硅钢资料

利用X-射线衍射织构分析和线形分析技术测定了交叉轧制双取向硅钢在制备工艺各阶段的织构及微结构,进而探讨了立方织构({100}<001>)的形成过程。通过对实验结果的分析可知,二次冷轧和交叉轧制工艺为立方织构提供了内能优势和有利的形变织构,而低温预退火工艺既强化了立方织构的内能优势,又为立方织构的异常长大提供了有利的组织保证,最终在抑制剂(AlN和MnS)的协同作用下,硅钢在二次再结晶退火后形成了强烈的立方织构。 The texture and substructure of the double oriented electrical steels produced by the cross rolling technology during the difference process has been measured by means of the X-ray texture and diffraction peak profile analysis technology,and research the formation mechanism of cube texture,{100}<001>.The results show that the dominances of inner energy and deformation texture were supplied by secondary cold rolling and the cross rolling technology and strengthened by pre-annealing at a low... 

运用电子背散射衍射(EBSD)和X射线衍射(XRD)技术对硅钢热轧板的织构在板厚方向的分布进行了研究,并分析了两种织构测量方法的特点。EBSD技术能直观给出板厚方向的微观织构,XRD能得到钢板的宏观统计织构信息,结合两种技术的分析,能更直观更精确的研究不同织构在板厚方向的分布。 The texture distribution along the thickness of the silicon steel has been investigated by electron backscatter diffraction(EBSD) and X-ray diffraction(XRD) technique.The characteristics of two technique of texture analysis have been investigated.Combined the two techniques,the texture distribution along the thickness of the silicon steel could be realized distinctly and accurately. 

电工钢反复弯曲次数是电工钢性能检验的重要指标之一,直接影响到用户在使用电工钢过程的机加工性能。主要分析了试样宽度、试样张力、晶粒取向、反复弯曲设备等因素对电工钢反复弯曲试验的影响,并对各个因素的影响程度进行量化以及原因探讨,从而归纳形成各影响因素的基本规律,以便为电工钢实际生产、用户使用提供科学指导。结果表明:试样宽度增加,反复弯曲次数也会不断增加,晶粒位向对取向电工钢的反复弯曲次数影响较大,当支座顶部到拨杆底部的距离减小或拉紧力增加时,反复弯曲次数会不断减小,但当拉紧力达到60N以上时,对反复弯曲次数影响不大,试样经退火后,反复弯曲次数略有上升。 The reverse bend number is an important performance of electrical steels′capabilities,affecting the machining performance directly when the customers used.It investigated some factors,such as sample′s width,sample′s tension load,grain orientation and equipment,how to effect the reverse bend test for electrical steel,measured the influence degree,and discussed the reason,in order to form basic rules which could be guided the manufacturing and using for electrical steel.Results showed that the rev... 

本发明公开了一种改善取向硅钢内外圈和边部表面质量的方法及环形炉，在一次冷轧工序中，采用错边卷曲，卷曲张力按渐变张力进行控制且头尾的卷曲张力大、中部的卷曲张力小，MgO的涂覆量与卷曲张力同步变化且头尾的涂覆量少、中部的涂覆量多；在高温退火工序中，环形炉的底板上增设一层由若干扇形块绕中心均布形成的垫层，相邻扇形块之间存在空隙，环形炉的内罩内钢卷的上端加盖通风式的盖板，盖板底面的内圈间隙伸入钢卷孔、外圈间隙套在钢卷上、中间通过绕中心均布的导流槽支撑在钢卷端面上，导流槽呈螺旋状且入口与盖板内圈上的开口一一对应连通、出口延伸至盖板底面外圈内侧。本发明可显著减少表面缺陷，明显改善表面质量和磁性，操作容易。

通过对激光粒度分析仪测量硅钢级氧化镁(MgO)的分析条件进行优化,如分散介质、分散方式、样品预处理、仪器暗淡度等,探讨了硅钢级MgO粒度范围测量重现性较好的试验方法,满足硅钢生产过程控制对MgO粒度的要求。 The analysis condition of the laser particle size analyzer on grain oriented silicon-steel grade magnesium oxide is optimized,including the dispersion medium,dispersion methods,sample preparation,and instrument obscuration,etc.Therefore,particle size measurement with good reproducibility for silicon-steel magnesium oxide is discussed,which may meet the requirement of MgO particle size for silicon-steel process control. 

