钢厂
双辊连铸法制备硅钢薄带的组织和性能
采用双辊连铸工艺制备了硅的质量分数分别为0.5%,1.0%,3.0%,4.5%的硅钢薄带,用光学显微镜观察其组织,并研究了后处理工艺对薄带组织和性能的影响。结果表明:硅含量为0.5%和1.0%的薄带适合采用一次冷轧+850~950℃退火的后处理工艺,而硅含量在3.0%以上的薄带适合采用二次冷轧+950℃退火的后处理工艺;硅含量为3.0%和4.5%的薄带在冷轧并950℃退火后,其磁性能最佳,铁芯损耗约为4.30 W·kg-1,磁感应强度约为1.68T。 Silicon steel thin strips with silicon content of 0.5wt%,1.0wt%,3.0wt%and 4.5wt%were prepared by twin-roll continuous casting process,and the microstructure of the strips were observed by means of optical microscopy,and on the basis,the effect of post-treatment process on microstructure and properties of the strips was studied.The results show that the post-treatment process of one-time cold rolling and annealing between 850—950℃was suitable for the strips with silicon content of 0.5wt%and 1.0wt...
EBSD技术在硅钢织构研究中的应用
运用电子背散射衍射(EBSD)和X射线衍射(XRD)技术对硅钢热轧板的织构在板厚方向的分布进行了研究,并分析了两种织构测量方法的特点。EBSD技术能直观给出板厚方向的微观织构,XRD能得到钢板的宏观统计织构信息,结合两种技术的分析,能更直观更精确的研究不同织构在板厚方向的分布。 The texture distribution along the thickness of the silicon steel has been investigated by electron backscatter diffraction(EBSD) and X-ray diffraction(XRD) technique.The characteristics of two technique of texture analysis have been investigated.Combined the two techniques,the texture distribution along the thickness of the silicon steel could be realized distinctly and accurately.
卷取工艺对新型冷轧无取向电工钢热轧带组织的影响
利用OM、SEM、TEM等实验方法研究了卷取工艺对一种新型含铜无取向电工钢晶粒度和析出相的影响。结果表明,该电工钢热轧带卷取后的晶粒尺寸为18~24μm,在卷取过程中,热轧带中有一定数量的第二相析出,经EDS能谱及选区电子衍射分析,这些析出相主要为AlN。随着卷取工艺的变化,该电工钢的晶粒度大小变化不明显,析出相的类型、尺寸大小不发生改变,体积分数发生一定的改变。 The effects of coiling process on grain size and precipitates of a new copper-bearing non-oriented electrical steel were investigated by OM,TEM and other experimental method.The results show that the grain size of hot-rolled bands after coiling is 18~24 μm.The second phases precipitate during coiling process.They are mainly AlN by EDS spectra and selected area electron diffraction.With the change of coiling process,the grain size of the electrical steel does not change significantly;the type and...
高牌号无取向电工钢RH深脱硫
以CaO-CaF2复合渣系为脱硫剂,在RH精炼过程采用真空投入法进行高牌号无取向电工钢深脱硫工业试验,采用KTH模型计算分析了RH炉渣成分对硫容量CS的影响。研究结果表明,炉渣成分控制在w((CaO))/w((SiO2))为5~7,w((CaO))/w((Al2O3))为1.5~1.8,w((Al2O3))为25%~30%,w((FeO+MnO))<5%,脱硫剂加入量为6~8kg/t时,钢中硫质量分数从平均0.003 1%降低到0.001 8%,最高脱硫率达到47.1%,平均脱硫率为41.7%。 The industrial trials on deep desulphurization of high grade non-oriented electrical steel were finished through using CaO-CaF2complex based fluxes in RH process.Using the KTH model,the effect of refining slag composition on the sulfide capacities was analyzed.The results show that the chemical composition of refining slag(mass fraction,%)is w((CaO/SiO2))between 5to 7,w((CaO))/w((Al2O3))beween 1.5to 1.8,w((Al2O3)) between 25%to 30%,w((FeO+MnO))less than 5%,and the desulphurizer addition level of...
