硅钢资料

本发明涉及取向硅钢制造技术领域，公开了一种快速判断取向硅钢初次再结晶晶粒直径的方法，包括如下步骤：选取取向硅钢热轧来料，进行生产，对产出的钢板在同部位各取若干个拉伸试样，加工拉伸和分析，取得屈服强度，在拉伸试样部位两侧连续制取金相试样，计算对应拉伸试样的平均晶粒直径D，将性能数据和平均晶粒直径进行统计分析，建立屈服强度与晶粒直径的对应关系，实际生产时，在产出的钢板上取判断试样，取得判断试样的屈服强度，进而取得判断试样的晶粒直径。本发明快速判断取向硅钢初次再结晶晶粒直径的方法，通过机械性能检验，来间接指示初次晶粒的大小，检测速度快，评价更准确。

本发明实施例公开了一种硅钢稀酸废水零排放处理方法和系统，所述方法包括：获得稀酸废水；对所述稀酸废水中的含硅固体杂质进行分离与回收，以获得稀酸废水净化液和含硅脱水泥饼；将所述稀酸废水净化液进行两级电吸附分盐处理，利用直流电场将稀酸废水中氯化亚铁组份浓缩分离，以获得分盐浓水和分盐淡水；将所述分盐浓水与酸再生工艺耦合，以获得再生盐酸；将所述分盐淡水调质再生处理，以获得铁系絮凝剂和再生工业净化水。所述硅钢稀酸废水零排放处理方法和系统，可以较低成本和能耗实现硅钢稀酸性废水全回用，真正实现废水零排放；可回收稀酸废水中的铁素和稀盐酸，不产生固体废物，可彻底实现废弃物资源化利用。

采用X-射线衍射分析技术测定了取向硅钢热轧板在不同压下率下不同厚度处的织构。结果表明,在压下率低于80%的情况下,几乎所有试样的不同厚度处的织构均为旋转立方织构类型{100}<011>,但不同压下率、不同厚度处的织构强度存在很大差异;在压下率大于80%的情况下,不同试样的不同厚度处的织构类型发生了变化,其织构类型为旋转立方织构或高斯织构{011}<100>,且当织构类型为旋转立方织构时,织构强度存在很大差异,而当织构类型为高斯织构时,织构强度差异相对较小。 The texture of the grain oriented silicon steel hot rolled plate at different compressibility has been measured.The experimental results have shown that the texture of all samples at different thickness is {100}<011> when the compressibility is below 80%,and its intensity at different compressibility and thickness is difference.The texture of all samples at different thickness is variable when the compressibility is above 80%,it is {100}<011> or {011}<100>,and the intensity of ... 

本发明公开了一种适用于无取向硅钢极薄带表面涂覆的涂液，它由水溶性丙烯树脂、成膜助剂、耐盐雾助剂、流平剂、纳米氢氧化锆、消泡剂、水按质量比100:(2～8):(1～3):(1～5):(0～1):(0.1～0.5):(70～130)组成。将该涂液在无取向硅钢极薄带表面可表现出良好的涂覆性，经烘烤固化后形成的绝缘涂层表面透明光滑，附着性和绝缘性能优良，可有效提升无取向硅钢极薄带的综合性能，适合推广应用。

硅钢工业退火炉温度控制具有强耦合、纯滞后、多扰动等特点,它的控制方法代表着一类非线性系统控制的解决方法。以硅钢工业退火炉温度为控制对象,在双交叉限幅控制的基础上引入了智能学习系统,形成了基于智能学习系统的双交叉限幅控制方法来解决此类非线性系统的控制问题,并通过模块化的编程来实现其功能。结果表明:与传统的PID控制相比,该控制方法的控制精度、抗扰性等控制指标有明显提高,是解决此类非线性控制的一种有效方法。 The temperature control of silicon steel industrial annealing furnace has the features of strong coupling,pure lag,multidisturbance. The control method represents the solution of a class of nonlinear control systems. The control object is the temperature control of silicon steel industrial an-nealing furnace, the intelligent learning system based on Double Across Limit Control is introducedand used to solve control problem of this kind of nonlinear system, and the module programming isused to re... 

某厂对电工钢的轧制策略进行了优化，粗轧道次由“1+5”改为“1+3”。在优化后的生产过程中，每次变换钢种，烫辊材就会出现窄尺现象，而紧随其后的电工钢板则出现超宽现象。文中针对该问题，介绍了宽度设定模型和宽度自适应模型的原理，阐述了该问题出现的原因及解决方案，并通过对宽度自适应模型的应用研究及优化攻关，有效地解决了问题，大幅提升了实物质量，降低了宽度封锁率。 The rolling strategy of electrical steel was optimized in a factory,and the rough rolling pass was changed from “1+5”to“1+3”.Subsequently,the following problems were occurred in the production process:when the steel grade changed,the roasting roller steel before the electrical steel appeared the narrow width phenomenon,and then the electrical steel appeared the ultra-wide phenomenon.This paper introduced the principle of width setting model and width adaptive model,and expounded the causes and s... 

