钢厂
硅钢常化炉段工艺特征及问题分析
连续酸洗退火机组(CPAL)对于当前生产高磁感取向硅钢和高牌号无取向硅钢是必不可少的一个环节。常化炉是常化酸洗机组关键的组成部分。本文对国内自主建造的两条退火酸洗机组的工艺流程,特别是常化炉段进行了对比分析。总结出了常化炉的工艺及组成特点,对生产过程中暴露的问题进行了仔细的分析并提出了改进的意见,对于以后新建常化炉具有一定的提示作用。 The continous pickling annealing line(CPAL) is an essential step in producing high magnetic induction grain-oriented silicon steel and high grade non-oriented silicon steel.The normalizing furnace is a very important part of the CAPL.In this paper,the process flows of two CAPL with independent manufacture in our country have been compared,especially the part of normalizing furnaces.The characteristics of process and component are summarized and problems of the normalizing furnace during the prod...
无取向硅钢夹杂物分析
采用非水溶液电解方法来提取无取向硅钢中夹杂物。通过扫描电镜(SEM)观察结果表明:无取向硅钢中主要夹杂物为六棱柱的AlN、不规则硅酸盐及球状的铁的硫化物和氧化物,其中AlN夹杂尺寸在1~5μm,数量较多,还有部分AlN的复合夹杂。进一步研究了AlN复合夹杂形成机理,采用了Thermo-Calc热力学计算软件计算出该钢样中AlN、MnS析出温度分别为1 240℃、1 200℃,而Al2O3析出温度大于1 800℃,从而为AlN复合夹杂形成机理提供了一个理论依据。 Extracting inclusions from non-oriented silicon steel in non-aqueous electrolysis is a nondestructive method to gain inclusions.Scanning electron microscopy shows that the main inclusions in non-oriented silicon steel were hexagonal AlN,which was of large quantity,irregular silicate,spherical iron sulfide and oxide.The size of AlN inclusions ranged from 1to 5μm,and there were some duplex inclusions of AlN.To further study the formation mechanism of AlN duplex inclusions,Thermo-Calc thermodynamic...
硅钢高温退火环形炉炉壳制作与安装技术
硅钢高温退火环形炉炉壳制作与安装精度要求较高,施工时通过对壳体原材料矫正、炉壳板拼焊、下料切割、型钢骨架组装及焊接、骨架及炉壳板矫正、骨架与炉壳板组装及焊接、炉壳矫正、零配件装置、定位钻孔、报验检查、出厂、内侧板安装、外侧板安装、顶板安装等环节的工艺技术控制,能保质高效地完成硅钢高温退火环形炉炉壳制作与安装,为以后同类工程的施工提供可借鉴经验。 The required precision of manufacture and installation technique of the silicon steel high temperature annealing annular-furnace shell is high.During construction , manufacture and installation of the silicon steel high temperature annealing annular-furnace shell could be finished high efficiently through correcting the raw materials of shell , furnace shell plate welding , material cutting , steel frame assembly and welding , skeleton and shell plate correction , skeleton and furnace shell asse...
二次冷轧压下率对高牌号无取向硅钢组织结构和磁性能的影响
研究二次冷轧压下率对于硅的质量分数为3.0%的无取向硅钢组织结构和磁性能的影响。结果表明:当第二次冷轧压下率从0变化至16.7%时,铁损逐渐增加,磁感逐渐降低。当第二次冷轧压下率大于16.7%时,随压下率的增加,铁损逐渐减小,磁感逐渐增加。当第二次冷轧压下率大于38%时,二次冷轧法所能获得的磁性能明显优于一次冷轧法。 Effect of double cold reduction on magnetic,microstructure and texture of 3.0% Si non-oriented silicon steel sheets was investigated.The results show that the iron loss increases and magnetic induction reduces as the percentage redcution in secondary cold rolling changes from 0 to 16.7%.The core loss can be reduced remarkably,and magnetic induction can get a little benefit if the percentage redcution in double cold reduction is higher 16.7%.In case of higher than 38% of the percentage redcution ...
普通取向硅钢轧制过程中组织和织构的演变
借助电子背散射衍射(EBSD)及ZEISS-200MAT金相显微镜对某钢厂普通取向硅钢(CGO)进行研究,研究结果表明:热轧板组织、织构沿板厚方向存在明显的不均匀性,在热轧板表层及次表层发生再结晶,同时存在强度较高的Goss织构,中心层存在较强的{001}<110>变形织构。冷轧组织均呈纤维状条带组织,一次冷轧后,热轧板中的Goss织构消失,织构主要为α、γ织构,经中间脱碳退火后,α、γ织构强度减弱,并出现一定强度的Goss织构和利于Goss织构发展的{554}<225>、{332}<113>等织构,经二次冷轧后,二次冷轧织构类型与一次冷轧织构一致,但织构强度不同。 The grain-oriented silicon steel produced by a steel factory was investigated by EBSD and ZEISS-200 MAT metallographic microscope.The results show that the textures and microstructures along thickness of hot rolled slab are inhomogeneous.The surface layer and the layer near that are recrystallized structure which has a high Goss texture,but there is deformation texture{001}<110>in the central layer.The structure after cold rolling is a structure like fiber strip.After the first cold rollin...
