于在晶粒生长期间持续变化的{111}〈112〉,{111}〈110〉和{100}〈001〉织构组分而言,虽然有、无拉应力作用下硅钢的{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率均下降,而{100}〈001〉织构组分的高取向差角度晶界频率则上升,但当有拉应力作用后,{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率下降的速率变小,{100}〈001〉织构组分的高取向差角度晶界频率上升的速率稍有变小。通过对无取向硅钢在晶粒长大过程中织构转变及晶界变化规律的研究,分析了合金原子在晶界的偏聚行为。 The rules of texture and grain boundary transformation in the nonoriented silicon steel under applied stress or without applied stress during grain growth were investigated by EBSD.The results show that the {111}〈112〉 and {111}〈110〉 components in the nonoriented silicon steel without stress are strengthened during grain growth whereas {100}〈001〉 component is weakened,but the growth rate of {111}〈112〉 and {111}〈110〉 component decreases,while the area fraction of {100}〈001〉 component doesn’t chang...
加热温度对W470高硅钢连铸坯氧化铁皮的影响
采用SEM、EDS和XRD对不同加热温度下W470连铸坯氧化铁皮的微观形貌及相结构进行研究。结果表明,W470氧化铁皮难以除去的原因是氧化铁皮熔化,液相包裹着FeO,凝固时发生共晶反应,生成FeO/Fe2SiO4共晶混合物,并深嵌入基体。降低加热炉的加热温度,使连铸坯全程在FeO/Fe2SiO4共晶混合物熔点(1177℃)以下加热,可降低氧化铁皮与基体的结合力,能够有效解决W470除鳞困难问题。 The microstructure and phase structure of iron scale of W470 continuous casting billet at different heating temperatures were investigated by SEM,EDS,and XRD.The results show that the reason why the iron scale of W470 removes hardly is that iron scale is melted and the FeO is surrounded by the liquid phase,which forms FeO / Fe2SiO4eutectic mixture and is embedded into the matrix after solidification.Lowering the heating temperature and keeping the continuous casting billet heating under the melt...
双辊薄带连铸3.98%Si-0.71%Al无取向硅钢的组织、织构和磁性能
采用双辊薄带连铸工艺制备了厚度为2.4mm的3.98%Si-0.71%Al无取向硅钢带,经常化、冷轧、不同温度退火后,对其显微组织、析出物、织构和磁性能进行了检测分析。结果表明:随着退火温度的提高,退火板晶粒尺寸增大,组织均匀性提高;退火板析出物主要是AlN和MnS与AlN复合析出物,尺寸较粗大,达0.5~2.5μm;退火板织构沿厚度方向变化明显,表层和1/2层存在较强的{100}织构,1/2层还存在较强的{111}织构,1/4层主要是{112}织构;随退火温度的升高相应的铁损和磁感应强度均降低。 Using twin roll thin strip continuous casting technique,the 3.98%Si-0.71%Al no-oriented silicon steel strip in thickness of 2.4mm was produced.The microstructure,precipitates,texture,and magnetic properties of the sheet after normalizing,cold rolling and annealing at different temperatures were studied.The results show that with annealing temperature increase,the grain size and uniformity of annealed sheet increased.The main precipitates in coarse size of 0.5-2.5μm in annealed sheet were AlN and...
酸溶铝对铸态取向硅钢中第二相粒子组成和形貌的影响
试验的铸态取向硅钢(/%:0.0440.056C,3.123.32Si,0.080.11Mn,0.0020.008S,0.002 90.029 1Als,0.006 20.010 9N)由30 kg高频真空感应炉熔炼。通过场发射扫描电子显微镜/能谱仪(FE-SEM/EDS)研究结果表明,0.002 9%Als钢中氧化物主要为SiO2,存在片状、棒状及近似球状的独立MnS,未发现含铝的氧化物或氮化物;0.0090%Als钢中出现以Al2O3为主的复合氧化夹杂物,存在MnS与AlN的复合析出物。钢中Als增加,复合析出物多呈簇状发展。氧化物容易成为MnS-AlN复合析出的核心,钢中Als含量越低,夹杂物中的MnS含量越高;作为核心的氧化物夹杂的尺寸越小,形成的复合夹杂物的形状越规则,尺寸也越小。热力学计算结果表明,钢中Als含量主要影响了钢中氧化物夹杂的组成和AlN的析出温度及析出量。 Test as-cast grain-oriented silicon steel(/%:0.044 0.056C,3.12 3.32Si,0.08 0.11Mn,0.0020.008S,0.002 90.029 1 Als,0.006 20.010 9N) is melted by a 30 kg high frequency vacuum induction furnace.The research results by using field emission-scanning electron microscope/energy dispersive spectrometer(FE-SEM/EDS) show that in 0.002 9%Als steel the main oxide is SiO2,and there is independent laminable,rod-like and approximate ...
锌浴中钛对含硅钢Fe-Zn反应的抑制作用
选用Q235和Q345钢,在纯锌浴和含钛量分别为0.05%、0.10%、0.15%、0.20%(质量分数)的合金浴中浸镀0.5、1、3、5、8 min。利用扫描电子显微镜和能谱仪研究了钛对热浸镀锌组织和生长动力学的影响,并提出钛对含硅钢铁锌反应抑制作用的机理。结果表明:钛的加入缩短了Γ的孕育期,促进了合金层中δ的生长和ζ的消失,δ的生长依然受扩散控制,呈抛物线生长规律;Zn-0.05%Ti锌浴可以很好的抑制高硅钢的硅反应性;含硅钢热浸镀锌钛合金浴时,在锌浴中会形成锌铁钛三元T相,该相能吸收ζ晶界处富集的硅,从而抑制了铁锌反应。 Both Q235 and Q345 steels were immersed for 0.5 to 8 min in Zn bath with different amount of Ti,ranging from 0 to 0.20 mass%,for galvanization.The effect of Ti in Zn bath on microstructure and growth kinetics of hot-dip galvanizing coatings on the two steels were investigated by means of SEM and EDS analysis.Base on the experiment,the mechanism of Ti additions in controlling Fe-Zn reaction was proposed.The results show that addition of Ti in the zinc bath decreases the incubation time of Γ phase...
