硅钢资料

利用OM,TEM,EDS与XRD技术,对Fe-3.15%Si低温取向硅钢热轧板不同常化处理后的显微组织、析出相及最终产品的磁性能进行了分析研究,并对热轧板和常化板经过冷轧后的冷轧板织构进行了对比分析.结果表明,采用1120℃保温3 min二段式冷却的常化处理工艺,常化板表层显微组织均匀,沿板厚方向的显微组织的不均匀性显著,对后续过程中形成高取向的Goss织构最有利,取向硅钢的磁性能最高;采用二段式冷却的常化冷却工艺最优,在此冷却工艺下析出的细小的析出物数量最多,且弥散分布在基体中,抑制剂的抑制效果最好,对成品获得高磁性最有利;热轧板、常化板经过冷轧后的冷轧板织构均主要由{111}〈110〉和{111}〈112〉织构组成,但常化板较热轧板冷轧后的冷轧板γ取向线织构密度明显增高,由此可以证实常化处理有助于取向硅钢最终获得高取向的Goss织构. The decreasing of slab heating temperature for grain-oriented silicon steel will reduce the amount of precipitates in hot rolled plate,and be disadvantage to the formation of ultimate Goss texture.The aim of normalizing is to control and adjust the amount,size and distribution of precipitates.Microstructures,precipitates and magnetic characteristics of finished products with different normalizing technologies for Fe-3.15%Si low temperature hot rolled grain-oriented silicon steel are researched,a... 

借助电子背散射(EBSD)技术对AlN为主抑制剂的Hi-B取向硅钢常化工艺的中间冷却制度进行了研究。结果表明:常化后试样均发生了完全再结晶,在60℃/s冷速下组织最均匀;在合适的冷却制度下常化板表层保留了强的Goss织构,它深入到1/4厚度处,并且形成对Goss织构有利的强{554}<225>织构。 The intermediate cooling system of Hi-B oriented silicon steel with AlN main inhibitor in normalizing process was studied by means of electron back diffraction(EBSD) technique. The results show that:the specimens after normalizing are fully recrystallization, and the microstructure is most uniform under the intermediate cooling rate of 60℃/s; under suitable cooling system, normalized plate surface retains strong Goss texture, it penetrates into the 1/4 thickness of the plate and forming strong {... 

通过对辉光放电发射光谱参数的优化,以铁元素为内标来消除基体效应,建立了测定硅钢薄板中微量硼元素的方法。优化的实验参数为:放电电压1200 V,放电电流50 mA,预溅射时间40 s,积分时间10 s。校准曲线硼元素含量范围0.0001%~0.022%,相关系数大于0.999,测量结果与认定值一致,相对标准偏差小于10%。完全能够满足日常分析测试的要求。 A glow discharge optical emission spectrometry(GD-OES) method for determining trace boron element in silicon steel sheets were established through optimization of instrumental parameters and using Fe element as an internal standard to eliminate the matrix effect.The optimized instrumental parameters included discharge voltage,discharge current,pre-sputtering time and integration time,which are 1200 V,50 mA,40 s,and 10 s,respectively.The content of boron element that can be determined from the ca... 

采用RH精炼添加钙合金方式对硅钢进行钙处理,结果表明,钙合金添加量为0.67、1.00和1.67 kg/t钢时,钢中Ca含量分别为0、2×10-6和4×10-(6质量分数);随着钙合金添加量的增加,钢中夹杂物粒度逐渐由0～2μm向2～4μm、4～6μm偏移;不同钙处理条件下,钢中均存在粒径小于1μm和粒径为1～5μm的MnS、CuxS夹杂物,后者或单独存在,或与AlN、CaS夹杂复合;钢中粒径为5～10μm的夹杂物基本以Ca的氧化物和硫化物为主。与未经钙处理的炉次相比,钙合金添加量为0.67、1.00和1.67 kg/t钢时,粒径小于1.0μm的夹杂物减少幅度分别为68.06%、87.50%和94.94%。钙合金添加量为1.67 kg/t钢时,可以去除钢中绝大部分的微细夹杂物。 In order to improve the properties of final silicon steels,the calcium treatment was adopted by adding Ca alloys into the liquid steel during the RH refining process.Results show that when the addition of Ca alloys is 0.67 kg/t,1.00 kg/t and 1.67 kg/t,the corresponding Ca content in silicon steels is 0,2 × 10-6 and 4 × 10-6 respectively.With the increase of Ca alloy addition,the particle sizes of inclusions in steels become 2～4 μm and 4～6 μm,from 0～2 μm.Under different calcium treatments,there e...