硅钢资料

试验研究了0.3 mm取向硅钢冷轧板(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005A1)的退火温度(760~880℃7 min)和退火时间(820℃3~9 min)对该钢的晶粒尺寸,再结晶和织构的影响。结果表明,最佳初次再结晶退火工艺为820℃5 min,该钢的平均晶粒尺寸为14.20μm,完全再结晶率为92%,不利{111}<110>结构含量为3.16%,有利织构{111}<112>,{012}<001>和高斯织构含量分别0.40%,4.73%和2.46%。 The effect of annealing temperature(at 760 ~ 880 X.for 7 min) and time(at 820℃ for 3~9 min) on grain size,recrystallization rate and texture of 0.3 mm cold-rolled sheet of oriented silicon steel(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005Al) has been tested and studied.Results show that with optimum recrystallized annealing at 820℃ for 5 min,the silicon steel average grain size is 14.20 fun,the complete recrystaUization rate is 92%,the unfavourable-texture {111}< 110 > content in steel is ... 

针对川威950的工艺现状,结合无取向低硅钢SGG生产的工艺特点,主要从控制其钢坯加热和轧制以及终轧温度和卷曲温度几方面入手,进行无取向低硅钢生产的工艺控制研究。同时根据近6000吨的生产实践表明,该工艺措施能很好的满足该钢种的需要。 950 process Chuanwei status quo,with non-oriented silicon steel production process features low,mainly from the control of billet heating and rolling and finish rolling temperature and coiling temperature of several aspects,for non-oriented silicon steel production process of low control at the same time According to nearly 6,000 tons of production practice shows that the process measures could well meet the needs of the steel. 

对硅钢板材分别进行异步和同步轧制,研究了轧制参数包括速比、压下量和道次对板材表面显微组织的演变的作用.结果表明,异步轧制硅钢板材表面形成了晶粒尺寸为10~50 nm,取向接近随机分布的纳米晶,而同步轧制板材的表面只形成了位错胞,证明异步轧制可以诱发表面纳米化.异步轧制板材表面纳米晶的形成过程为:在剪切力的反复作用下,高密度位错形成、滑移、湮灭和重组形成亚微米尺度的亚微晶/位错胞.随着压下量和轧制道次增加,高密度位错重复以上过程使晶粒尺寸减小、取向差增大,最终形成取向接近随机分布的纳米晶组织.大压下量和多道次是异步轧制诱发板材表面纳米化的关键,而速比的增加可以加快纳米化进程. Surface nanocrystallization(SNC) can effectively enhance the surface and global properties of the metallic materials,such as microhardness,intensity,fatigue,wear and corrosion resistances,therefore provides more promising practical industrial applicability.Up to now,several SNC treatment methods were developed based either on the principles of ball impactions or friction sliding,however,difficulty still exists for the surface treatment of large-dimensional samples with high efficiency.Recently,m... 

研究了热轧卷取时间对无取向电工钢晶粒组织、织构演变、铁损和磁感的影响。结果表明,成品晶粒尺寸在120～140μm之间,随卷取时间的增加,成品晶粒尺寸增大。成品织构主要由γ纤维、а纤维和高斯织构等构成。随着保温时间的增加,{111}<110>和{112}<110>织构强度降低。随卷取时间的增加,成品P1.5降低。热轧板最佳的卷取工艺为550℃保温2～3 h,电工钢的综合磁性能优良。 The effects of hot-rolling coiling time on microstructure,texture,core loss and magnetic induction of a new cold-rolled non-oriented electrical steel containing copper were investigated.The test results showed that for final product the grain sizes are 120-140um,with the increase of coiling time,the grain size increase.For final product there are mainly γ-fibre,а-fibre,and {110}<001> texture,Coiling at 550℃ for hot rolled plate,the {111}<110>,{112}<110> texture was weaked with ... 

为满足用户对无取向电工钢中硫含量的要求,采用CaO-CaF2复合渣系为脱硫剂,利用RH投入法对无取向电工钢进行深脱硫试验。试验结果表明,RH精炼渣成分控制在w CaO43%~51%、w Al2O325%~31%、w MgO4%~6%、w SiO29%~12%、w(FeO+MnO)3%~6%,在脱硫剂加入量为6~8 kg/t时,钢中平均硫含量从32×10-6降低到18×10-6,RH平均脱硫率为43.3%,最高达47.1%。利用KTH模型计算精炼终渣平均硫容量为0.003 1,RH精炼结束时渣-钢间实际平均硫分配比从14增加到52。 In order to satisfy the requirements of consumers on sulfur content in non-oriented electrical steel,taking( CaO-CaF 2) based flux as desulfurizer,industrial experiments on deep desulphurization of non-oriented electrical steel were carried out during RH process. The results show that as the compositions of refining slag are appropriately controlled with w CaO of 43% ~ 51%,w Al2O3 of 25% ~ 31%,w MgO of 4% ~ 6%,w SiO2 of 9% ~ 12%,and w( FeO + MnO) of 3% ~ 6%,and the desulfurizer added are at 6 ~ ... 

