硅钢资料

通过对取向硅钢进行脉冲磁场退火实验,发现在相同的退火时间(6.0 min)内,低于1 T的脉冲磁场可以在一定程度上提高取向硅钢的磁感(B8),而高于1 T的脉冲磁场则会使取向硅钢的磁性能急剧恶化.同时发现,脉冲直流电加热方式会使取向硅钢的磁性能恶化.研究表明,脉冲磁场退火有望成为一种调控材料微观结构的有效手段. We have carried out experiments of annealing by pulse magnetic field.The results show that a pulse magnetic field with intensity lower than 1 T can promote magnetic induction density(B8) of grain-oriented silicon steel,while the magnetic properties deteriorate sharply when intensity is higher than 1 T.It has also been found that heating by using pulse direct current can cause the magnetic properties to deteriorate,in contrast to the traditional heating using resistance furnace.Our research shows... 

研究了CSP工艺流程生产的硅含量为1.5%的无取向电工钢在不同常化温度下对磁性能的变化。研究结果表明:随着常化温度的提高,热轧板的晶粒尺寸增大,且组织均匀性提高;此外成品的有利织构组分{100}<0vw>、α、η增强,不利织构组分减弱;铁损P1.5/50呈下降趋势,磁感B50上升平缓。在常化工艺为970℃×2.5min下,对应的铁损P1.5/50<3.4W/kg,磁感B50>1.74T。 The effect of normalizing temperature on the magnetic properties of non-oriented electrical steel containing 1.5%silicon produced by CSP process was studied.The results show that with increasing normalizing temperature,the average grain size of hot-rolled plate increases and the microstructure uniformity is improved.Furthermore,the texture components of finished products are improved through enhancing of{100}<0vw>,αandηtextures and weakening of{111}<112>texture;the core loss P1.5/50 ... 

通过对激光粒度分析仪测量硅钢级氧化镁(MgO)的分析条件进行优化,如分散介质、分散方式、样品预处理、仪器暗淡度等,探讨了硅钢级MgO粒度范围测量重现性较好的试验方法,满足硅钢生产过程控制对MgO粒度的要求。 The analysis condition of the laser particle size analyzer on grain oriented silicon-steel grade magnesium oxide is optimized,including the dispersion medium,dispersion methods,sample preparation,and instrument obscuration,etc.Therefore,particle size measurement with good reproducibility for silicon-steel magnesium oxide is discussed,which may meet the requirement of MgO particle size for silicon-steel process control. 

针对新能源汽车的发展，制备了含Ni固溶强化、含Cu析出强化以及含Ni+Cu复合强化3%Si无取向硅钢，研究了强化方式对无取向硅钢组织、织构和性能的影响。结果表明：固溶强化型无取向硅钢热轧板中形成了粗大{221}<221>晶粒，冷轧过程中剪切变形明显并在退火后形成良好再结晶织构。析出强化型无取向硅钢热轧板中心层形成γ取向粗大晶粒，在后续的加工中γ织构逐渐增强并最终得到相对细小的再结晶晶粒。复合强化型无取向硅钢热轧板中保留了强λ取向带状组织，退火后形成了有益的Goss织构和λ织构。固溶强化型与复合强化型无取向硅钢磁感应强度B₅₀分别达到1.742、1.688 T,高于析出强化型无取向硅钢的1.645 T。同时，复合强化型无取向硅钢高频铁损最低，其P_1.0/400和P_{1.0/1 000}分别低至20.97、82.69 W/kg,这与其较小的晶粒尺寸和织构改善有关。强度计算结果表明：Ni元素固溶强化对强度的提高有限，屈服强度为468 MPa,纳米Cu析出可显著提高屈服强度（强度增量约200 MPa）,且主要来自于模量强... For the development of new energy vehicles, 3%Si non-oriented silicon steel were processed by solid solution strengthening with Ni, precipitation strengthening with Cu, and composite strengthening with Ni and Cu. The effects of different strengthening methods on the microstructure, texture and properties of high-strength non oriented silicon steel were studied.The results show that coarse {221}<221> grains are formed in the hot rolled sheet of solution strengthened non-oriented silicon ste... 

利用XRD和EBSD研究了长轴分别平行于轧向(RD)、横向(TD)和轧面法向(ND)的柱状晶样品在热轧、冷轧及退火过程中的组织、织构演变规律,并分别从几何诱导和取向诱导两个方面分析了晶界的交互作用.结果表明,热轧时由表面摩擦剪切作用引起的组织和织构梯度直接影响并遗传给后续冷轧及退火样品.热轧后,不同样品的初始晶粒形状各向异性差异消失,形成相同的各向异性晶界组织,但晶体学各向异性发生改变,导致随后冷轧、退火组织及织构的变化均不同于直接冷轧的柱状晶样品.研究中特别关注了对磁性能有利的{100}取向区域与晶界的关系. Columnar grains show their special characteristics of morphological and crystallographic anisotropies, and thus markedly influence the microstructure and texture evolution during rolling and annealing process in electrical steel. The rolling and annealing microstructure and texture of three columnar grained samples with the long axes arranged along different directions were investigated by means of XRD and EBSD techniques, and the effects of columnar grain boundaries were analyzed from the view ... 