高牌号无取向电工钢热轧板常化退火组织的EBSD分析
借助于EBSD对比研究了常化退火对高牌号无取向电工钢热轧组织和织构演变的影响,分析了常化退火对热轧板各厚度层织构的演变规律。结果表明,常化退火改善了热轧组织的均匀性,并弱化了热轧变形的γ纤维织构。升高常化退火温度,可增大热轧板的晶粒尺寸,提高{100}和{110}织构组分占有率,有利于提高无取向电工钢成品板的磁性能。 Effects of normalizing annealing on microstructure and texture of high-grade non-oriented electrical steel hot-rolled sheet were investigated by EBSD. Emphasis was put on the effects of normalizing annealing on texture evolution in the sheet thickness. The results show that the hot-rolled microstructure homogeneity is improved and the γ-fiber texture is weakened by normalizing annealing treatment. The grain size of hot-rolled sheet and intensity of the {100} and {110} favorable texture can be in...
冷轧产线硅钢激光高速切边实验研究
为了解决目前冷轧产线硅钢现有切边技术存在的微裂纹、应力、毛刺和边浪等问题,采用光纤激光器进行了高速切割实验,对激光功率、切割速度、激光模式等影响因素进行了分析,同时对高速切割时的切割前沿形状进行了研究。结果表明,切割最高速度随着功率的增加而增加;随着离焦量的增加,切割质量下降,挂渣增多,切缝宽度增加,切割深度变浅;基模激光器能量密度更高,所以薄板切割时的切割速度高于多模激光器;切割前沿随着切割速度的增加会变得平缓,速度足够大时,切割前沿甚至接近与切割方向平行,此时切缝下部存在挂渣现象。 In order to solve the problems such as micro crack,stress,burr,edge waves and so on,existing in cold rolling production line of silicon steel side cutting,experimentsof high speed laser cutting using fiber laser were carried out.Laser power,cutting speed,laser mode and other factors were analyzed,at the same time,cutting front geometries were studied.The results show that the maximum speed increases with power.And the increases of defocus result in poor quality,wider kerf and shallowerkerf.Energ...
大压下率冷轧无取向硅钢织构演变及性能
组织和织构是影响无取向硅钢性能的重要因素。为改善产品性能,研究了冷轧压下率(71.7%~87.0%)对高牌号无取向硅钢组织、织构、磁性能和力学性能的影响。结果表明,随冷轧压下率的增加,退火晶粒平均尺寸先减小后增大;高斯和立方织构强度减弱,γ纤维织构增强,α纤维织构转变为较强的α*({h, 1, 1}〈1/h, 1, 2〉)织构,并随冷轧压下率的增加而增强,同时其峰值逐渐向{111}面移动;工频铁损P1.5/50、高频铁损P1.0/400和磁极化强度J5000同时降低,屈服强度变化不大,表面硬度逐渐增加。当冷轧压下率由84.7%增至87.0%、厚度减至0.30 mm时,高频铁损降幅是工频铁损的11倍,表面硬度增幅变大。以上研究成果对硅钢减薄后织构及组织的优化提供了很好的指导。 Microstructure and texture are critical factors on non-oriented silicon steel properties. In order to improve product properties, this paper studied the effect of cold rolling reduction rate(71.7%-87.0%) on microstructure, texture, magnetic properties and mechanical properties of high-grade non-oriented silicon steel. The results show that with the increase of cold rolling reduction rate, the average size of annealing grain decreases first and then increases. The intensity of Goss and λ fiber te...
在动态热处理条件下对取向电工钢二次再结晶的研究
对应用动态加热进行短时温度退火的取向电工钢进行了二次再结晶研究。所进行研究的实验用取向电工钢是经过终冷轧和后续罩式退火后的一条工业化生产线生产的。研究结果表明,运用短时热处理条件可引起研究钢完全的异常晶粒长大。在实验室处理的材料的织构和金相组织与工业化生产的经过终退火而获得的相同的取向电工钢类似。但是,在实验室处理的取向电工钢的二次再结晶的矩阵中可观测到\"寄生\"晶粒。从磁性观点看,这些\"寄生\"晶粒含有不理想的{111}取向织构。 The present study was made to investigate secondary recrystallization in grain-oriented steels annealed at short time temperature exposures with application of dynamical heating.The investigated GO(Grain Oriented) steels for experiments were taken from one industrial line after final cold rolling reduction and subsequent box annealing.It was shown that application of short time heat treatment conditions could lead to complete abnormal grain growth in the investigated GO steel.The texture and mic...
