钢厂
脉冲磁场热处理对CGO取向硅钢脱碳退火过程中组织和织构的影响
采用自主研发的脉冲磁场退火装置,在取向硅钢脱碳退火过程中分别施加不同强度的磁场,并采用光学显微镜和X射线衍射仪研究了脉冲磁场脱碳退火后试样的显微组织和宏观织构。结果表明,脱碳退火过程中施加脉冲磁场后取向硅钢的平均晶粒尺寸均增加,当磁场强度为40 mT时,平均晶粒尺寸最大,为13.06μm。此外,取向硅钢试样的立方织构{001}<100>强度减弱,高斯织构{110}<001>和{111}<112>织构增强,有利于获得更好的成品织构和磁性能。 Self-developed pulsed magnetic field annealing device was used to apply magnetic field of different intensities during decarburization annealing of an oriented silicon steel, and microstructure and macro-texture of the specimens after decarburization annealing in a pulsed magnetic field were studied by using optical microscope and X-ray diffractometer. The results show that the average grain size of the oriented silicon steel increases with the application of pulsed magnetic field during decarbu...
低温高磁感取向硅钢高温退火过程高斯晶粒的演变
对低温加热工艺生产的以AlN为主抑制剂的高磁感取向硅钢高温退火过程进行中断实验,借助电子背散射衍射技术对高温退火过程中高斯晶粒的演变进行了研究.在升温过程中高斯晶粒平均尺寸先减小再增大.800℃时取向分布函数图出现高斯织构组分,但强度很弱,高斯晶粒偏离角在10°以上;900℃时高斯晶粒平均生长速率超过其他晶粒;950~1000℃时高斯晶粒异常长大,偏离角3°~6°;在1000℃之前高斯取向晶粒相比于其他晶粒没有尺寸优势. The high-temperature annealing process of high permeability grain-oriented silicon steel with AlN as an inhibitor was studied by interrupting test.The evolution of Goss texture in this process was analyzed by electron back-scattered diffraction.It is found that the Goss grain size first decreases and then increases with the rise of temperature.Goss texture appears in the orientation distribution function at 800 ℃,but the intensity is very weak and the deviation angle is more than 10°.The average...
硅钢级氧化镁颗粒度检测工艺的研究
通过对激光粒度分析仪测量硅钢级氧化镁(MgO)的分析条件进行优化,如分散介质、分散方式、样品预处理、仪器暗淡度等,探讨了硅钢级MgO粒度范围测量重现性较好的试验方法,满足硅钢生产过程控制对MgO粒度的要求。 The analysis condition of the laser particle size analyzer on grain oriented silicon-steel grade magnesium oxide is optimized,including the dispersion medium,dispersion methods,sample preparation,and instrument obscuration,etc.Therefore,particle size measurement with good reproducibility for silicon-steel magnesium oxide is discussed,which may meet the requirement of MgO particle size for silicon-steel process control.
取向硅钢常化水冷温度模型及控制方法研究
取向硅钢常化工序主要采用现场实测带钢温度的方式测定冷却速率,并通过稳定冷却水温、调整冷却水量及喷梁运行数量等方式保证合理的冷却速率,给常化工艺设计和生产带来诸多不便。通过对常化工艺水冷过程带钢的传热分析求解,在建立带钢水冷温度模型的基础上,研究了不同冷却工艺参数对带钢温度及冷却速率的影响规律以及冷却工艺的交互作用结果。结果表明:模型计算结果能够较好地反映取向硅钢在常化水冷过程中的温度及冷却速率的变化,其计算误差为0.80%~4.11%;在特定取向硅钢厚度规格和常化工艺下,随着常化冷却水量及有效冷却长度的增加,带钢水冷温度及冷却速率与呈非线性变化;常化水冷工艺主要通过调控带钢与冷却水之间热交换量和交换时间实现对带钢温度的控制,实际生产中需综合考虑机组速度、冷却水量及有效冷却长度之间的交互作用,选定喷梁投入数量和冷却水量以获得稳定的冷却速率。 The cooling rate of normalization process mainly determined by measuring the grain oriented silicon steel strip temperature on site, and ensures the cooling rate by stabilizing the cooling water temperature, adjusting the cooling water volume and the operation quantity of spray beam, which brings inconvenience to the normalization process design and production. Based on the heat transfer of strip in the water cooling section of normalization process, the water cooling temperature model for the n...
