硅钢资料

在实验室模拟CSP工艺条件下制备了取向硅钢,研究了二次冷轧中间退火工艺对组织和织构的影响。结果表明,中间退火温度对取向硅钢脱碳,高温退火组织及织构均产生明显影响。经940℃中间退火后,取向硅钢脱碳再结晶晶粒较850℃中间退火的多,且再经高温退火处理后,晶粒粗化,最大晶粒尺寸达4.8 mm;高斯织构组分密度达27.00,较850℃中间退火试样高。 Grain-oriented silicon steel was prepared by simulated CSP technology in laboratory. Effects of secondary cold-rolled intermediate annealing on microstructure and texture were studied. The results show that intermediate annealing has obvious effects on the microstructure and texture of the steels after decarburization annealing and high temperature annealing. After intermediate annealing at 940 ℃,recrystallized grain of decarburization annealed steel is more than that of intermediate annealed at... 

针对某硅钢车间ST机组的除尘系统除尘效率较低、排放浓度不达标、二次污染较严重的问题,通过现场调研,对除尘系统、含尘气体组分与物性参数等进行测试和分析,运用管道伴热技术改善粉尘黏性后,再选取合适的除尘器对粉尘进行除尘处理,大大地提高了系统的除尘效率。 To solve the problems of low dust removal efficiency, substandard emission concentration and severe secondary pollution, some investigations are conducted to test and analyze the dust removal system,dust-gas composition and relevant physical parameters.Moreover, dust removal efficiency is greatly improved by the use of pipe heat tracing technology and by choosing appropriate dust remover. 

以轻烧氧化镁粉为原料,经消化、碳化制得重镁水,在热解反应前采用络合剂对重镁水中的杂质钙、铁进行络合掩蔽,再经热解得到碱式碳酸镁,碱式碳酸镁经煅烧可制得钙、铁杂质含量较低的氧化镁。在重镁水络合除杂过程中,考察了络合剂三乙醇胺、柠檬酸、草酸单独和复合使用的除铁、除钙效果。以三乙醇胺为络合剂时,在200 mL重镁水中加10 mL三乙醇胺(1∶1),氧化镁产品中w(氧化镁)=99.3%、w(氧化钙)=0.31%、w(氧化铁)=0.042%;使用草酸和柠檬酸作为复合络合剂时,在200 mL重镁水中加入1.0 g柠檬酸和2.0 g草酸,氧化镁产品中w(氧化镁)=98.2%、w(氧化钙)=0.24%、w(氧化铁)=0.030%。 Light-burned magnesia as a raw material was hydrated and carbonated to obtain magnesium bicarbonate liquor.Before the pyrolyzing of magnesium bicarbonate liquor,complexants were used to cover Fe and Ca impurities.Then the treated liquid was pyrolyzed to obtain basic magnesium carbonate which was calcined to magnesium oxide with low calcium and iron content.During the complexing purification of magnesium bicarbonate liquor,the Fe and Ca removing effects of single or compound complexing agents,suc... 

通过对激光粒度分析仪测量硅钢级氧化镁(MgO)的分析条件进行优化,如分散介质、分散方式、样品预处理、仪器暗淡度等,探讨了硅钢级MgO粒度范围测量重现性较好的试验方法,满足硅钢生产过程控制对MgO粒度的要求。 The analysis condition of the laser particle size analyzer on grain oriented silicon-steel grade magnesium oxide is optimized,including the dispersion medium,dispersion methods,sample preparation,and instrument obscuration,etc.Therefore,particle size measurement with good reproducibility for silicon-steel magnesium oxide is discussed,which may meet the requirement of MgO particle size for silicon-steel process control. 

采用EBSD技术研究了有、无拉应力作用下无取向硅钢在晶粒长大过程中织构转变及晶界变化的规律。结果表明:在晶粒生长期间,无应力作用下的硅钢中,{111}〈112〉,{111}〈110〉织构组分强化,而{100}〈001〉织构组分弱化;与无拉应力作用下的情况相比,施加5MPa的拉应力时,{111}〈112〉,{111}〈110〉织构组分强化的速率下降,{100}〈001〉织构组分变化不明显。对于在晶粒生长期间持续变化的{111}〈112〉,{111}〈110〉和{100}〈001〉织构组分而言,虽然有、无拉应力作用下硅钢的{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率均下降,而{100}〈001〉织构组分的高取向差角度晶界频率则上升,但当有拉应力作用后,{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率下降的速率变小,{100}〈001〉织构组分的高取向差角度晶界频率上升的速率稍有变小。通过对无取向硅钢在晶粒长大过程中织构转变及晶界变化规律的研究,分析了合金原子在晶界的偏聚行为。 The rules of texture and grain boundary transformation in the nonoriented silicon steel under applied stress or without applied stress during grain growth were investigated by EBSD.The results show that the {111}〈112〉 and {111}〈110〉 components in the nonoriented silicon steel without stress are strengthened during grain growth whereas {100}〈001〉 component is weakened,but the growth rate of {111}〈112〉 and {111}〈110〉 component decreases,while the area fraction of {100}〈001〉 component doesn’t chang... 