研究了传统工艺流程生产的2%Si无取向电工钢在不同退火温度下的磁性能。研究结果表明,随着退火温度的升高,显微组织均匀性提高且晶粒尺寸增大;有利织构组分{100}<0vw>、α、η增强,不利织构组分减弱;成品的铁损P1.5/50先下降后略有上升,磁感B50上升平缓;在890℃×2 min的退火工艺条件下,成品电工钢的磁性能最佳,对应的铁损P1.5/50小于3.2 W/kg,磁感B50高于1.74 T。 In this paper,the effect of annealing temperature on magnetic properties of non-oriented electrical steel with 2% silicon was studied.Results show that the uniformity of microstructure and the average grain size increase with the rise of annealing temperature.The texture components of annealing can be improved by enhancing {100} <0vw>,α,η fiber textures and weakening {111} <112> fiber texture.The tendency of core loss P1.5/50 shows that it decreases first and then increases,while the... 

连续酸洗退火机组(CPAL)对于当前生产高磁感取向硅钢和高牌号无取向硅钢是必不可少的一个环节。常化炉是常化酸洗机组关键的组成部分。本文对国内自主建造的两条退火酸洗机组的工艺流程,特别是常化炉段进行了对比分析。总结出了常化炉的工艺及组成特点,对生产过程中暴露的问题进行了仔细的分析并提出了改进的意见,对于以后新建常化炉具有一定的提示作用。 The continous pickling annealing line(CPAL) is an essential step in producing high magnetic induction grain-oriented silicon steel and high grade non-oriented silicon steel.The normalizing furnace is a very important part of the CAPL.In this paper,the process flows of two CAPL with independent manufacture in our country have been compared,especially the part of normalizing furnaces.The characteristics of process and component are summarized and problems of the normalizing furnace during the prod... 

根据新日铁、JFE及浦项等国外钢铁公司2008年以来在日本专利局、欧洲专利局(EP)及世界知识产权组织(WIPO)申请公开的有关生产Hi-B取向电工钢典型专利技术,概述了近年来国外大型钢铁企业采用低温板坯加热(坯加热温度<1 280℃)技术生产Hi-B取向电工钢主要技术重点,即将调节关键化学成分Al、N、Sn及Sb等与工艺改进相结合。最后介绍了国外大型钢铁企业采用低温板坯加热技术生产Hi-B取向电工钢实例。 The latest developments on technology for manufacturing Hi-B grain oriented electrical steel sheets developed by Nippon Steel Corp.,JFE Steel and POSCO were described according to the patents published by World Intellectual Property Organization,Japan Patent Office and European Patent Office over the recent years.The low temperature slab heating process(particularly slab-heating temperature<1 280 ℃) together with suitably adjusting key chemical elements such as Al,N,Sn and Sb elements was the... 

【作者】 朱传芳； 潘恒韬； ...

采用扫描电镜、场发射扫描电镜、能谱仪等对50SW1300冷轧无取向硅钢中的夹杂物分不同尺寸区间进行数量统计,利用主成分回归分析法,即数据的标准化处理—主成分分析—回归分析—标准化的变量还原成原始变量—确定显著影响因素,综合分析夹杂物总量及各尺寸区间的夹杂物数量对无取向硅钢磁性能的影响。结果表明:主成分回归分析能够从夹杂物尺寸区间及数量的多个影响因素中提取主要的因素,定量研究其对磁性能的影响。分析表明,显著影响无取向硅钢铁损的夹杂物为100~500nm的AlN、AlN+MnS、MnS、Al2O3、AlN+Al2O3,而劣化磁感最明显的夹杂物尺寸区间为100~200nm。 Different size intervals of inclusions in cold rolled non-oriented silicon steel 50SW1300 were counted by scanning electron microscope(SEM),field emission scanning electron microscope(FESEM)and energy disperse spectroscopy(EDS).With principal component regression method:standardization for experimental data,principal component analysis,regression analysis,transform standardized variables into original variables,determination of significant factor,effects of the total number of inclusions and the... 

以太钢热连轧厂的硅钢为研究对象,利用凸度仪测量热轧带钢出口凸度值,采用矩阵和失效模式的分析方法了解影响带钢凸度变化的主次因素。研究结果表明:通过有效控制轧制过程中的加热温度、时间及采用合理的辊型,硅钢凸度精度提高了4.34%左右。 In this paper,we take the hot-rolled silicon steelsheet of Taigang as the research symbol,exit profile was measured by convex instrument,the primary and secondary factors that affect the strip profile were measured by using matrix and failure mode analysis methed.The results indicate that convexity accuracy has significantly improved by nearly 4.34% through the effective control of the heating temperature,heating time and the use of correct roller type in the process of hot rolling. 

在15 kg真空感应炉上,用CaO-Al2O3-SiO2-MgO渣系进行脱硫试验,探讨了脱硫渣系碱度、MI、Al2O3、CaF2对脱硫效果的影响。研究结果表明,随脱硫渣系碱度、MI、Al2O3和CaF2含量的增加,脱硫率都呈现先增加后减少的趋势。初始硫含量为0.009 33%~0.010 73%,加入脱硫渣系4 min时间内表观脱硫速率为(0.000 96~0.001 49)%/min,平均脱硫率为81.2%,最高达86.8%。当脱硫渣中w(CaO)=58.15%、w(SiO2)=4.85%、w(Al2O3)=25%、w(MgO)=6%、w(CaF2)=6%,脱硫效果最好,此时钢液中硫为0.001 33%。 Experiments on desulfurization of molten steel using CaO-Al2O3-SiO2-MgO based desulfurization slag was carried out in a 15 kg vacuum induction furnace. The effects of desulfurization slag basicity,MI, Al2O3and CaF2on desulfurization of molten steel were studied. The results show that with the increase of basicity,MI,Al2O3or CaF2in desulfurization slag,the desulfurization rate rises initially and then decreases. In addition,as the initial sulfur content is 0. 009 33% ~ 0. 010 73%,the apparent des...