钢厂
210 t BOF-RH-CC炼钢过程无取向硅钢XG800WR洁净度的试验研究
两炉次无取向硅钢XG800WR(/%:0.003~0.004C、0.71~0.75Si、0.32~0.33Mn、0.004~0.007S、0.016P)的炼钢流程为铁水预处理(KR)-210 t顶底复吹转炉-钢包吹氩-RH脱碳精炼-230mm×1220 mm板坯连铸。53 t中间包钢水过热度为25~30℃,钢包到中间包采用长水口全程吹氩保护浇铸,中间包至结晶器采用浸入式水口浇铸。结果表明,在RH、中间包、结晶器过程中钢中总氧以及夹杂物数量和尺寸均明显降低;但在钢包到中间包过程T[O]、[N]和钢中夹杂物数量增加,说明长水口浇铸过程存在二次氧化。连铸坯中T[O]、[N]平均他分别为11×10-6和30×10-6,显微夹杂物数量平均为4个/mm2。铸坯中的显微夹杂物主要为3~5μm的AlN,同时存在少量的MnS、Al2O3·AlN和Al2O3·MgO·MnS。 The steelmaking flow sheet for two heats non-oriented silicon steel XG800WR(/%:0.003~0.004C. 0.71~0.75Si,0.32~0.33Mn,0.004~0.007S,0.016P) is hot metal pretreatment(KR)-210 t top and bottom combined blown converter-ladle argon blowing-RH decarburization refining-230 mm×1 220 mm slab casting.The superheating extent of liquid in 53 t tundish is 25~30℃,whole casting is shielded by blowing argon with long nozzle from ladle to tundish and the submerged nozzle is adopted in casting from tundish to mold...
优化脱氧工艺改善低碳低硅钢钢水可浇性
介绍了重庆钢铁股份有限公司炼钢厂生产低碳低硅钢的脱氧工艺,对连铸过程中水口结瘤的原因进行分析,并提出了优化措施。生产实践表明:钢水中的活性氧质量分数控制在10×10-6~30×10-6时,单中包浇铸炉数由6~7炉提高到11~12炉,同时能保证连铸顺行和减少铸坯气孔。 The deoxidation process of low-carbon and low-silicon steel in steel plant of Chongqing Steel was introduced.The nuzzle clogging was analyzed and some measures were put forward.Production experiments showed that when the active oxygen was controlled between 10×10-6~30×10-6,the amount of furnaces would rise from 6~7 to 11~12,which will make the casting process work well and reduce casting holes.
火花源原子发射光谱法测定取向硅钢中碳硅锰磷硫
通过试验确定氩气分析流量为3.5L/min,静态流量为0.75L/min,冲洗时间为3s,预燃时间为12s,积分时间为5s的激发条件,采用火花源原子发射光谱法测定取向硅钢中碳、硅、锰、磷、硫。分别采用铣床铣样、砂轮磨样两种制样方式进行了精密度考察,发现制样方式对结果影响不大;讨论了取向硅钢样品中碳、硅、锰、磷、硫测定时可能存在的共存元素干扰,发现硅对锰元素的干扰不可忽略,采用干扰系数法进行了校正,据此拟合得到各元素校准曲线的相关系数均在0.999 0以上。精密度考察结果表明,碳、硅、锰、磷、硫的相对标准偏差(n=10)在0.71%~9.4%之间。对两块取向硅钢生产样品进行分析,并与钢铁研究总院进行比对分析,结果一致,且偏差均在允许范围内。 Carbon,silicon,manganese,phosphorus and sulfur in oriented silicon steel were determined by spark source atomic emission spectrometry.The selected excitation conditions were as follows:the analytical flow rate of argon was 3.5L/min,the static flow rate was 0.75L/min,the flush time was3s,the precombustion time was 12sand the integration time was 5s.Two sample preparation methods,including milling machine and grinding wheel,were investigated.The precision test results showed that,the determination...