常化和退火工艺对冷轧无取向硅钢高频磁性能和强度的影响
冷轧无取向硅钢(/%:0.003C,2.35Si,0.22Mn,0.011P,0.002S,0.36A1,0.003 0N)经890℃或940℃3 min常化的2.3 mm热轧板冷轧成0.35 mm薄板。研究了常化温度和800920℃3 min退火对该钢高频(400Hz)磁性能和抗拉强度的影响。结果表明,830920℃退火时高频铁损P10/400值最低,随退火温度增加,晶粒尺寸增大,钢的抗拉强度降低;该钢的最佳热处理工艺为常化温度940℃,退火温度830℃,其抗拉强度Rm、高频铁损P10/400和磁感应强度J50分别为565 MPa,21.5 W/kg和1.69 T。 The cold-rolled non-oriented silicon steel(/%:0.003C,2.35Si,0.22Mn,0.011P,0.002S,0.36A1,0.003 0N) is cold-rolled to 0.35 mm sheet from 2.3 mm hot-rolled plate normalized at 890 ℃ or 940℃ for 3 min.The effect of normalizing temperature and annealing process at 800 920 °C for 3 min on high frequency(400 Hz) magnetic properties and tensile strength of the steel has been tested and studied.Results show that with annealing at 830 920 ℃the high frequency iron loss value P10...
无取向电工钢织构的演变及其沿带钢宽度方向上的差异
采用EBSD检测技术,分析了50W800无取向电工钢在重要生产工序间织构的演变以及织构沿带钢宽度方向上的差异性。结果表明:热轧板织构沿带钢宽度方向上的差异性主要体现在表层织构。带钢边部表层织构主要由旋转立方织构、α纤维织构以及少量的γ纤维织构组成,带钢宽度1/4处的表层织构主要存在高斯织构,带钢宽度1/2处的表层织构主要为(110)面织构以及少量的铜型织构。各处的带钢宽度1/4处和1/2处的织构类型基本一致,都以α纤维织构和旋转立方织构为主。冷轧后,各处的表层织构类型差异较小,均为γ纤维织构和α纤维织构。由板宽边部至中心处织构强度值逐渐降低。退火后,各处织构的组分基本一致,为较强的γ纤维织构和较弱的(100)面织构。各处织构强度值差异较小,变化趋势与冷轧板一致。 The texture of non-oriented electrical steel 50W800 was detected by EBSD technique.The evolution of the texture between important processes and the difference of texture along the width direction of strip were analyzed.The result shows that the difference along the width direction of strip of texture at the surface of hot rolled plate is most obvious.The texture at the surface of strip edge is primarily made of rotating cube texture,αfiber texture and weakγfiber texture.Goss texture is mainly co...
氢氧化镁煅烧制备硅钢级氧化镁的研究
以青海盐湖氯化镁为初级原料,采用喷雾热解法制备原料氧化镁。原料氧化镁通过水化制备氢氧化镁。将氢氧化镁过滤、洗涤、烘干、粉碎、煅烧,制备硅钢级氧化镁。本文重点考察煅烧温度、煅烧时间、料层厚度等因素对氧化镁水化率的影响,采用均匀实验设计和DPS数据处理,确定最优煅烧实验条件为:煅烧温度1250℃,煅烧保温时间4小时,料层厚度0.5cm。在此条件下得到的硅钢级氧化镁完全满足硅钢及氧化镁的行业标准。 The magnesium oxide is prepared by Spray pyrolysis process,which magnesium chloride from Qinghai Salt Lake is used as primary raw material,and hydrated to magnesium hydroxide,then obtained silicon steel magnesia through filtering,washing,drying,crushing and calcinations.In this paper,influences of some factors on magnesia hydration rate are studied,such as calcination temperature,calcination time and material thickness.After average experimental design and DPS data processing,optimal calcination...