低温板坯加热取向硅钢形变和初次再结晶织构的演变规律
采用取向分布函数和取向线分析方法对低温板坯加热取向硅钢从热轧到初次再结晶工艺阶段的织构进行了研究。研究表明:一次冷轧后各层的织构组分与热轧板各层面的织构组分存在着继承关系,次表层存在很强的{001}<110>织构,中心层的织构和热轧板的中心层相似,存在强的{001}<110>和{112}<110>织构;中间退火后发生再结晶,各织构组分的强度有所减弱,Goss织构组分再次出现;二次冷轧后沿厚度方向上的织构不均匀性不明显,{111}<112>织构强度最高,几乎是其他织构组分的1倍,{001}<110>织构大幅降低;初次再结晶后织构沿厚度方向没有明显的不均匀性,{111}<110>为最强的织构组分,并且具有一定强度的Goss位向。 The texture from the first cold rolling to the primary recrystallization of low temperature slab reheating grain-oriented electrical steel were researched by orientation distribution function and orientation distribution intensity technique.The results show that after the first stage of cold rolling,there is a strong {001}<110> texture in the subsurface and the texture in center layer is very similar to the center layer of hot band which has strong {001}<110> and {112}<110> tex...
微合金元素对冷轧取向电工钢再结晶行为的影响
以取向电工钢成分为基础,制备了含C或Mn和S的4种实验钢。观察了接近平衡析出状态实验钢经60%冷轧后在600~1000℃范围再结晶退火过程中微观组织演变,统计分析了再结晶体积分数随退火时间的变化规律,进而计算了各实验钢静态再结晶的激活能。观察了高含C实验钢退火初期再结晶晶粒优先出现的部位。结果表明900~1000℃范围内各实验钢铁素体的化学成分相似,因而其再结晶激活能基本一致。在600~800℃范围内铁素体内会有阻碍再结晶进程的三次渗碳体析出,从而使再结晶激活能明显提高。高C含量实验钢中还会有从奥氏体转变而来的粗大珠光体或渗碳体,轧制过程中其附近形成的变形区会促进600~800℃加热时该区域附近率先发生再结晶形核、降低再结晶激活能。固溶的Mn、S元素可微弱提高再结晶激活能,但高Mn、S含量会改变粗渗碳体从奥氏体析出时的形态。 Four experimental steels based on grain oriented electrical steel containing C,or Mn and S were prepared.Microstructure evolution of the steels close to a state of equilibrium precipitation were observed during annealing processes at 600-1000 ℃after 60% cold rolling,the changes of recrystallization volume fraction were analyzed statistically as the annealing was prolonged,and the activation energy for static recrystallization of the steels were calculated.The locations,where the recrystallizatio...
大数据技术在硅钢产品质量管控中的应用实践
磁性能指标是硅钢产品最关键的质量指标之一,但是目前磁性能判定100%依赖于样品的离线实验室检测结果,生产线配置的在线检测仪的测量结果由于精度问题,不宜直接用于成品牌号判级。本文在现有硅钢产品质量管控体系基础上,利用大数据技术对生产数据进行分析与建模,构建不同磁性能指标在线检测模型,并在现有信息系统上完成模型库的集成部署,实现硅钢产品全长、多指标磁性能结果的拟合数据输出,支撑取样优化、精准分切、辅助综合判定等功能应用,进一步优化硅钢产品质量管控体系。 The magnetic performance index of silicon steel products is one of the most critical quality indexes.However,at present,100%determination of magnetic performance depends on the offline laboratory test results of samples,and the measurement results of the online detector configured in the production line cannot be applied in practice due to the accuracy problem.Based on the existing quality control system of silicon steel products,big data technology was used to analyze and model the production d...
热处理工艺对含Mn高硅钢热轧带的组织及硬度的影响
研究了热处理工艺(退火温度、保温时间、冷却方式)对含Mn的Fe-6.5wt%Si高硅钢热轧带的显微组织及硬度的影响。结果表明,退火温度对Fe-6.5wt%Si合金的组织和显微硬度均有较大影响,随退火温度升高,平均晶粒尺寸和显微硬度均明显增大。小于1 h退火时,晶粒长大缓慢,而长时间(>1 h)退火时,一些次表层晶粒将发生异常长大。水冷组织比空冷组织略细小,但水冷显著降低了显微硬度。Mn含量提高能抑制850℃退火时晶粒的长大,并且促进退火后高硅钢的软化。 The influences of heat treatment process(annealing temperature,heating time,cooling methods) on the microstructure and microhardness of Fe-6.5wt%Si high silicon steel containing manganese for hot rolled strip were studied.The results show that the annealing temperature has a great effect on the microstructure and microhardness of Fe-6.5wt%Si alloy,and as the annealing temperature increases,the average grain sizes and microhardness will significantly increase.When annealing time for less than 1 h...
氢氧化镁煅烧制备硅钢级氧化镁的研究
以青海盐湖氯化镁为初级原料,采用喷雾热解法制备原料氧化镁。原料氧化镁通过水化制备氢氧化镁。将氢氧化镁过滤、洗涤、烘干、粉碎、煅烧,制备硅钢级氧化镁。本文重点考察煅烧温度、煅烧时间、料层厚度等因素对氧化镁水化率的影响,采用均匀实验设计和DPS数据处理,确定最优煅烧实验条件为:煅烧温度1250℃,煅烧保温时间4小时,料层厚度0.5cm。在此条件下得到的硅钢级氧化镁完全满足硅钢及氧化镁的行业标准。 The magnesium oxide is prepared by Spray pyrolysis process,which magnesium chloride from Qinghai Salt Lake is used as primary raw material,and hydrated to magnesium hydroxide,then obtained silicon steel magnesia through filtering,washing,drying,crushing and calcinations.In this paper,influences of some factors on magnesia hydration rate are studied,such as calcination temperature,calcination time and material thickness.After average experimental design and DPS data processing,optimal calcination...

