钢厂
提高热轧硅钢凸度精度的工艺措施
以太钢热连轧厂的硅钢为研究对象,利用凸度仪测量热轧带钢出口凸度值,采用矩阵和失效模式的分析方法了解影响带钢凸度变化的主次因素。研究结果表明:通过有效控制轧制过程中的加热温度、时间及采用合理的辊型,硅钢凸度精度提高了4.34%左右。 In this paper,we take the hot-rolled silicon steelsheet of Taigang as the research symbol,exit profile was measured by convex instrument,the primary and secondary factors that affect the strip profile were measured by using matrix and failure mode analysis methed.The results indicate that convexity accuracy has significantly improved by nearly 4.34% through the effective control of the heating temperature,heating time and the use of correct roller type in the process of hot rolling.
0.3 mm厚的高强无取向电工钢的退火组织与性能
借助光学显微镜、扫描电镜、交流磁性能测量仪和万能拉伸试验机研究了0.3 mm厚高强无取向电工钢冷轧板在780、820、860和900℃退火保温2 min后的组织、织构和性能。结果表明:在退火温度范围内,试验钢均发生了完全再结晶,得到等轴状的铁素体晶粒;随着退火温度的升高,平均晶粒尺寸从9.2μm增长到41.3μm,工频铁损和400 Hz高频铁损均先大幅减小后趋于平缓,磁感应强度先升高后降低。在820℃退火时,铁损P1.5/50=5.51 W/kg,P1.0/400=33.22 W/kg均处于较低值,磁感应强度B5000最大,为1.649 T。试验钢的屈服强度和抗拉强度均随退火温度的升高而降低,780℃退火时屈服强度为496 MPa, 900℃退火时降低至407 MPa。综合磁性能和力学性能考虑,试验钢的最佳退火温度是820℃。 Microstructure, texture and properties of 0.3 mm thick high strength non-oriented electrical steel cold rolled sheet annealed at 780 ℃, 820 ℃, 860 ℃ and 900 ℃ for 2 min were studied by means of optical microscope, scanning electron microscopy, AC magnetic property tester and universal tensile testing machine. The results show that in the annealing temperature range, complete recrystallization of the experimental steel occurs and equiaxed ferrite grains are obtained. With the increase of annealin...
无取向硅钢铬酸镁绝缘涂层高温固化工艺
为了确保硅钢铬酸盐涂料的环保性,需要严格控制涂料的固化工艺,保证涂料固化过程中涂料中的六价铬充分转化为三价铬。对涂料及原料进行热重分析(TG)及差示扫描量热法分析(DSC)。结果表明,MgO与铬酐混合转化为MgCrO4,使六价铬稳定性增强,其中大部分Cr6+转变为Cr3+发生在620~700℃,在450~500℃高于铬酐发生大量失重,因此必须加入还原剂保证涂料中六价铬被充分还原;超过360℃后树脂会发生分解,因此实际板温不能超过360℃;加入了还原剂的整体涂料的失重温度区间主要在260~320℃,因此涂料固化时钢板的实际温度最佳区间为320~360℃。 Because of the silicon steel chromate coating’s environmental requirements,the paint curing process must be controlled strictly to ensure all Cr( Ⅵ) transforms to Cr( Ⅲ). The TG and DSC analyses of the paint are studied. The reaction of MgO and CrO3 would generate MgCrO4,enhancing the stability of Cr( Ⅵ). The most r( Ⅵ) in MgCrO4 changes to Cr( Ⅲ) at 620-700 ℃,while the CrO3 has a large weight loss at 450-500 ℃. The reductant must be added in the paint to make sure the Cr( Ⅵ) could transform suf...
微量Sn对0.4%Si无取向硅钢组织和磁性能的影响
结合实际生产0.4%Si无取向硅钢，统计了不含Sn和0.025%Sn无取向硅钢的磁性能变化，利用金相显微镜、X射线衍射仪观察分析不同成分下试样的显微组织和微观织构。试验结果表明：Sn元素可以显著降低无取向硅钢的晶粒尺寸，0.025%Sn试样的平均晶粒尺寸比不含Sn减小28.4%;加入Sn元素后抑制了无取向硅钢中不利于磁性能的{111}面织构组分强度，提高了对磁性能有利的{100}面织构组分强度，0.025%Sn与不含Sn相比磁感均值从1.756 T提升至1.768 T,铁损均值从5.476 W/kg降低至5.204 W/kg,明显改善了无取向硅钢磁性能。 In this paper combined with the actual production of 0.4% Si non oriented silicon steel, the magnetic properties of non oriented silicon steel without Sn and 0.025% Sn were counted. The microstructure and microtexture of samples with different compositions were observed and analyzed by metallographic microscope and X-ray diffraction. The results show that: Sn can significantly reduce the grain size of non oriented silicon steel, and the average grain size of 0.025% Sn sample is 28.4% smaller tha...