CN202111457976.8一种超低碳含钇取向硅钢及其制备方法
本发明的一种超低碳含钇取向硅钢及其制备方法,化学组成及质量百分比为Si:2.0~4.5%,C:≤0.003%,Y:0.001~0.1%,Mn:0.1~0.25%,Al:0.01~0.02%,Cu:0~0.3%,S:0.02~0.035%,N:0.009~0.011%,其余为Fe和不可避免的杂质元素。生产工艺为:连铸、铸坯加热、热轧、常化、冷轧、初次再结晶退火、二次再结晶退火。本发明采用超低碳的成分,取消了常规取向硅钢脱碳退火工艺,简化了生产流程。通过稀土微合金化解决了因超低碳成分导致的单向铁素体组织抑制剂析出困难的技术难题。本发明制备的含钇取向硅钢厚度为0.2~0.35mm,磁感应强度B8为1.85~1.94T,铁损P17/50为0.9~1.2W/kg,可以用于变压器的铁芯材料,制备流程更为简洁。
硅钢连退机组无氧化炉加热能力计算
无氧化炉具有加热效率高、投资与运营成本低、作业率高、表面质量及板型良好、NOx排放相对低等优势,在硅钢热处理领域应用前景广泛。本文阐述了确定无氧化炉(NOF)加热能力详细过程,涵盖炉温、炉断面尺寸、炉长、热平衡结算、加热能力计算等,为今后无氧化炉(NOF)在硅钢热处理应用时的设计提供了借鉴,同时也为今后明火直接加热的工业炉设计提供了参考。 Non-oxidation furnace has the advantage s of high heating efficiency, low investment and operation cost, high operation rate, good surface quality and plate shape, and relatively low NOxemission,and it still has wide application prospect in the field of silicon steel heat treatment. The detailed process of determining the heating capacity of a non-oxidizing furnace(NOF) is described, covering furnace temperature, furnace section size, furnace length, heat balance settlement, heating capacity cal...
CN202110029902.8一种基于临界变形制备高强度无取向电工钢的方法
一种基于临界变形制备高强度无取向电工钢的方法,按以下步骤进行:(1)按电工钢成分真空精炼钢水,连铸制成连铸坯;(2)在900~1100℃热处理30~120min,然后热轧制成热轧板;(3)冷轧冷轧板;冷轧板厚度为目标厚度+(0.01~0.1)mm;(4)在400~700℃进行一次退火处理,在850~1200℃进行二次退火处理;(5)酸洗去除氧化层,然后进行温轧或二次冷轧进行临界变形。本发明的方法利用位错强化机制采用临界变形提高无取向电工钢的强度的原理,利用一次退火二次退火进行一次调控织构并临界变形对织构二次调控的方法增加对磁性能有利的再结晶织构来优化磁性能,该生产方式工艺简单,成本较低,生产效率高,适用于大批量生产。
CN202111247576.4一种冷轧硅钢厚度缺陷识别方法、装置及系统
本发明涉及一种冷轧硅钢厚度缺陷识别方法、装置及系统,本发明的方法包括如下步骤:采集带钢设定厚度及其实际测量厚度并保存;将带钢实际测量厚度与带钢设定厚度相减得到实时厚度差;根据实时厚度差计算厚度缺陷评分;根据评分结果,确定带钢在厚度这一指标的缺陷等级。本发明评估过程考虑了厚度波动情况,并进行量化,能成功识别冷轧硅钢的厚度缺陷,设别准确性较高,提高了冷轧硅钢生产水平,为冷轧硅钢质量控制提供依据。
CN202110777440.8一种适应高频率工况下低铁损无取向电工钢及其生产方法
本发明公开了一种适应高频率工况下低铁损无取向电工钢及其生产方法,所述生产方法包括以下步骤:钢水连续浇铸成板坯—热轧—正火—酸洗—冷轧—连续退火—涂绝缘涂层并固化;所述冷轧步骤中,采用六辊单机架往复式轧机经5道次一次冷轧至目标厚度,冷轧过程中前三道次采用变速异步轧制方法,使钢板表层在剪应力作用下位错密度增加,这样在退火后表层晶粒尺寸细化而心部晶粒粗大,通过本发明的方法可生产得到心部为粗大等轴晶粒,表层为纳米级细等轴晶粒的电工钢产品,该产品的铁损P1.5/50≤2.35W/kg,P1.0/400≤14.0W/kg。
CN202110670657.9无取向硅钢及其生产方法
