硅钢资料

分析总结退火工艺各参数对冷轧无取向硅钢磁性能的影响,结合设计和生产实践经验介绍退火工艺中各参数的实际生产取值,并针对现生产工艺过程中出现的典型问题提出解决办法。 It is analyzed and summarized the great influences on magnetism of cold rolled non-oriented silicon steel affected by various annealing process data in this article.The relevant settled ways is raised.According to the actual value presetting ways for various annealing process data based on design and production,as well as typical problems occurred during production. 

【作者】 潘恒韬； 刘涛； ...

用Gleeble1500D模拟试验机在变形温度为950～1 200℃、应变速率为0.01～8s-1、最大变形程度为60%的条件下,对硅钢50A1300做单道次压缩试验,首先分析了不同参数对流变应力的影响,然后用回归法确定了应力模型中的变形激活能及材料常数,得到硅钢50A1300在峰值应力条件和稳态应力条件下的变形激活能分别为270.360和91.557kJ/mol,同时得到了流变峰值应力模型,模型的相关系数为0.997。最后通过作lnθ-ε图的方法找到了硅钢50A1300发生动态再结晶的临界应变量,并回归得到峰值应变量、临界应变量与参数Z/C的关系式。 To analyze the effects of different parameters on the flow stress and critical strain of the dynamic recrystallization,single-pass compression experiments were carried out with silicon steel 50A1300 specimens using a Gleeble1500D thermal simulator at a temperature range of 950-1 200 ℃ and strain rate range of 0.01-8 s-1 under the condition of maximum deformation of 60%.The average deformation activation energy is respectively 270.360 and 91.557 kJ/mol under the peak stress and steady-state stres... 

无取向硅钢特别是中牌号以上的无取向硅钢,随着含硅量的提高,常温下塑性较差,冷轧过程中轧制力明显提高,如果存在原料质量问题,极易发生断带事故,影响硅钢冷轧过程的成材率和生产效率。通过优化冷轧工艺参数,可提高冷轧稳定性。生产中通过合理分配冷轧各道次压下量和轧制速度,保证了轧制过程的稳定,很大程度减少了冷轧断带事故的发生。 Non-oriented silicon steel, especially in the low and middle grade, with the increase of silicon content, plasticity is poor at room temperature, rolling force in cold rolling process significantly improved .If there is the quality defect of raw materials , easily sheet is rolling off. Affect finished product rate and production efficiency in process of cold-rolled silicon steel. Through optimization of cold rolled process parameter , improve the stability of cold-rolling process. Through reason... 

为满足用户对无取向电工钢中硫含量的要求,采用CaO-CaF2复合渣系为脱硫剂,利用RH投入法对无取向电工钢进行深脱硫试验。试验结果表明,RH精炼渣成分控制在w CaO43%~51%、w Al2O325%~31%、w MgO4%~6%、w SiO29%~12%、w(FeO+MnO)3%~6%,在脱硫剂加入量为6~8 kg/t时,钢中平均硫含量从32×10-6降低到18×10-6,RH平均脱硫率为43.3%,最高达47.1%。利用KTH模型计算精炼终渣平均硫容量为0.003 1,RH精炼结束时渣-钢间实际平均硫分配比从14增加到52。 In order to satisfy the requirements of consumers on sulfur content in non-oriented electrical steel,taking( CaO-CaF 2) based flux as desulfurizer,industrial experiments on deep desulphurization of non-oriented electrical steel were carried out during RH process. The results show that as the compositions of refining slag are appropriately controlled with w CaO of 43% ~ 51%,w Al2O3 of 25% ~ 31%,w MgO of 4% ~ 6%,w SiO2 of 9% ~ 12%,and w( FeO + MnO) of 3% ~ 6%,and the desulfurizer added are at 6 ~ ... 

阐述了影响硅钢卷材下料利用率的因素,并结合具体事例利用计算机排样系统进行了详细分析,对提高硅钢卷材的利用率具有一定的指导作用。 It describes the factors influenceing the the utilization ratio of the roll of Silicon steel,and analyzes it in detail combined with concrete examples by a computer arrangement system,which can give a guide for increasing the utilization ratio of the roll of Silicon steel. 