氧硫交互作用对硅钢中非金属夹杂物生成的影响
结合工业化生产的无取向硅钢,探讨了氧硫交互作用对钢中夹杂物生成的影响。借助非水溶液电解+扫描电镜法,研究了不同O、S含量下钢中夹杂物的变化规律。结果表明,本实验条件下,提高O含量、降低S含量,会劣化热轧组织再结晶效果。在劣化效果上,O的作用大于S;低Si、无Al硅钢中,应尽可能降低O含量、适当提高S含量,以粗化钢中微细夹杂物,减少尺寸小于1.0μm的夹杂物的数量;O、S含量与钢中夹杂物数量不具有关联性。生产过程中,不仅要严格控制O、S含量,还要严格控制生产工艺,以免生成较多的有害夹杂物。 Based on the industrial production of non-oriented silicon steel,the effects of interaction between oxygen and sulfur on the formation of inclusions were discussed.The change of non-metallic inclusions in steel sheets was investigated by means of electrolysis with non-aqueous solution under different oxygen and sulfur content.Results show that the recrystallization microstructure of hot rolled sheets will be deteriorated with the increase of oxygen content and the decrease of sulfur content.The ...
热变形温度对3%SiCGO硅钢组织和织构的影响
通过对3%Si CGO硅钢进行恒变形速率、不同变形温度下的单道次压缩实验,结合Thermal-Calc软件,金相分析,SEM及EBSD技术,研究了取向硅钢热变形过程中组织和微观织构的变化规律。结果表明:实验钢是在双相区变形,变形后组织主要是铁素体和少量的珠光体。随变形温度的升高,晶粒由长条状变为等轴状,尺寸逐渐变大;CGO硅钢在热变形过程中立方{100}<001>取向是较为稳定存在的。随着变形温度的提高,{111}<110>等取向逐渐转向{110}<1 10>取向,且{110}<1 10>取向逐渐变得锋锐。 3% Si CGO silicon steel was studied at constant strain rate and different deformation temperatures by single-pass compression deformation experiments to reveal the evolution of microstructure and texture during thermal deformation in oriented silicon steel,and the Thermal-Calc software,metallurgical,SEM and EBSD technique was used in the experiment. The results show that experimental steel is deformed at the temperatures of two-phase zone. The microstructure of the deformed steel consists of fer...
加热温度对W470高硅钢连铸坯氧化铁皮的影响
采用SEM、EDS和XRD对不同加热温度下W470连铸坯氧化铁皮的微观形貌及相结构进行研究。结果表明,W470氧化铁皮难以除去的原因是氧化铁皮熔化,液相包裹着FeO,凝固时发生共晶反应,生成FeO/Fe2SiO4共晶混合物,并深嵌入基体。降低加热炉的加热温度,使连铸坯全程在FeO/Fe2SiO4共晶混合物熔点(1177℃)以下加热,可降低氧化铁皮与基体的结合力,能够有效解决W470除鳞困难问题。 The microstructure and phase structure of iron scale of W470 continuous casting billet at different heating temperatures were investigated by SEM,EDS,and XRD.The results show that the reason why the iron scale of W470 removes hardly is that iron scale is melted and the FeO is surrounded by the liquid phase,which forms FeO / Fe2SiO4eutectic mixture and is embedded into the matrix after solidification.Lowering the heating temperature and keeping the continuous casting billet heating under the melt...
卷取工艺对新型冷轧无取向电工钢热轧带组织的影响
利用OM、SEM、TEM等实验方法研究了卷取工艺对一种新型含铜无取向电工钢晶粒度和析出相的影响。结果表明,该电工钢热轧带卷取后的晶粒尺寸为18～24μm,在卷取过程中,热轧带中有一定数量的第二相析出,经EDS能谱及选区电子衍射分析,这些析出相主要为AlN。随着卷取工艺的变化,该电工钢的晶粒度大小变化不明显,析出相的类型、尺寸大小不发生改变,体积分数发生一定的改变。 The effects of coiling process on grain size and precipitates of a new copper-bearing non-oriented electrical steel were investigated by OM,TEM and other experimental method.The results show that the grain size of hot-rolled bands after coiling is 18～24 μm.The second phases precipitate during coiling process.They are mainly AlN by EDS spectra and selected area electron diffraction.With the change of coiling process,the grain size of the electrical steel does not change significantly;the type and...