热卷箱在取向硅钢生产中的应用
热卷箱位于热连轧带钢生产线粗轧与精轧机之间,是热连轧生产中比较理想的中间保温设备。由于取向硅钢变形温度区间较窄,在生产中易出现边裂现象,同时中间坯的边部温度难于得到保证,因此一般不采用热卷箱设备生产,限制了传统热连轧生产线产品开发的品种。通过合理优化热卷箱控制工艺参数,解决了某厂传统热连轧生产线用热卷箱生产取向硅钢的边部质量问题,成功地生产出取向硅钢带。 The hot coil-box is an ideal heat retaining apparatus for hot rolling,lined between roughing mill and finishing mill. But oriented silicon steel has a narrow deformation temperature range,so that the edge crack easily occurs and it is difficult to insure the temperature of the intermediate blank. Therefore,the hot coil-box is rarely used in producing oriented silicon steel,which restricts the product development of the traditional hot rolling line. The article reasonable optimized process parame...
高温硅钢加热炉双蓄热燃烧技术的探讨
介绍了双蓄热燃烧技术的特点和高温硅钢加热炉的特点,探讨了双蓄热燃烧技术在高温硅钢加热炉中使用的技术难点,分析了双蓄热燃烧技术在高温硅钢加热炉上使用的可能性。 Introduced characteristics of double regenerative combustion technology and high temperature silicon steel reheating furnace,discussed technical difficulties for using double regenerative combustion technology,analyzed the possibility of double regenerative combustion technology applied to high temperature silicon steel reheating furnace.
热轧组织对无取向硅钢织构的影响
采用X射线衍射仪分析无取向硅钢冷轧织构和再结晶退火织构的演化,研究了热轧组织对无取向硅钢织构以及磁性能的影响。结果表明,具有均匀、粗大晶粒组织的热轧板,冷轧形成更多的剪切带,导致成品板形成高的高斯织构组分,并提高了{100}织构强度,降低了γ纤维织构,最终导致成品磁感应强度升高,铁损下降。 The texture evolution of non-oriented silicon steel during cold-rolling and recrystallization annealing was investigated by X-ray diffractometer.The effects of hot band microstructure on the texture and magnetic properties of non-oriented silicon steel were analyzed.The results show that more shear bands appear during cold rolling due to homogeneous coarse grain in hot band.So strong{110}<001> texture after recrystallization annealing forms.At the same time,the {100} texture components inc...
电脉冲对取向硅钢凝固组织的影响
对熔融态钢液进行处理,研究了电脉冲对于取向硅钢凝固组织的影响作用,利用正交试验法研究了脉冲电容、频率、处理时间和电压等脉冲参数的作用效果。结果表明:电脉冲对钢锭晶粒组织具有明显的细化作用,凝固组织的等轴晶比例大幅上升,影响等轴晶比例的最显著性因素为脉冲频率,最优正交试验参数为电容1 200μF,脉冲频率1 Hz,处理时间5 s,脉冲电压800 V。随着输入能量的增大等轴晶率先增大后减小,脉冲输入能量为某值时,等轴晶率最大,利用经典形核理论和热力学对这一现象进行了解释。 The influence of electric pulse on the solidification structure of oriented silicon steel was investigated by applying electric pulse in molten steel.The affection due to different electric pulse parameters such as electric capacity,frequency,applied time and voltage was studied by orthogonal design test.The result showed that solidification structure of oriented silicon steel could be improved by the electric pulse,and the equiaxed crystal ratio increased obviously.The most influential paramete...
晶界位向对硅钢立方/旋转立方取向双晶轧制取向变化的影响
晶界和{100}柱状晶在硅钢生产过程中对织构的遗传和演变有关键作用,因此本文利用晶体塑性有限元方法进行立方和旋转立方取向双晶在晶界不同位向时晶体取向演变的全场模拟。模拟显示,三种晶界位向下,晶界都具有诱发晶内产生S形状形变不均匀和缓解局部形变不均匀区取向转动的特点,立方和旋转立方取向双晶在带有剪切作用的轧制条件下都显示明显的取向稳定性。GB⊥RD(表示晶界垂直于轧向)晶界位向时,旋转立方取向晶粒优先在晶界中心位置发生取向转动,而立方取向则优先在远离晶界的端部发生取向转动。GB⊥TD(表示晶界垂直于横向)的晶界位向下,其晶界阻碍作用最小,双晶内产生的取向漫散度大,织构强度较低;除绕TD转动外,也具有复杂的绕RD、ND的取向转动。GB⊥ND(表示晶界垂直于法向)的晶界位向下,取向转动与GB⊥RD时相近,但有少量取向绕ND转动。 Grain boundaries and initial{100}columnar grains play a key role in the inheritance and evolution of texture in the production of electrical steels.In this paper,the crystal plasticity finite element method was used to simulate the grain orientation evolution of cube and rotated-cube oriented bicrystals when grain boundary was set to different orientations.It was shown that the grain boundary in three grain boundary orientations demonstrated the characteristics of inducing Sshape deformation inh...

