钢厂
低温取向硅钢热轧态组织及织构的研究
利用热模拟试验机、光学显微镜和X射线衍射仪对Fe-3.2%Si低温取向硅钢热轧工艺参数对组织及织构的影响进行了研究。结果表明,Fe-3.2%Si硅钢在1110℃粗轧、880℃终轧,轧后以10℃/s的速度冷却到550℃卷取,然后空冷到室温,热轧硅钢板沿板厚方向的显微组织不均匀性显著,对后续发展完善的二次再结晶有重要作用。无论是热轧板,常化板还是冷轧板,它们的织构集中分布在γ取向线上,γ取向线的织构除取向密度不同外,织构种类是一致的,这说明γ取向线上织构是有继承性的。从热轧到常化,织构取向密度显著减小,经二次冷轧后,织构密度又显著升高,可见,轧制变形有助于织构的形成并使织构强度升高。 The influence of hot-rolled process parameters on the microstructure and texture of Fe-3.2%Si low temperature hot rolled grain-oriented silicon steel were researched by hot simulation experiment machine,light microscope and X-ray diffractometer.The results show that,Fe-3.2%Si silicon steel is rolled by the technology with a temperature of rough rolling of1110℃,finish rolling of 880℃,coiling with the speed of 10℃ /s,and then cooled to room temperature with air.The microstructure of hot-rolled sil...
正火对双辊薄带连铸5.28%Si-1.11%Al无取向高硅钢磁性能的影响
采用双辊薄带连铸工艺试制了2.6 mm厚5.28%Si-1.11%Al高硅钢薄带,对比了1050℃×5 min正火及不正火铸带280℃冷轧至0.5 mm后,再经900～1100℃退火的磁性能。结果表明,高硅钢铸带显微组织为等轴晶组织,正火后铸带边部晶粒长大,中心层晶粒变化较小。成品中析出物主要为较粗大的AlN和AlN+MnS复合析出物,尺寸为0.5～2.5μm。与不正火试样相比,正火试样成品铁损大幅降低,磁感小幅下降;随退火温度的升高,两种工艺下铁损和磁感都是先降低后升高,在1050℃出现最低值。 2.6 mm thickness 5.28% Si-1.11% Al non-oriented high silicon steel was produced by twin roll thin strip casting.Magnetic property of the strip un-normalized and normalized at 1050 ℃×5 min was contrasted after cold rolled to 0.5 mm at 280 ℃ and 900-1100 ℃ final annealing.The results show that microstructure of the strip is equiaxed crystal.The surface grain is coarsened and the center layer grain has little change of the normalized strip.The main precipitates are AlN and MnS+AlN with 0.5-2.5 μm s...
退火工艺对普通取向硅钢初次再结晶组织的影响
为研究退火工艺对普通取向硅钢初次再结晶组织的影响,对经不同温度、保温时间和升温速率退火后的材料组织进行了分析。结果表明:在等温退火条件下,加热至600℃时开始发生初次再结晶,800℃以上初次再结晶组织发展完善;而在最终冷轧板直接进行最终高温退火的情况下,加热温度在500～700℃时,将升温速率提高到80℃/h,初次再结晶组织更易于发展完善。 To investigate the influence of annealing process on the recrystallization of common grain oriented silicon steel,microstructures of sheets annealed at different temperature,soaking time and heating rate are observed.Results show that under the condition of isothermal annealing,recrystallization begins at 600℃ and fully develops above 800℃,while in the case that the final cold rolled sheets are directly thrown to final high temperature annealing,recrystallization is likely to develop with the he...
酸溶铝对铸态取向硅钢中第二相粒子组成和形貌的影响
试验的铸态取向硅钢（/%:0.0440.056C,3.123.32Si,0.080.11Mn,0.0020.008S,0.002 90.029 1Als,0.006 20.010 9N）由30 kg高频真空感应炉熔炼。通过场发射扫描电子显微镜/能谱仪（FE-SEM/EDS）研究结果表明,0.002 9%Als钢中氧化物主要为SiO2,存在片状、棒状及近似球状的独立MnS,未发现含铝的氧化物或氮化物;0.0090%Als钢中出现以Al2O3为主的复合氧化夹杂物,存在MnS与AlN的复合析出物。钢中Als增加,复合析出物多呈簇状发展。氧化物容易成为MnS-AlN复合析出的核心,钢中Als含量越低,夹杂物中的MnS含量越高;作为核心的氧化物夹杂的尺寸越小,形成的复合夹杂物的形状越规则,尺寸也越小。热力学计算结果表明,钢中Als含量主要影响了钢中氧化物夹杂的组成和AlN的析出温度及析出量。 Test as-cast grain-oriented silicon steel（/%:0.044 0.056C,3.12 3.32Si,0.08 0.11Mn,0.0020.008S,0.002 90.029 1 Als,0.006 20.010 9N） is melted by a 30 kg high frequency vacuum induction furnace.The research results by using field emission-scanning electron microscope/energy dispersive spectrometer（FE-SEM/EDS） show that in 0.002 9%Als steel the main oxide is SiO2,and there is independent laminable,rod-like and approximate ...