结合工业化生产的高效硅钢,进行了RH精炼稀土处理试验研究。针对不同的稀土处理条件,观察了夹杂物的形貌和尺寸分布,探讨了稀土处理后钢中的夹杂物形成、变化规律。结果表明:试验条件下,最佳的稀土合金添加数量为0.6～0.9 kg/t。经过合适的稀土处理后,可以有效抑制尺寸相对较小的、不规则的AlN、MnS复合夹杂生成,促进钢中微细夹杂物的聚合、上浮,钢质纯净度得到明显提高。此时,钢中全氧含量最低,脱硫效果最佳,钢中的夹杂物主要是尺寸相对较大的、近似球形或者椭球形的稀土类夹杂。 Based on the industrial production of non-oriented silicon steel,the experiment on RE treatment during the RH refining process was studied.The morphology and the size distribution were observed for the steel specimens treated with different RE treatment conditions.Further more,the formation and change of inclusions of final steel sheets after RE treatment were discussed.The results show that the suitable RE added amount was 0.6～0.9 kg/t.After the suitable RE treatment,the formation of AlN and Mn... 

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

从影响高牌号无取向硅钢退火工艺的主要参数入手,介绍高牌号无取向硅钢退火炉在加热、气氛控制、冷却、涂层烘烤方面的新技术,并展望无取向硅钢退火炉的发展方向。 Based on the technology parameters of high-grade non-oriented silicon steel annealing,the new technology of the annealing line,which includes heating,atmosphere control,cooling,coating baking,is introduced,and the development direction of non-oriented silicon steel annealing furnace is pointed out. 

采用Nb对Fe-6.5%Si(质量分数)高硅钢进行微合金化处理,结果表明:Nb在高硅钢薄板制备过程中细晶效果明显.铸态、锻态和热轧态组织的晶粒分别细化了17.50%,24.51%和30.13%.铸态样品压缩强度由1365 MPa提高至1520 MPa,延伸率提高77.78%;温轧板试样室温拉伸强度由573 MPa提高至621 MPa,延伸率提高44.44%.利用XRD对厚度为0.30—1.68 mm的温轧板的板面织构演变过程进行跟踪测量,结果发现:初始织构以(011)〈100〉Goss织构为主,单道次变形量为26.2%的情况下,Goss织构完全转化为(100)〈011〉旋转立方织构,随后,在单道次变形为22.6%的情况下,旋转立方织构完全转化为{111}面织构,即纤维织构,并稳定保持至0.30 mm. Fe-6.5%Si（mass fraction） alloy possess perfect magnetic properties,though intermetallics of Fe₁₄Si₂ phase brought 6.5%Si leads to room temperature brittleness and hinder this significant materials industrialization.Nb was adopted into micro-alloying of Fe-6.5%Si high silicon steel. OM,thermal simulated test machine and XRD were employed to study the influence of Nb on high silicon steel in processing stages.Textures of warm-rolled high silicon steel strips were determined b... 

对无取向电工钢中的夹杂进行了系统的分析。利用小样电解,采取不同电解液,不同的分离方法对无取向电工钢中稳定和不稳定夹杂物进行了提取、分离和收集。利用扫描电镜(SEM)、X-射线衍射、ICP等对电解分离收集的夹杂物进行了定性和定量分析。 The inclusion analysis of the non-oriented electrical steel has been investigated.By using small sample electrolytic analysis,with different electrolytes and different separation ways,the stable inclusions and unstable inclusions was drew,separated,and collected.With utilizing the methods of SEM,X-ray and ICP,the qualitative and quantitative analysis of inclusions in the non-oriented electrical steel was obtained. 

应用CAFE法对6.5%Si高硅钢铸锭凝固组织进行了模拟研究,确定出了适合高硅钢组织模拟的模型。进一步用该模型研究了过热度及冷却条件对凝固组织的影响,结果表明,随着过热度的降低,凝固组织中柱状晶比例和晶粒平均面积均减小。水冷条件下,高硅钢铸锭凝固组织几乎全是柱状晶,而且晶粒粗大。空冷条件下,等轴晶区扩大,但柱状晶仍占主要部分。缓冷条件下,等轴晶区占主要部分,晶粒平均面积和空冷条件下相当。 The solidification structure of 6. 5% Si steel ingot was simulated based on CAFE method and the model suitable for simulating the structure of high silicon steel wad ascertained. The influence of superheat and cooling condition on the solidification structure were studied. It was shown that with the superheat decreasing,the proportion of columnar crystals decrease,and the average grain size become smaller. Under water cooling condition,the solidification structure of casting was composed of almo...