硅钢资料

通过后天抑制剂获得法制备了取向硅钢,对渗氮前后和高温退火升温阶段析出物的析出和转化规律进行了研究。研究结果表明,渗氮前脱碳退火态基体中存在少量的粗大AlN颗粒和细小AlN颗粒,渗氮处理后新析出大量的Si3N4析出物,高温退火升温阶段Si3N4将转化为(Al,Si)N,随着温度的继续升高(Al,Si)N颗粒将发生粗化,(Al,Si)N是后天抑制剂获得法制备取向硅钢的主要抑制剂。 Grain-oriented silicon steels were produced by acquired inhibitor method.The rule of precipitate transformation was studied after nitriding treatment and high-temperature finishing annealing.The results show that a small amount of large AlN and fine AlN are found in matrix before nitriding treatment,and a large amount of Si3N4 is precipitated in matrix after nitriding treatment.During the temperature rising period of high-temperature finishing annealing,Si3N4 would transform into(Al,Si)N,and(Al,... 

无氧化炉具有加热效率高、投资与运营成本低、作业率高、表面质量及板型良好、NOx排放相对低等优势,在硅钢热处理领域应用前景广泛。本文阐述了确定无氧化炉(NOF)加热能力详细过程,涵盖炉温、炉断面尺寸、炉长、热平衡结算、加热能力计算等,为今后无氧化炉(NOF)在硅钢热处理应用时的设计提供了借鉴,同时也为今后明火直接加热的工业炉设计提供了参考。 Non-oxidation furnace has the advantage s of high heating efficiency, low investment and operation cost, high operation rate, good surface quality and plate shape, and relatively low NOxemission,and it still has wide application prospect in the field of silicon steel heat treatment. The detailed process of determining the heating capacity of a non-oxidizing furnace(NOF) is described, covering furnace temperature, furnace section size, furnace length, heat balance settlement, heating capacity cal... 

对商用50W330型无取向硅钢成品在930℃下保温2 h固溶并以不同方式冷却处理,利用磁性检测仪检测分析了处理前后的磁感和铁损变化,应用光学显微镜、扫描电子显微镜、X射线衍射仪观测分析了显微组织结构的演变。考察了平均晶粒尺寸、织构组分比及第二相粒子状态对磁性能的影响规律,结果表明:固溶处理前后平均晶粒尺寸的变化对硅钢磁性能的影响非常显著;当平均晶粒尺寸相差不大时,织构组分比[Goss+{100}]/{111}越大,磁感会越高;固溶处理会将细小弥散的第二相粒子重新回溶到基体中,减小了其对磁畴壁的钉扎作用,铁损随之下降。 The commercial 50W330 non-oriented silicon steel samples were heat treated at 930℃ for 2 h and cooled in different ways,then the iron loss and the magnetic induction of the samples before and after solution treatment were measured with a magnetic detector.The evolution of microstructural texture was analyzed by optical microscopy,scanning electron microscopy and X-ray diffractometry.The effects of average grain size,texture composition ratio and the second phase particles on the magnetic propert... 

通过微观组织表征、高温拉伸和断口形貌分析,研究了钇(Y)元素对6.5%Si无取向硅钢组织、高温拉伸及断裂机制的影响。研究结果表明,添加Y元素可以在钢液中形成YS和YP的复合析出。YS和YP可以充当异质形核基底,提高形核率,细化凝固组织。热轧组织不均匀,由表层至芯部分别形成等轴晶、等轴晶/拉长晶和拉长晶的混合组织。退火后,热轧变形组织转变为等轴晶,含Y实验钢的退火组织得到明显细化。500℃时效处理后,含Y实验钢具备较低的有序度,300℃的拉伸断口呈现韧性断裂特征,断后伸长率达到20.2%。相反,无Y实验钢发生脆性断裂,断后伸长率仅为2.1%。研究结果证实,Y元素可以通过组织细化和降低有序度提高6.5%Si无取向硅钢的中温塑性。 The effects of yttrium(Y)on microstructure,elevated-temperature tensile properties and fracture mechanism of 6.5% Si non-oriented electrical steel were investigated by means of microstructure characterization,high-temperature tensile test and fracture analysis.The results showed that the doping of Y introduced composite Y-rich precipitates(YS/YP)in the melt.YS and YP precipitates were qualified for heterogeneous nucleation agents,which thus raised the nucleation rate and refined the solidificati... 

取向硅钢利用析出物作为抑制剂,抑制初次再结晶晶粒的长大,抑制剂是取向硅钢发生二次再结晶的基本条件之一。文中通过低温板坯加热技术制备取向硅钢,采用透射电镜(TEM)观察并研究了高温退火阶段抑制剂的演化过程。结果表明,渗氮后形成的非晶态Si3N4析出物不稳定,在700～750℃退火升温阶段转化为(Al,Si)N;(Al,Si)N颗粒在800℃发生团聚,随后长大并粗化;(Al,Si)N是低温取向硅钢主要抑制剂,随退火温度的升高,(Al,Si)N抑制力大幅下降。 Precipitates as inhibitor are used to inhibit the grain growth of primary recrystallization in grain-oriented silicon steel,and inhibitor is one of the basic conditions for occurring of secondary recrystallization.The grain-oriented silicon steel was produced by low temperature slab heating and nitriding technique.The evolution of inhibitor was observed by transmission electron microscopy.The results show that Si3N4 particles are precipitated after nitriding,and Si3N4 particles are amorphous and... 