硅钢高温氧化铁皮的显微结构表征
利用电子探针面分析、状态分析及电子背散射衍射相分析技术研究硅钢高温氧化铁皮的显微结构。电子探针面分析可以直观的看出元素的分布状态,初步判断氧化铁皮的结构,而状态分析可以准确表征常规氧化铁皮中铁元素的状态,对于合金元素富集区域则通过电子背散射衍射相分析技术来标定。结果表明,高温氧化铁皮的结构主要有4层,即最外层为厚度约为10μm的Fe2O3相,次外层为Fe3O4相,中间层为FeO相上分布有颗粒状的Fe3O4相,最内层为FeO相和Si元素富集的Fe2SiO4相。其中Fe2SiO4层的分布特征与加热温度密切相关:1 100℃时,Fe2SiO4相呈颗粒状,弥散分布在FeO层;1 200℃时,Fe2SiO4相呈液态,侵入基体和疏松的FeO层,且沿着FeO晶界呈网状分布。 The microstructure of high temperature oxide scale on silicon steel was characterized by electron probe microanalyzer(EPMA)mapping analysis,state analysis and electron backscatter diffraction(EBSD)phase analysis.The element distribution and the initial structure of the oxide scale could be detected by EPMA mapping analysis apparently.And the state of iron in the conventional oxide scales could be determined by state analysis.Meanwhile,the alloy-rich region could be identified by EBSD phase analy...
电工钢热压缩时动、静态再结晶组织及取向分析
采用热模拟方法及EBSD技术,研究Fe-3 wt%Si电工钢在不同温度下组织的动、静态再结晶及晶粒取向特征,特别是少量奥氏体对铁素体动、静态再结晶组织及取向的影响。结果表明,不同温度形变的组织主要分三类:形变长条铁素体、珠光体和等轴细小铁素体。长条形变铁素体内发生动态回复或连续式的动态再结晶,奥氏体周围的铁素体动态再结晶加速,部分以传统的不连续方式动态再结晶。铁素体、奥氏体都可发生静态再结晶。奥氏体的静态再结晶在1050℃以上明显,铁素体的静态再结晶随温度的升高逐渐进行,最显著的再结晶发生在1050℃。不同温度形变的样品,其形变晶粒取向主要以<111>和<100>为主,小等轴铁素体晶粒除与大形变铁素体取向相近外,出现了<110>取向及其它取向。 Static and dynamic recrystallization and grain orientations in a hot-compressed Fe-3 wt% Si electrical steels were studied at different temperatures using Gleeble simulator and EBSD technique,particularly focusing on the effect of small amount of austenite on ferritic microstructure and orientations.The results show that microstructure of the compressed steel,depending on deformation temperature,consisted of elongated and deformed ferrite,pearlite and fine equal-axed ferrite.The elongated ferrit...
节能电机用无取向电工钢带退火工艺的试验与应用
针对节能电机对无取向电工钢在磁性能方面的特殊要求,采用普通W600牌号的热轧板为原料,通过大量的现场工艺试验,研究总结出了\"超低张力\"的运行工艺、\"先快后慢\"的加热工艺、\"先湿后干\"的退火脱碳工艺、\"先缓后急\"的冷却工艺,生产出P1.5/50≤4.0 W/kg、B50≥1.70 T的冷轧电工钢产品,满足了节能电机的要求。 Based on the special requirements of no-oriented electrical steel for saving energy motor in magnetic aspects,using common W600 brand of hot rolled plate as raw material,through a large number of real tests,an ultra-low tension process,heating process which was quick at first and then slow,annealing decarburization process which was dry after the first wet,and a cooling technology of \"slow after the first urgent\" were concluded.Electrical steel product with P1.5/50≤4.0W/kg,B50≥1.70T was produced...
新日铁高强度无取向电工钢的研究进展
针对新日铁公开的相关专利,总结日本高强度无取向电工钢的研究进展,分析了各专利化学成分、生产工艺及产品性能的特点,指出固溶强化、细晶强化、析出强化、位错强化都有可能被用来提高无取向电工钢的强度。在高强度无取向电工钢的研发过程中,需要根据其具体用途确定目标性能,再采用合适的强化手段,从而实现力学性能、磁性能和生产性能之间的平衡。 Authors summarize the research progress of high strength non-oriented electrical steel in Japan by learning related patents brought into the public by Nippon Steel. Authors also analyze the characteristics of the chemical composition, production technology and properties of products in the patents and point out that any ones of solution strengthening method, fine-grain strengthening method, precipitation strengthening method or dislocations strengthening method may be used to improve the strengt...