无取向电工钢织构的演变及其沿带钢宽度方向上的差异
采用EBSD检测技术,分析了50W800无取向电工钢在重要生产工序间织构的演变以及织构沿带钢宽度方向上的差异性。结果表明:热轧板织构沿带钢宽度方向上的差异性主要体现在表层织构。带钢边部表层织构主要由旋转立方织构、α纤维织构以及少量的γ纤维织构组成,带钢宽度1/4处的表层织构主要存在高斯织构,带钢宽度1/2处的表层织构主要为(110)面织构以及少量的铜型织构。各处的带钢宽度1/4处和1/2处的织构类型基本一致,都以α纤维织构和旋转立方织构为主。冷轧后,各处的表层织构类型差异较小,均为γ纤维织构和α纤维织构。由板宽边部至中心处织构强度值逐渐降低。退火后,各处织构的组分基本一致,为较强的γ纤维织构和较弱的(100)面织构。各处织构强度值差异较小,变化趋势与冷轧板一致。 The texture of non-oriented electrical steel 50W800 was detected by EBSD technique.The evolution of the texture between important processes and the difference of texture along the width direction of strip were analyzed.The result shows that the difference along the width direction of strip of texture at the surface of hot rolled plate is most obvious.The texture at the surface of strip edge is primarily made of rotating cube texture,αfiber texture and weakγfiber texture.Goss texture is mainly co...
低温取向硅钢热轧态组织及织构的研究
利用热模拟试验机、光学显微镜和X射线衍射仪对Fe-3.2%Si低温取向硅钢热轧工艺参数对组织及织构的影响进行了研究。结果表明,Fe-3.2%Si硅钢在1110℃粗轧、880℃终轧,轧后以10℃/s的速度冷却到550℃卷取,然后空冷到室温,热轧硅钢板沿板厚方向的显微组织不均匀性显著,对后续发展完善的二次再结晶有重要作用。无论是热轧板,常化板还是冷轧板,它们的织构集中分布在γ取向线上,γ取向线的织构除取向密度不同外,织构种类是一致的,这说明γ取向线上织构是有继承性的。从热轧到常化,织构取向密度显著减小,经二次冷轧后,织构密度又显著升高,可见,轧制变形有助于织构的形成并使织构强度升高。 The influence of hot-rolled process parameters on the microstructure and texture of Fe-3.2%Si low temperature hot rolled grain-oriented silicon steel were researched by hot simulation experiment machine,light microscope and X-ray diffractometer.The results show that,Fe-3.2%Si silicon steel is rolled by the technology with a temperature of rough rolling of1110℃,finish rolling of 880℃,coiling with the speed of 10℃ /s,and then cooled to room temperature with air.The microstructure of hot-rolled sil...
卷取工艺对新型冷轧无取向电工钢热轧带组织的影响
利用OM、SEM、TEM等实验方法研究了卷取工艺对一种新型含铜无取向电工钢晶粒度和析出相的影响。结果表明,该电工钢热轧带卷取后的晶粒尺寸为18~24μm,在卷取过程中,热轧带中有一定数量的第二相析出,经EDS能谱及选区电子衍射分析,这些析出相主要为AlN。随着卷取工艺的变化,该电工钢的晶粒度大小变化不明显,析出相的类型、尺寸大小不发生改变,体积分数发生一定的改变。 The effects of coiling process on grain size and precipitates of a new copper-bearing non-oriented electrical steel were investigated by OM,TEM and other experimental method.The results show that the grain size of hot-rolled bands after coiling is 18~24 μm.The second phases precipitate during coiling process.They are mainly AlN by EDS spectra and selected area electron diffraction.With the change of coiling process,the grain size of the electrical steel does not change significantly;the type and...
制备硅钢级氧化镁前驱体的原料水化研究
以青海盐湖水氯镁石为初级原料,采用喷雾热解法制备原料氧化镁,原料氧化镁通过水化制备硅钢级氧化镁前驱体氢氧化镁。原料氧化镁水化实验中对水化剂、水化温度、水化时间、液固比、搅拌速度及陈化时间对水化率、过滤速度和纯度的影响进行系统研究。采用均匀实验设计和DPS数据处理,(依次)通过建模分析、二次多项式模型回归建立数学模型,再通过各因素方差分析和总方差分析,确定了理论最优实验条件,再用理论最优条件作重复实验进行验证,最终确定了原料氧化镁的最佳水化条件。在水化温度60℃,水化时间105 min,液固比4,陈化时间4 h,水化剂1含量4.0%,水化剂2含量3.15%,洗水量4倍,搅拌速度120 r/min时,原料氧化镁的水化率达99.50%以上,得到的硅钢级氧化镁前驱体氢氧化镁纯度高、过滤性能良好。 By spray pyrolysis method,bischofite in Qinghai salt Lake,as primary raw material,was used to prepare precursor raw material MgO for silicon-steel MgO.The precursor raw material MgO was used for preparing Mg(OH)2 which was the precursor of silicon-steel MgO,by hydration method.In the hydration experiment of precursor raw material MgO,some experiment parameters were investigated systematically.such as the hydrated agent,the temperature and time of hydration,liquid/solid ratio that affected the hy...