主要研究了氧化锌对以Al(H2PO4)3为基料的无铬无取向硅钢绝缘涂层各项性能的影响.用盐雾实验和动电位极化研究了不同氧化锌含量对硅钢绝缘涂层的耐蚀性和电化学行为的影响.采用SEM和体视显微镜对涂层的表面形貌和附着性能进行研究.结果表明,氧化锌含量为4.0%时,氧化锌能完全中和涂层表面的游离磷酸,涂层的耐蚀性和附着性最好;氧化锌含量过少或过多时,涂层的耐蚀性和附着性都较差. This paper studies the influence of zinc oxide on the performance of chromium-free non-oriented silicon steel insulating coating which based on aluminum dihydrogen phosphate.Salt spray experiment and potentiodynamic polarization were used to study the influence of zinc oxide content on the corrosion resistance and electrochemical behavior of the insulation coating of silicon steel.The surface morphology and adhesion of coating were tested by SEM and stereo microscope.The results show that when t... 

对w(Si)=3%无取向硅钢进行表面机械研磨处理(SMAT)和异步轧制(CSR),获得表面纳米结构,再进行550～650℃、4 h固体粉末渗硅处理,用透射电镜(TEM)、扫描电镜(SEM)和X射线衍射仪(XRD)研究表层组织演变。结果表明:经过SMAT后,w(Si)=3%无取向硅钢表面形成了等轴状、取向呈随机分布的、晶粒尺寸为10 nm的纳米晶组织;异步轧制后,表面纳米晶组织保持不变;550～650℃、4 h渗硅处理后,SMAT+CSR样品表面形成化合物层,其厚度随着温度的升高由17μm增加到52μm;化合物层由Fe3Si和FeSi相组成. Nanostructured surface layer was fabricated on a 3%(mass fraction) non-grain oriented silicon steel by means of surface mechanical attrition treatment(SMAT) and cross-shear rolling(CSR),and then a solid powder siliconizing treatment was carried out for the SMAT+CSR sample at 550~650 ℃ for 4 h.The microstructural evolution was examined by using transmission electron microscopy(TEM),scanning electron microscopy(SEM) and X-ray diffraction(XRD).Experimental results show that: equiaxed nanocrystallin... 

采用中、厚板坯生产技术对取向硅钢进行了研制和开发,对热轧及后工序样品进行了金相组织观察和EBSD分析,探讨了两种组织及织构的差异性,研究结果表明:除高温退火样品外,中板坯生产的取向硅钢各工序样品平均晶粒尺寸大;厚板坯生产的取向硅钢热轧和常化样品亚表层Goss织构强;中板坯和厚板坯的脱碳退火板织构没有明显区别。中板坯生产的取向硅钢成本低,产品磁性能和质量与厚板坯相当。 Grain oriented silicon steel was researched and developed by medium thickness slab and thick slab.Microstructures observation and EBSD analysis to the samples of hot rolling and following processes were carried out,respectively.The differences between the two kinds of microstructures and textures were discussed.The results show that the average grain sizes of every process samples are larger except that of high temperature annealing samples of grain oriented silicon steel produced by medium thic... 

硅钢高温退火环形炉炉壳制作与安装精度要求较高,施工时通过对壳体原材料矫正、炉壳板拼焊、下料切割、型钢骨架组装及焊接、骨架及炉壳板矫正、骨架与炉壳板组装及焊接、炉壳矫正、零配件装置、定位钻孔、报验检查、出厂、内侧板安装、外侧板安装、顶板安装等环节的工艺技术控制,能保质高效地完成硅钢高温退火环形炉炉壳制作与安装,为以后同类工程的施工提供可借鉴经验。 The required precision of manufacture and installation technique of the silicon steel high temperature annealing annular-furnace shell is high.During construction , manufacture and installation of the silicon steel high temperature annealing annular-furnace shell could be finished high efficiently through correcting the raw materials of shell , furnace shell plate welding , material cutting , steel frame assembly and welding , skeleton and shell plate correction , skeleton and furnace shell asse... 

【机构】 中国金属学会电工钢分会； ...

森吉米尔二十辊轧机是冷轧电工钢的主要机型,具有整体刚度大,辊径小,轧制道次压下量大,产品精度高等特点,简要介绍了近年来冷轧电工钢森吉米尔二十辊轧机领域进展,在轧机结构、厚度自动控制、板形自动控制等方面的技术及研究。 20-h Sendzmir reversible mill is the main type of cold rolled electrical steel which has the characteristic of high integral stiffness,small roller diameter,high pass reduction and high product quality.In this paper,the recent progress of frame structure,automatic gauge control,automatic flatness control of Sendzmir mill is introduced. 

研究了硼酸对以Al(H2PO4)3为基料的无铬无取向硅钢绝缘涂层各项性能的影响。用盐雾实验、动电位极化及交流阻抗等试验手段研究了不同硼酸含量对硅钢绝缘涂层的耐蚀性和电化学行为的影响,同时采用SEM对涂层的表面形貌进行了研究。结果表明,硼酸含量为9.7%时,涂层的耐盐雾性及电化学性能最好;硼酸含量过少或过多时,涂层的耐蚀性和电化学性能都较差。 Influence of boric acid on the performance of chromium-free non-oriented silicon steel insulating coating based on aluminum dihydrogen phosphate was investigated.Salt spray experiment,potentiodynamic polarization and electrochemical impedance spectroscopy were used to study the influence of boric acid content on the corrosion resistance and electrochemical behavior of the insulation coating of silicon steel.Surface morphologies of the coatings were tested by SEM.Result shows that when the boric ...