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低温高磁感取向硅钢高温退火过程织构及析出物的演变行为

【作者】
樊立峰;
项利;
唐广波;
仇圣桃;

【Author】
FAN Li-feng;XIANG Li;TANG Guang-bo;QIU Sheng-tao;State Key Laboratory of Advanced Steel Processing and Products, Central Iron and Steel Research Institute;National Engineering Research Center of Continuous Casting Technology, Central Iron and Steel Research Institute;Research Institute of Special Steel,Central Iron and Steel Research Institute;

【机构】
先进钢铁流程及材料国家重点实验室;
钢铁研究总院连铸技术国家工程研究中心;
钢铁研究总院特殊钢研究所;

【摘要】 对低温法生产的以AlN为主抑制剂的Hi-B取向硅钢高温退火过程进行了中断实验,借助EBSD及TEM技术对高温退火连续升温过程中织构与析出物的演变进行了研究。实验结果表明,800℃时ODF图出现高斯织构组分,但强度很弱,高斯晶粒偏离角在10°以上;950~1 000℃时高斯晶粒异常长大,偏离角3~6°;高温退火过程析出物主要有球形、规则立方形及不规则多面体形3种形貌,由于渗N的影响,Zener因子先增大再减小,并且析出物在高斯晶界前沿优先粗化。 

【Abstract】 The annealing process at high temperature of Hi-B silicon steel using low slab reheat temperature and with AlN as the inhibitor has been studied by interrupting test,and the evolution of texture and precipitates during continuous heating-up in the annealing process at high temperature was analyzed by EBSD and TEM. The results showed that Goss texture appears in ODF at 800 ℃,but the intensity of Goss texture was very weak and the deviation angle was more than10°. Goss grains grow abnormally durin… 

【关键词】 高磁感取向硅钢;
高斯织构;
二次再结晶;
析出物;
Zener因子;

【Key words】 Hi-B steel;
Goss texture;
secondary recrystallization;
precipitate;
Zener factor;
【基金】 国家自然科学基金资助项目(50934009)

原文发表于《功能材料》2013年第23期

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