硅钢连续退火线是无取向硅钢生产的成品线。由于受机组布置的影响,带钢经转向辊进出口活套后,当套量达到60%后就出现偏离生产线的情况,从而影响最终产品的质量及成材率,甚至损坏设备。针对某冷轧厂硅钢连续退火机组出口活套入口处带钢跑偏开展纠偏研究,利用Matlab对该纠偏系统进行动态仿真研究,分析系统的稳定性。 Silicon steel continuous annealing line is non oriented silicon steel production of finished product line.Due to the influence of unit layout,strip by roll Import & Export loop,when the set volume reached 60% after the emergence of deviation from the production line,thus affecting the quality of the final product and the rate of finished products,and even damage the equipment.For the export of continuous annealing line in cold rolling silicon steel strip deviation rectification loop at the e... 

对商用50W330型无取向硅钢成品在930℃下保温2 h固溶并以不同方式冷却处理,利用磁性检测仪检测分析了处理前后的磁感和铁损变化,应用光学显微镜、扫描电子显微镜、X射线衍射仪观测分析了显微组织结构的演变。考察了平均晶粒尺寸、织构组分比及第二相粒子状态对磁性能的影响规律,结果表明:固溶处理前后平均晶粒尺寸的变化对硅钢磁性能的影响非常显著;当平均晶粒尺寸相差不大时,织构组分比[Goss+{100}]/{111}越大,磁感会越高;固溶处理会将细小弥散的第二相粒子重新回溶到基体中,减小了其对磁畴壁的钉扎作用,铁损随之下降。 The commercial 50W330 non-oriented silicon steel samples were heat treated at 930℃ for 2 h and cooled in different ways,then the iron loss and the magnetic induction of the samples before and after solution treatment were measured with a magnetic detector.The evolution of microstructural texture was analyzed by optical microscopy,scanning electron microscopy and X-ray diffractometry.The effects of average grain size,texture composition ratio and the second phase particles on the magnetic propert... 

【作者】 王磊； ...

对无取向电工钢中的夹杂进行了系统的分析。利用小样电解,采取不同电解液,不同的分离方法对无取向电工钢中稳定和不稳定夹杂物进行了提取、分离和收集。利用扫描电镜(SEM)、X-射线衍射、ICP等对电解分离收集的夹杂物进行了定性和定量分析。 The inclusion analysis of the non-oriented electrical steel has been investigated.By using small sample electrolytic analysis,with different electrolytes and different separation ways,the stable inclusions and unstable inclusions was drew,separated,and collected.With utilizing the methods of SEM,X-ray and ICP,the qualitative and quantitative analysis of inclusions in the non-oriented electrical steel was obtained. 

通过金相分析和电子背散射衍射技术研究了一种新型含铜无取向电工钢在950℃退火不同时间(3～180s)空冷后的组织和织构取向的演变。结果表明:该钢在退火3s时的主要织构为α和γ线织构,{100}<110>织构最强;退火20s时织构以<111><112>、{111}<110>、{112}<110>、高斯织构和立方织构为主,随着退火时间的延长,高斯织构和立方织构强度呈减弱趋势;合理控制保温时间有利于提高{100}、{110}面织构的占有率。 Evolution of microstructure and texture oriented of a new non-oriented electrical steel during annealing at 950℃for different times(3-180) s and air cooling was studied by metallography and electron back-scattering diffraction analysis.The results show that after annealing for 3 s most of the texture oriented alongα-fibre andγ-fibre,the intensity of {100}〈110〉was the strongest.{111}〈112〉,{111}〈110〉,{112}〈110〉,Gauss texture and cube texture were the main texture after annealing for 20 s,with the ... 

通过微观组织表征、高温拉伸和断口形貌分析,研究了钇(Y)元素对6.5%Si无取向硅钢组织、高温拉伸及断裂机制的影响。研究结果表明,添加Y元素可以在钢液中形成YS和YP的复合析出。YS和YP可以充当异质形核基底,提高形核率,细化凝固组织。热轧组织不均匀,由表层至芯部分别形成等轴晶、等轴晶/拉长晶和拉长晶的混合组织。退火后,热轧变形组织转变为等轴晶,含Y实验钢的退火组织得到明显细化。500℃时效处理后,含Y实验钢具备较低的有序度,300℃的拉伸断口呈现韧性断裂特征,断后伸长率达到20.2%。相反,无Y实验钢发生脆性断裂,断后伸长率仅为2.1%。研究结果证实,Y元素可以通过组织细化和降低有序度提高6.5%Si无取向硅钢的中温塑性。 The effects of yttrium(Y)on microstructure,elevated-temperature tensile properties and fracture mechanism of 6.5% Si non-oriented electrical steel were investigated by means of microstructure characterization,high-temperature tensile test and fracture analysis.The results showed that the doping of Y introduced composite Y-rich precipitates(YS/YP)in the melt.YS and YP precipitates were qualified for heterogeneous nucleation agents,which thus raised the nucleation rate and refined the solidificati... 

用还原分离-原子荧光光谱法分析了硅钢中的痕量汞.分析方法的不确定度主要来自测量重复性,样品溶液浓度,工作曲线变动性,标准溶液,移取、配制标准溶液,仪器变动性等.文章分别对上述构成合成不确定度大小的分量进行了计算讨论. Trace mercury in silicon steel and galvanized sheet was analyzed by adopting reduced separation-atomic fluorescence spectrometry.The uncertainty of the analysis method mainly comes from measurement repeatability,sample concentration,working curve volatility,standard solution,pipetting and preparation of standard solution,and instrument variability,etc.The essay conducted all calculations and discussions on the above components that determine uncertainty.