本发明揭示了一种无取向硅钢及其生产方法。所述生产方法包括:按照Si0.8~1.1%、Mn0.2~0.4%、不添加Sn和Sb进行炼钢,并制坯;将铸坯加热到1060~1120℃并保温150min以上,而后轧成厚度40~45mm的中间坯,再经精轧、卷取得到厚度为3.00±0.25mm的热轧卷板,精轧开轧温度≤872℃+1000*(11*[Si]‑14*[Mn]+21*[Al]);精轧终轧温度≤820℃,卷取温度≤560℃;常化、酸连轧,得到厚度为0.500±0.005mm的冷硬卷,常化温度850~900℃;成品退火温度820~880℃,退火后经冷却、涂层和精整,得到无取向硅钢。
大压下率冷轧无取向硅钢再结晶织构演变
研究了冷轧95%变形量无取向硅钢不同退火温度(710~1 050℃)下再结晶织构特征.再结晶刚完成时(710℃退火),呈现强γ({111<112>~<134>)与弱{114}<481>织构特征;随退火温度升高至900℃,γ明显减弱,{114}<481>组分持续增强,形成典型的{h,1,1}<1/h,1,2>织构;进一步升温至1 050℃,再结晶织构不再发生明显变化.基于EBSD分析,{114}<481>组分的持续强化可归因于其明显的尺寸优势以及较高频率的高能晶界(取向差角为20°~45°). A non-oriented silicon steel was heavily rolled to 95% reduction and subsequently annealed at 710~1 050 ℃ to investigate recrystallization texture evolution.When annealed at 710 ℃ with complete recrystallization,the texture is characterized by a strong partial γ fiber spreading from {111}<112> to {111}<134> and a weak {114}<481> component.As annealing at 900 ℃,γ fiber is decreased significantly while {114}<481> is increased consistently,producing a typical {h,1,1}<1/h,...
薄板坯连铸连轧流程试制含钒钛取向硅钢中氮化物析出相
通过热力学计算与模拟试验研究了含钒钛取向硅钢中氮化物析出相的析出规律与析出行为,并探讨了含钒钛元素的氮化物析出相作为薄板坯连铸连轧流程制备取向硅钢中辅助抑制剂的可行性.研究表明,在所冶炼的含钒钛取向硅钢的成分范围内,Ti N在钢液凝固末期便具备析出的热力学条件,而Al N与VN只可能在凝固后的α+γ或α+Fe3C两相区内析出.含钒钛取向硅钢中氮化物析出相以成分复杂的复合析出相为主,且随着钒钛加入量的增加,钢中抑制剂析出相总的分布密度由于含钒钛元素的氮化物析出相的增加而明显提高,使抑制剂抑制初次再结晶晶粒正常长大的能力得以加强,最终成品的磁感应强度值B8由1.857 T提升至1.898 T.同时,加入不高于0.007%的Ti与不高于0.005%的V不会影响中间脱碳退火工序的脱碳效果以及高温退火净化阶段硫、氮的脱除效果,其形成的含钒钛元素的纳米级氮化物析出相适合作为薄板坯连铸连轧流程制备取向硅钢的辅助抑制剂. The precipitation behavior of nitride precipitates in grain-oriented silicon steel containing vanadium and titanium elements produced by thin slab casting and rolling process was studied by thermodynamic calculation and simulation experiment. The feasibility of nitride precipitates containing V and Ti elements as auxiliary inhibitors was also investigated. It is found that Ti N is likely to precipitate at the final stage of solidification in the grain-oriented silicon steel,but VN and Al N can p...