硅钢级氧化镁的研究进展
随着中国电工钢产量的增加,硅钢级氧化镁需求量不断增加,传统的以白云石为原料制备氧化镁的工艺已经无法满足市场需求。中国是一个卤水资源丰富的国家,因此,研究如何资源化综合利用盐湖资源变得越来越重要。硅钢级氧化镁是一种制备取向硅钢的涂层材料,主要用于取向硅钢高温退火处理阶段,起到隔离剂、绝缘膜层、脱硫、脱磷等作用。综述了制备硅钢级氧化镁的方法、工艺流程、研究进展及存在的问题,指出了硅钢级氧化镁制备技术的发展方向,并对中国卤水资源的利用提出了建议。 With the increasing output of electric steel,the demand for silicon steel grade magnesium oxide(MgO) is larger and larger in China,and the traditional MgO production process with dolomite as raw material has been unable to meet market demand.China is a brine resource-rich country,the study of how to comprehensively utilize salt lake resources has become increasingly important.As a coating material used for preparing oriented silicon steel,silicon steel grade MgO is mainly used in the process of ...
卷取工艺对新型冷轧无取向电工钢组织性能的影响
研究了卷取工艺对一种新型含铜无取向电工钢晶粒尺寸、织构演变、铁损和磁感应强度的影响。结果表明,试样织构组分主要为{111}、{112}、{100}和高斯织构,在550℃卷取、保温2~3h,{100}织构有增强趋势,磁感应强度较高,铁损较低。 The effects of coiling process on grain size,texture,core loss and magnetic induction of a new cold rolled non-oriented electrical steel with copper were investigated.The results show that there are mainly {111},{112},{100} and {110}<001> texture.Coiling at 550℃and keeping for 2~3 hours,the {100} texture is enhanced,magnetic induction is higher and core loss is lower.
轧制复合法制备硅浓度梯度高硅钢薄带的织构演变
采用\"热轧复合+冷轧减薄+退火\"方法成功制备了0.20mm厚的硅浓度梯度高硅钢薄带,并采用SEM和X射线衍射技术对制备过程中组织和织构演变进行了研究。热轧复合板微观组织呈明显层状分布,复合界面为紧密冶金结合且经过83%的大冷轧变形未开裂。热轧和冷轧复合板带中均形成强α和γ织构,再结晶退火后形成强γ织构。冷轧和退火织构沿板厚呈显著的梯度分布特征,其主要来自于复合界面两侧硅浓度和初始热轧织构的差异性以及冷变形的不均匀性。 Gradient high silicon steel thin sheets with thickness of 0.20 mm were successfully produced by the rolling and annealing method,including hot rolling bonding,cold rolling,and annealing.Microstructure and texture evolution was investigated by means of SEM and X-ray diffraction.Microstructure of hot-rolling-bonding shows obviously layered distribution,the composite interface was closely metallurgical bonding and no cracking appears even after 83%cold rolling.Strongαandγfibers develop in the hot a...
电动汽车电机用电工钢疲劳性能测试技术研究
电动汽车电机在高速旋转时承受离心力和电磁力的作用,在进行电机转子设计时,既要考虑电磁性能,还要考虑机械性能。对电机转子受力情况进行了综述,分析了转子用电工钢疲劳性能参数的重要性,详细阐述了试样抛光、表面处理、试样的对中和安装对测试结果的影响。 The motor of electric vehicle bears big force for high speed rotors,mainly including centrifugal and electromagnetic forces.The magnetic and mechanical aspects of the electrical steel are crucial to machine design.In this paper,the forces applied on the motor were summarized and importance of fatigue properties was analyzed.The influence of specimen polish,surface treatment,alignment and installation on fatigue testing result were represented in detail.
电工钢RH脱硫渣系研究
针对攀枝花钢钒有限公司难以稳定生产w(S)≤0.006%高级别电工钢的问题,通过开发RH脱硫剂、钢包渣改性及工艺参数控制,形成了RH脱硫系统工艺技术。经工业试验表明,采用该工艺技术后,钢水脱硫率最高达到42%,成品w(S)控制在0.005%以下,全氧、氮含量也得到了较好的控制,且脱硫剂没有引起钢水增碳,满足高级别电工钢的生产要求。 In light of the difficulty of production of high level electrical steel w(S)≤0.006 % steadily in Panzhihua steel & vanadium Co.,Ltd.the process technology of RH desulfurization system has been formed by developing the RH desulfurizer,modifying the ladle slag and controlling the process parameters.Industrial experiments show that the desulfurization rate of hot metal rises to 42 % and the w(S) of the finished products is controlled in below 0.005 % and total oxygen and nitrogen contents are a...

