钢厂
辉光放电发射光谱法测定硅钢薄板中微量硼元素
通过对辉光放电发射光谱参数的优化,以铁元素为内标来消除基体效应,建立了测定硅钢薄板中微量硼元素的方法。优化的实验参数为:放电电压1200 V,放电电流50 mA,预溅射时间40 s,积分时间10 s。校准曲线硼元素含量范围0.0001%~0.022%,相关系数大于0.999,测量结果与认定值一致,相对标准偏差小于10%。完全能够满足日常分析测试的要求。 A glow discharge optical emission spectrometry(GD-OES) method for determining trace boron element in silicon steel sheets were established through optimization of instrumental parameters and using Fe element as an internal standard to eliminate the matrix effect.The optimized instrumental parameters included discharge voltage,discharge current,pre-sputtering time and integration time,which are 1200 V,50 mA,40 s,and 10 s,respectively.The content of boron element that can be determined from the ca...
双辊连铸无取向硅钢铸带特征及常化作用研究
双辊连铸技术是冶金及材料领域内的一项前沿技术,对于生产高品质硅钢具有独特优势.本实验研究了一种双辊铸轧w[Si]=4.5%的无取向硅钢,考察其铸态和常化处理后样品的组织、织构及析出相尺寸特征.结果表明:铸带组织以与铸带法向成5~20(°)倾角的柱状晶为主,晶内存在少量0.3~0.4μm的AlN析出相,铸带织构以λ(<001>//ND)织构为主,表层织构漫散.950℃/10 min常化处理后,析出相尺寸增大,表层λ织构增强. As an advanced technique of metallurgy and material science,twin- roll strip casting has unique advantages for producing high quality silicon steel. The present study was aimed at a 4. 5% Si non- oriented electrical steel for analyzing the structure,texture and the size of precipitates at the initial and normalized state. The results revealed that the initial structure mainly consisted of columnar grains with 5 ~ 20( °) angle to the normal of cast strip,and some AlN precipitates of 0. 3 ~ 0. 4 μ...
多元抑制剂对高磁感取向硅钢性能的影响
介绍在取向硅钢生产中抑制剂的作用以及多元抑制剂的机理和应用情况,分析多元抑制剂方案中各种元素对高磁感取向硅钢性能的影响,并根据生产实践提出了进一步研究的方向. The role of an inhibitor in the production of grain oriented silicon steel,and the mechanism of multiplex inhibitor in the production are described in the present article.In addition,the influence of various elements in the multiplex inhibitor on the performance of grain oriented silicon steel with high magnetic induction is elucidated.Further work needed in this research is also indicated.
电解清洗装置在电工钢生产线上的应用
介绍了电工钢生产线连退机组的表面处理工艺,特别是电解清洗系统的工作机理、设备构造、生产工艺及各种影响因素。 This paper introduces the technology of surface treatment of continuous annealing unit in electrical steel production line,in particular the working mechanism,structure of equipment,production techniques and various influence factors of the electrolytic cleaning system.
常化温度对TSCR流程制备低碳低硅无取向硅钢组织和性能的影响
在实验室试制了TSCR流程的低碳低硅无取向硅钢,研究了在850~1050℃不同温度常化对冷轧量0.5mm厚钢板再经950℃×7min退火后的组织、织构和磁性能的影响。结果表明:随常化温度的升高,使热轧板晶粒尺寸增大,晶界更清晰,组织均匀性更好;由于第二相AlN和MnS析出物尺寸比较大,使冷轧退火后钢板晶粒也随常化温度升高呈单调增大趋势;γ有利织构和{111}、{112}不利织构与常化温度升高同时增强,但前者增强更多;冷轧板退火后铁损随常化温度升高呈单调下降,磁感呈单调上升趋势。 The low-carbon and low-silicon non-oriented silicon steel was prepared by thin slab casting and rolling(TSCR) in lab.The effect of normalizing at different temperatures in 850-1 050℃on microstructure, texture and magnetic properties of 0.5 mm cold-rolled sheets after annealing at 950℃for 7 min was researched. The results show that with increasing the normalizing temperature,the grain size of hot-rolled sheets increased,the grain boundaries were more clear and the rnicrostructure uniformity was b...
