硅钢资料

研究了薄板坯连铸连轧流程(TSCR)条件下热轧工艺对3.2%Si-0.7%Al无取向硅钢组织、织构演变及磁性能的影响规律。结果表明,提高均热温度和热轧温度有助于获得粗大的变形组织和强烈的{001}〈110〉织构,进而对后续的组织、织构演变进程及磁性能产生有利的遗传影响。与低温均热和低温热轧相比,高温均热和高温热轧得到的最终成品板的再结晶晶粒较粗大,λ纤维再结晶织构较强而γ纤维再结晶织构较弱,磁感应强度较高。 It was investigated that the effects of thin slab cast rolling(TSCR) hot rolling processes on microstructural,textural evolution and magnetic properties of 3.2%Si-0.7%Al non-oriented silicon steel.The results show that much larger hot rolling deformed microstructure and much stronger {001}〈110〉 texture could be obtained by increasing the soaking and hot rolling temperatures,which had good heritable effects on subsequent microstructural,textural evolution and magnetic properties.The final sheets ... 

日本住友金属成功地开发了一种资源节约型高强度无取向电工钢SXRC,这种电工钢是通过固溶铌适度抑制位错的合并对消而得到一种特殊的微观组织,因此兼具很高的力学性能和磁性,特别适用于HEV、EV驱动电机转子。而且,不使用昂贵的镍就可以达到期望的强度,合金成本可控,是一种优越的资源节约型产品。 Sumitomo metal industries ltd of Japan successfully developed a type of high strength non-orientation electrical steel SXRC of resources-saving.The steel has both high mechanical performance and good magnetic property thanks to the special microstructure produced by the formation of Nb solid solution serving to appropriately inhibit the combination and cancellation of dislocations.The material is,in particular,suitable for manufacturing rotors of HEV and EV driving motors.Besides,expected streng... 

【作者】 宋波； 朱一知； ...

用还原分离-原子荧光光谱法分析了硅钢中的痕量汞.分析方法的不确定度主要来自测量重复性,样品溶液浓度,工作曲线变动性,标准溶液,移取、配制标准溶液,仪器变动性等.文章分别对上述构成合成不确定度大小的分量进行了计算讨论. Trace mercury in silicon steel and galvanized sheet was analyzed by adopting reduced separation-atomic fluorescence spectrometry.The uncertainty of the analysis method mainly comes from measurement repeatability,sample concentration,working curve volatility,standard solution,pipetting and preparation of standard solution,and instrument variability,etc.The essay conducted all calculations and discussions on the above components that determine uncertainty. 

介绍了国内无底层取向电工钢生产技术水平、产量和用途，简述了无底层取向电工钢作为取向电工钢超/极薄带母料及应用于制作大型发电机组铁心、风电等电机铁心和变压器铁心等的情况。 The production technology level,output and application of domestic glassless grainoriented electrical steel were introduced,and the application of glassless grain-oriented electrical steel as parent material of ultra-thin strip of grain-oriented electrical steel and in making large-scale electric generator cores,wind power motor cores and transformer cores were briefly described. 

对w(Si)=3%无取向硅钢进行表面机械研磨处理(SMAT)和异步轧制(CSR),获得表面纳米结构,再进行550～650℃、4 h固体粉末渗硅处理,用透射电镜(TEM)、扫描电镜(SEM)和X射线衍射仪(XRD)研究表层组织演变。结果表明:经过SMAT后,w(Si)=3%无取向硅钢表面形成了等轴状、取向呈随机分布的、晶粒尺寸为10 nm的纳米晶组织;异步轧制后,表面纳米晶组织保持不变;550～650℃、4 h渗硅处理后,SMAT+CSR样品表面形成化合物层,其厚度随着温度的升高由17μm增加到52μm;化合物层由Fe3Si和FeSi相组成. Nanostructured surface layer was fabricated on a 3%(mass fraction) non-grain oriented silicon steel by means of surface mechanical attrition treatment(SMAT) and cross-shear rolling(CSR),and then a solid powder siliconizing treatment was carried out for the SMAT+CSR sample at 550~650 ℃ for 4 h.The microstructural evolution was examined by using transmission electron microscopy(TEM),scanning electron microscopy(SEM) and X-ray diffraction(XRD).Experimental results show that: equiaxed nanocrystallin... 