【作者】 谌剑； ...

本发明公开了一种高磁感取向硅钢高效脱碳退火工艺，主要工艺流程为：炼钢连铸→热轧→酸洗常化→冷轧→脱碳和初次再结晶退火→渗氮处理(低温Hi‑B)→涂覆氧化镁隔离剂→高温退火→拉伸平整退火→涂覆绝缘涂层→精整，低温HiB不同于高温Hi‑B的工艺流程主要是在脱碳退火后增加了渗氮段。本发明在保证产品实物质量不低于现有水平(国内领先水平)的前提下，使Hi‑B钢退火效率达到世界领先，制造成本大幅降低。

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

目的提高硅钢的磁性能。方法采用多弧离子镀技术,在普通取向硅钢薄板两面沉积高硅FeSi合金层制得高硅梯度硅钢,并进行热处理,观察其显微组织,测量磁性能。结果退火态高硅梯度硅钢表面的高硅FeSi合金层与基底结合紧密,均匀致密。高硅梯度硅钢中硅含量呈梯度分布,最表层硅质量分数为11.0%,随着深度增加,硅含量逐渐降低,在距表面20μm处硅质量分数仍能达到6.5%。沉积态高硅梯度硅钢的电阻率ρ、低频铁损P10/50、高频铁损P10/1k及磁感应强度B8分别为68.6μΩ·cm,0.82W/kg,83.3 W/kg和1.73 T,退火后分别为63.1μΩ·cm,0.44 W/kg,54.38 W/kg和1.89 T。结论由于表层高硅FeSi合金层的存在,梯度高硅钢的低频磁学性能良好,但高频损耗需进一步改善。 Objective To improve the magnetic properties of silicon steel. Methods FeSi alloy coatings with high-silicon content were deposited on the surface of common grain-oriented silicon steel by cathodic arc plasma evaporation,and then a kind of high silicon gradient steel was prepared. The morphologies,content and magnetic properties of the samples were tested. Results FeSi alloy coatings were featured with compact microstructures and excellent adhesive quality with the substrates. The silicon conten... 

研究了铝和铬元素在无取向电工钢晶粒长大过程中对织构及晶界变化的影响规律。试验结果表明:电工钢在晶粒长大过程中的主要织构组分均为{111}<112>。在晶粒生长期间,不加铝的1号试样中,{111}<112>、{111}<110>织构组分强化,而{100}<001>织构组分弱化;与1号试样相比,在加入0.2%的铝(质量分数,下同)的2号试样中,{111}<112>、{111}<110>织构组分强化(增加)的速率下降,{100}<001>织构组分变化不明显,甚至稍有增加。在含铝的试样中再加入0.3 5%的铬之后(3号试样),{111}<112>{、111}<110>和{100}<001>织构组分的变化规律与1号试样相似,但当电工钢中加入0.72%的铬之后(4号试样),上述3种织构组分的变化规律与2号试样相似。对于在晶粒生长期间持续变化的3种织构组分而言,1号试样的{1 1 1}<112>和{111}<110>织构组分的高(低)取向差角度晶界频率下降(... The effect rule of Aluminm and Chromium on texture and grain boundary transformation in the nonoriented electrical steel during grain growth was investigated.The experimental result shows that the main texture component is {111}<112> in the electrical steel.The {111}<112> and {111}<110> components in specimen 1 without Alumium were strengthened during grain growth whereas {100}<001> component was weakened.But the growth rate of {111}<112> and {111}<110> compon... 

本发明涉及含Cu无取向硅钢的生产方法，转炉炼钢，真空处理过后连铸成坯；铸坯化学成分：1.0≤Si/Cu≤3.0,3.0≤Si+Cu≤5.5％，S≤0.0015％，(Mn+Cu)/S≥3000，其他为Fe,Als,P以及不可避免的杂质元素；对铸坯进行粗轧；粗轧后的中间坯采用热卷机进行强制卷取，开卷后中间坯进入保温箱，控制保温箱内冷却速度≤5℃/s；进入保温箱的中间坯温度T1满足：1000‑(Si+Cu)×103≤T1≤1100‑(Si+Cu)×103；高压除鳞，精轧，层流冷却，卷取；连续酸洗；冷轧到目标厚度，成品退火，涂层；成品卷进行时效处理。成品卷具有较低的中高频铁损，高磁感和高屈服强度。