冷轧工艺对取向硅钢初次再结晶织构的影响
研究了取向硅钢制备过程中常见的两种冷轧工艺,主要研究了一阶段冷轧与两阶段冷轧+中间退火工艺对初次再结晶组织及织构的影响.结果表明:采用两阶段冷轧+中间退火工艺制备以Cu2S为主抑制剂的取向硅钢,其初次再结晶平均晶粒尺寸为18.1μm,高斯晶粒的体积分数为0.6%,迁移性强的重位点阵晶界(Σ5+Σ9)和高能晶界(20°~45°取向偏差角)所占比例分别为1.8%和50.4%.与一阶段冷轧工艺相比,其初次再结晶晶粒较细,且高斯晶核与特征晶界所占的比例较高,有利于高斯晶粒发生二次再结晶. Two common cold-rolling processes of grain oriented silicon steel and the effects of the single stage cold rolling and tw o-stage cold rolling w ith intermediate annealing processes on the primary recrystallization microstructure and texture w ere investigated. The results revealed that for the grain oriented silicon steel prepared under the tw o-stage cold rolling process w ith intermediate annealing w ith Cu 2 S as the main inhibitor,the average grain size of the primary recrystallization micr...
高牌号无取向电工钢热轧板常化退火组织的EBSD分析
借助于EBSD对比研究了常化退火对高牌号无取向电工钢热轧组织和织构演变的影响,分析了常化退火对热轧板各厚度层织构的演变规律。结果表明,常化退火改善了热轧组织的均匀性,并弱化了热轧变形的γ纤维织构。升高常化退火温度,可增大热轧板的晶粒尺寸,提高{100}和{110}织构组分占有率,有利于提高无取向电工钢成品板的磁性能。 Effects of normalizing annealing on microstructure and texture of high-grade non-oriented electrical steel hot-rolled sheet were investigated by EBSD. Emphasis was put on the effects of normalizing annealing on texture evolution in the sheet thickness. The results show that the hot-rolled microstructure homogeneity is improved and the γ-fiber texture is weakened by normalizing annealing treatment. The grain size of hot-rolled sheet and intensity of the {100} and {110} favorable texture can be in...
固溶处理对高牌号无取向硅钢磁性能的影响
对商用50W330型无取向硅钢成品在930℃下保温2 h固溶并以不同方式冷却处理,利用磁性检测仪检测分析了处理前后的磁感和铁损变化,应用光学显微镜、扫描电子显微镜、X射线衍射仪观测分析了显微组织结构的演变。考察了平均晶粒尺寸、织构组分比及第二相粒子状态对磁性能的影响规律,结果表明:固溶处理前后平均晶粒尺寸的变化对硅钢磁性能的影响非常显著;当平均晶粒尺寸相差不大时,织构组分比[Goss+{100}]/{111}越大,磁感会越高;固溶处理会将细小弥散的第二相粒子重新回溶到基体中,减小了其对磁畴壁的钉扎作用,铁损随之下降。 The commercial 50W330 non-oriented silicon steel samples were heat treated at 930℃ for 2 h and cooled in different ways,then the iron loss and the magnetic induction of the samples before and after solution treatment were measured with a magnetic detector.The evolution of microstructural texture was analyzed by optical microscopy,scanning electron microscopy and X-ray diffractometry.The effects of average grain size,texture composition ratio and the second phase particles on the magnetic propert...
PDSOFT在硅钢退火炉管道设计中的应用
结合硅钢退火炉项目中应用PDSOFT软件进行三维配管设计的案例,描述PDSOFT软件的应用过程,总结其使用要点,分析其优缺点,并提出了推广三维设计软件的思路,对今后PDSOFT在相似项目中的推广应用有参考和借鉴价值。 Combining the case of using PDSOFT software to design the three-dimensional piping,the application process of the PDSOFT software is described,the using points are summarized,the advantages and disadvantages are analyzed,and the ideas of promoting the three-dimensional design software are put forward,which have a strong reference value for the promotion and application of PDSOFT in similar projects in the future.
冷轧连退硅钢线工程中SF炉电加热体的焊接技术
通过对连退线SF炉内的电加热体的焊接技术进行总结分析,得出焊接时应采用的主要方法,采用本焊接方法可提高电加热体的焊接速度和焊接质量,保证了焊接质量和施工工期。 SF furnace for continuous annealing line heating body welding technology summary,the main method used in welding,welding method by using the electric heater to improve the welding speed and welding quality through the implementation of this method to ensure the welding quality and Construction period.