系统研究了无取向硅钢用磷酸盐系涂层性能的影响因素。以氢氧化铝和磷酸为原料制备磷酸二氢铝,再添加适量的添加剂酒石酸铵、二氧化硅、环氧树脂,得到的涂液涂布于硅钢表面,并控制合适的烘干温度,通过耐盐雾实验考察各因素对涂液耐腐蚀性能的影响。实验结果表明,在磷酸与氢氧化铝物质的量比为3.4∶1、酒石酸铵用量为2%、二氧化硅用量为1%、环氧树脂用量为5%、烘干温度为300℃条件下,所得涂层材料的防(耐)腐蚀效果最佳。 The factors influencing the performance of phosphate anticorrosive coating for non-oriented silicon were systematically studied.Aluminum dihydrogen phosphate was prepared with aluminum hydroxide and phosphoric acid as raw materials.Then added the right amount of additives,such as ammonium tartrate,silicon dioxide,and epoxy resin to prepare the liquid coating,which was coated on the surface of the silicon steel,and finally controlled a suitable drying temperature.The influences of various factors... 

选取了三种50W 800无取向电工钢,分析了化学成分、晶粒尺寸、织构、以及200℃时效处理48 h前后的磁性能和第二相粒子析出状态的变化。结果表明,钢板中第二相粒子的分布密度对钢板铁损有最重要的影响。降低钢中C、N元素含量,或改进钢板热加工参数以降低成品钢板中第二相粒子形成元素的过饱和度均有利于明显降低钢板磁时效过程中的铁损增幅。钢板中对磁性能有利的织构也有利于降低钢板铁损的时效幅度。 The evolution of chemical composition,grain size,texture,as well as magnetic property after aging treatment at 200 ℃ for 48 h and distribution of second phase particles precipitation in three selected 50W800 non-oriented electrical steels were analyzed.The results show that the distribution density of second phase particles has great influence on core loss.Reducing C and N content,or improving hot-working parameters to reduce the supersaturation of elements forming second phase particles in prod... 

在实验室模拟CSP工艺条件下制备了取向硅钢,研究了二次冷轧中间退火工艺对组织和织构的影响。结果表明,中间退火温度对取向硅钢脱碳,高温退火组织及织构均产生明显影响。经940℃中间退火后,取向硅钢脱碳再结晶晶粒较850℃中间退火的多,且再经高温退火处理后,晶粒粗化,最大晶粒尺寸达4.8 mm;高斯织构组分密度达27.00,较850℃中间退火试样高。 Grain-oriented silicon steel was prepared by simulated CSP technology in laboratory. Effects of secondary cold-rolled intermediate annealing on microstructure and texture were studied. The results show that intermediate annealing has obvious effects on the microstructure and texture of the steels after decarburization annealing and high temperature annealing. After intermediate annealing at 940 ℃,recrystallized grain of decarburization annealed steel is more than that of intermediate annealed at... 

通过对取向硅钢进行脉冲磁场退火实验,发现在相同的退火时间(6.0 min)内,低于1 T的脉冲磁场可以在一定程度上提高取向硅钢的磁感(B8),而高于1 T的脉冲磁场则会使取向硅钢的磁性能急剧恶化.同时发现,脉冲直流电加热方式会使取向硅钢的磁性能恶化.研究表明,脉冲磁场退火有望成为一种调控材料微观结构的有效手段. We have carried out experiments of annealing by pulse magnetic field.The results show that a pulse magnetic field with intensity lower than 1 T can promote magnetic induction density(B8) of grain-oriented silicon steel,while the magnetic properties deteriorate sharply when intensity is higher than 1 T.It has also been found that heating by using pulse direct current can cause the magnetic properties to deteriorate,in contrast to the traditional heating using resistance furnace.Our research shows... 

【作者】 李波； 杨晓江； ...

利用电子背散射衍射(EBSD)技术和场发射电子扫描显微镜(FESEM)研究了电工钢中柱状晶不同初始取向50%热压缩变形后的演变规律及其对粒子析出行为的影响。结果表明:〈100〉晶粒形变后仍为〈100〉取向,只发生绕ND∥〈100〉方向的转动,具有遗传性,粒子析出数量少。柱状晶长轴与压缩轴的偏转度增加,取向的稳定性变差,超过40°,可形成〈111〉取向,期间发生复杂的滑移系交互作用,产生较高的缺陷密度,促进粒子析出。MnS粒子主要在晶内析出,变形温度高、形变量低,粒子均无法充分析出。回复时,形变晶粒内高的储能和缺陷密度是促进粒子进一步析出的必要条件。 The evolution of initial orientations and their influence on precipitation of columnar-grained electrical steel after 50% hot compression deformation were investigated by electron backscatter diffraction technique and field emission scanning electron microscopy.The results indicate that the〈100〉orientated columnar grains remain still〈100〉after hot compression deformation,with only rotation around ND parallel to〈100〉direction,with heredity,and less precipitation.As the deviation angle between the...