目前随着电工钢用户冲压设备的升级,冲压速度逐步提高,对电工钢产品的硬度和强度指标提出了更高的要求。与普通硬度级别的无取向硅钢相比,高硬度50BW600的Hv硬度提高15~20,达到125以上,同时对电磁性能指标也有较高要求。本钢通过化学成份和热轧及冷轧连退生产工艺的设计,经过小批量生产试验,满足用户要求。通过对工艺的严格控制,在大批量生产过程中,保证了产品的力学性能和电磁性的检验合格率。 Currently with upgrading of stamping equipment of silicon steel user, gradually increasing of stamping speed, propose higher demand for hardness and strength of silicon steel. Compared with conventional 50BW600, high hardness 50BW600 have higher hardness, reach greater than 125Hv. Through design of chemical composition with hot mill and annealing, production test of small quantities, stamping performance meet user request. 

【作者】 凌健； ...

将Fe-1.5Si硅钢试样分别在1 000~1 200℃空气条件下氧化30 min,观察发现在1 000℃和1 100℃时,氧化层与基体界面处存在硅酸亚铁,而当温度为1 200℃时,硅酸亚铁不但存在于界面处,同时也存在于氧化层中.将各温度下得到的带有氧化层的试样进行单道次热轧试验,压下率分别为10%和30%,发现1 000℃和1 100℃时,较高的压下率使氧化层破碎更加严重,但是单道次热轧未能改变氧化层的结构;当温度为1 200℃时,由于液态的硅酸亚铁的出现,单道次热轧能够将界面处的液化的硅酸亚铁层挤压到氧化层中,消除了硅酸亚铁层的钉扎基体的效应,改善了氧化层与基体界面的平直度. Specimens of Fe-1.5Si silicon steel were oxidized at 1 000 ~ 1 200 ℃ in air for 30 min.At 1 000 ℃ and 1 100 ℃ fayalite was observed at the scale/substrate interface.While at 1 200 ℃fayalite was found both at the scale/substrate interface and at the outer oxide layer.Then after the single-pass hot rolling process,with the compression ratio of 10% and 30%,it was found that at 1000 ℃ and 1 100 ℃,higher compression rate accelerated the broken of the scale layers,but the scale structure was not affec... 

综述了国内外大钢铁企业与研究机构采用获得抑制剂法生产低温高磁感取向硅钢的开发及应用情况,分析了以该法生产高磁感取向硅钢过程中抑制剂的控制技术,包括固有抑制剂组成方案、气态渗氮方式与工艺及高温退火工艺的制定.研究表明,固有抑制剂组成方案的设计思路大体一致,化合物抑制剂以AlN为主、硫化物为辅,同时添加少量Sn,Sb等单元素抑制剂,但组成元素含量存在一定差别;在脱碳退火后用NH3进行非平衡渗氮处理已成为气态渗氮的主要方式,但最佳方式仍未明确,具体选择需依据实际生产条件,相应脱碳及渗氮工艺的控制条件差别较大;高温退火工艺中升温制度差别不大,升温阶段退火气氛中N2含量的选择存在差别.此外,分析了抑制剂控制技术目前存在的关键问题,并指出了进一步的研究方向. The current application and exploitation on production of low-temperature high magnetic induction grain-oriented silicon steel with acquired inhibitor method at both iron and steel enterprises and research institutions in the world are reviewed. The control techniques of inhibitors, which include the composition design for inherent inhibitors, nitriding method and process, and secondary recrystallization annealing, are thoroughly analyzed and proposed. It is indicated that the design ideas for i... 

某厂对电工钢的轧制策略进行了优化，粗轧道次由“1+5”改为“1+3”。在优化后的生产过程中，每次变换钢种，烫辊材就会出现窄尺现象，而紧随其后的电工钢板则出现超宽现象。文中针对该问题，介绍了宽度设定模型和宽度自适应模型的原理，阐述了该问题出现的原因及解决方案，并通过对宽度自适应模型的应用研究及优化攻关，有效地解决了问题，大幅提升了实物质量，降低了宽度封锁率。 The rolling strategy of electrical steel was optimized in a factory,and the rough rolling pass was changed from “1+5”to“1+3”.Subsequently,the following problems were occurred in the production process:when the steel grade changed,the roasting roller steel before the electrical steel appeared the narrow width phenomenon,and then the electrical steel appeared the ultra-wide phenomenon.This paper introduced the principle of width setting model and width adaptive model,and expounded the causes and s... 

【作者】 吴清； ...

研究二次冷轧压下率对于硅的质量分数为3.0%的无取向硅钢组织结构和磁性能的影响。结果表明:当第二次冷轧压下率从0变化至16.7%时,铁损逐渐增加,磁感逐渐降低。当第二次冷轧压下率大于16.7%时,随压下率的增加,铁损逐渐减小,磁感逐渐增加。当第二次冷轧压下率大于38%时,二次冷轧法所能获得的磁性能明显优于一次冷轧法。 Effect of double cold reduction on magnetic,microstructure and texture of 3.0% Si non-oriented silicon steel sheets was investigated.The results show that the iron loss increases and magnetic induction reduces as the percentage redcution in secondary cold rolling changes from 0 to 16.7%.The core loss can be reduced remarkably,and magnetic induction can get a little benefit if the percentage redcution in double cold reduction is higher 16.7%.In case of higher than 38% of the percentage redcution ...