采用EBSD技术研究了有、无拉应力作用下无取向硅钢在晶粒长大过程中织构转变及晶界变化的规律。结果表明:在晶粒生长期间,无应力作用下的硅钢中,{111}〈112〉,{111}〈110〉织构组分强化,而{100}〈001〉织构组分弱化;与无拉应力作用下的情况相比,施加5MPa的拉应力时,{111}〈112〉,{111}〈110〉织构组分强化的速率下降,{100}〈001〉织构组分变化不明显。对于在晶粒生长期间持续变化的{111}〈112〉,{111}〈110〉和{100}〈001〉织构组分而言,虽然有、无拉应力作用下硅钢的{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率均下降,而{100}〈001〉织构组分的高取向差角度晶界频率则上升,但当有拉应力作用后,{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率下降的速率变小,{100}〈001〉织构组分的高取向差角度晶界频率上升的速率稍有变小。通过对无取向硅钢在晶粒长大过程中织构转变及晶界变化规律的研究,分析了合金原子在晶界的偏聚行为。 The rules of texture and grain boundary transformation in the nonoriented silicon steel under applied stress or without applied stress during grain growth were investigated by EBSD.The results show that the {111}〈112〉 and {111}〈110〉 components in the nonoriented silicon steel without stress are strengthened during grain growth whereas {100}〈001〉 component is weakened,but the growth rate of {111}〈112〉 and {111}〈110〉 component decreases,while the area fraction of {100}〈001〉 component doesn’t chang... 

本发明公开了一种高牌号硅钢的穿带激光焊接方法，包括：将焊缝中硅含量降低到Si焊＜1.9%。采用激光+填丝焊接，填丝ER50‑6碳钢焊丝；根据焊缝截面积和激光焊接速度；激光填丝焊接时，激光线能量应足够大，达到填丝在熔池中充分混合，均匀分布，不至于填丝的成分浮在熔池的上半部分。采用此方法使焊缝组织从粗大铁素体变成细小、致密的无碳贝氏体，晶内沉淀相和晶间脆性相相对大幅减少，提高了焊缝韧性和成形性能，保证了高硅硅钢带的穿带焊接和连续生产。

本发明涉及无取向硅钢生产技术领域，公开了一种改善含Cu高强度无取向硅钢冷轧质量的方法，包括如下步骤：A)含Cu高强度无取向硅钢热轧卷化学成分(wt,％)：Si：2.0～3.5％，Als≤1.5％，Cu：1～3％，其他为Fe,Als,Mn以及不可避免的杂质元素，对热轧卷进行常化酸洗处理，常化温度T常满足：T常≤1620‑(0.5Als+1.5Si+Cu)％×104，单位℃；B)将常化后的热轧卷在电磁感应加热炉内进行加热；C)在冷轧机组开卷机进行开卷，冷轧第一道次开卷温度T冷轧满足：1.5×(Si+Cu)％×103‑T室温≤T冷轧≤40+2×(Si+Cu)％×103，单位℃，式中，T室温为室温；D)按照4‑6道次冷轧到目标厚度。本发明改善含Cu高强度无取向硅钢冷轧质量的方法，在采用传统常化工艺路线，保证较高的强度和磁性水平前提下，改善冷轧质量，提高成品成材率。

【作者】 姚昌国； ...

研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%～100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 

【机构】 武汉钢铁学院轧钢七二级电工钢结业小组； ...

【作者】 谌剑； ...