钢厂
ICP-AES法测定硅钢中铌的不确定度评定
分析了电感耦合等离子体发射光谱法(ICP-AES)测定硅钢中铌的检测过程,讨论了该检测过程中不确定度的主要来源,建立了该方法的定量的数学模型,并根据这一模型计算出了检测结果的合成标准不确定度和扩展不确定度。 The measurement of niobium content in silicon steel by inductively coupled plasma atomic emission spectrometry(ICP-AES) was analyzed,by which the main factors affecting the uncertainty of the measurement were ascertained and the calculation formula was given.Finally,according to the formula the combined uncertainty and expanded uncertainty were obtained.
脉冲电场对取向硅钢磁性能及织构的影响
采用硅钢自动测量装置及X射线衍射仪检测出样品在实验前后的磁性能参数和织构强度.结果表明:较低的电压、9 Hz、较长的处理时间以及退火温度为650℃有利于增高铁损降低比例;较低的电压、较高的频率以及退火温度为650℃有利于增加磁感应强度增高比例.最佳的提高磁性能的实验参数是:频率为9 Hz,电压为500 V,处理时间为6 min,退火温度为650℃.通过织构分析可以验证:取向硅钢磁感应强度的变化取决于{110}<001>晶粒取向度值,而{110}<001>取向度值可看成是一个反映总体平均偏离角大小情况的综合值. An automatic measurement system for silicon steel and an X-ray diffraction meter were used for measuring the magnetic property parameters and texture of ex-processed samples and processed samples.It is shown that under the condition of a lower voltage,9Hz,a longer processed time and an annealing temperature of 650℃,the decrease rate of iron loss can be increased;a lower voltage,a higher frequency and an annealing temperature of 650℃ are in favor of improving the increase rate of magnetic inducti...
无取向电工钢孔洞缺陷控制实践
针对马钢无取向电工钢孔洞缺陷的分布规律及形貌特征,对缺陷样进行了显微分析,并利用生产实绩数据分析了该缺陷产生的原因。结合热轧生产过程,主要通过避免带钢撞击导卫以及降低导卫结瘤的产生等措施,可有效抑制热卷异物压入产生,从而降低冷轧工序孔洞的产生。 In viewing of the distribution and morphology characteristics of the hole defect of non-oriented electrical steel in Maanshan Iron and Steel Co.,Ltd.,the causes of the defect were analyzed by micro analysis of the defect sample and the production data.Combined with the production process of hot rolling,by avoiding the impact of strip steel on the guide and reducing the nodule formation on the guide,the pressing of foreign bodies in hot coiling could be effectively suppressed,thus reducing the fo...
50A1300牌号无取向硅钢磁性能改善工业实践
结合工业化生产的50A1300牌号无取向硅钢,分析了化学成分、RH精炼脱氧方式、板坯装炉温度以及热轧平整工艺等对磁性能的影响,探讨成品钢磁性能的改善。结果表明,采取改善后,50A1300牌号无取向硅钢的磁性能得到明显改善。2012年,该钢种平均铁损、磁感应强度分别达到5.26 W/kg、1.762 T,能够较好地满足用户市场需求及同行对标需要。 Based on the industrial manufacture of 50A1300 grade non-oriented silicon steel sheets,effects of chemical composition,deoxidization method in RH vacuum refining,charging temperature of steel slabs,hot rolling and flattening progress on magnetic properties are analyzed.The optimization methods of magnetic properties of steels are discussed. Results show that the magnetic properties are obviously improved by the adopted measures above. In 2012,the average core loss and the magnetic induction of 5...
电工钢RH脱硫渣系研究
针对攀枝花钢钒有限公司难以稳定生产w(S)≤0.006%高级别电工钢的问题,通过开发RH脱硫剂、钢包渣改性及工艺参数控制,形成了RH脱硫系统工艺技术。经工业试验表明,采用该工艺技术后,钢水脱硫率最高达到42%,成品w(S)控制在0.005%以下,全氧、氮含量也得到了较好的控制,且脱硫剂没有引起钢水增碳,满足高级别电工钢的生产要求。 In light of the difficulty of production of high level electrical steel w(S)≤0.006 % steadily in Panzhihua steel & vanadium Co.,Ltd.the process technology of RH desulfurization system has been formed by developing the RH desulfurizer,modifying the ladle slag and controlling the process parameters.Industrial experiments show that the desulfurization rate of hot metal rises to 42 % and the w(S) of the finished products is controlled in below 0.005 % and total oxygen and nitrogen contents are a...
无取向电工钢硫含量控制技术研究
针对采用含钒铁水生产无取向电工钢存在的铁水脱硫率低、转炉冶炼过程回硫量大、成品硫含量偏高的问题,通过对含钒钛铁水脱硫,减少转炉冶炼过程回硫以及RH脱硫技术等方面的研究,大幅度降低了电工钢成品硫含量。生产表明钢中w(S)=0.001 9%~0.006 9%,平均为0.004 2%;w(S)≤0.008%的比例达到了100%,且w(S)≤0.005%的比例也达到了91.43%。 In cognizance of the problems of low desulphurization rate for hot metal,large sulfur-recovery in converter as well as high sulfur content in products in producing non-orientation electrical steel with vanadium-content hot metal countermeasures have been carried out.Sulfur content in non-orientation electrical steel is decreased obviously by way of study on technologies of desulphurization for hot metal with vanadium & titanium,sulfur-recovery control in converter and desulphurization in RH ...
常化退火处理对无取向硅钢组织和织构的影响
采用光学显微镜和X射线衍射仪研究了常化退火处理对无取向硅钢热轧板和成品退火板显微组织和织构的影响。结果表明:常化退火处理消除了热轧板中的变形组织,促使变形晶粒完成再结晶;常化退火处理使高斯织构和立方织构易通过再结晶在变形带内形核和长大,可显著降低成品退火板的{111}和{112}不利织构组分的占有率,提高{100}和{110}有利织构组分的占有率,从而有利于提高无取向硅钢成品板的磁性能。 The effect of normalizing annealing treatment on microstructure and texture of non-oriented silicon steel hot rolled plates and final products were investigated by means of optical microscope and X-ray diffractometer analysis.The results show that the deformed microstructure of the hot rolled plates transformed into recrystallized grain after normalizing annealing treatment.The grains of Goss texture and cubic texture crystallographic orientation were formed and grown by recrystallization in the...
冷轧生产线硅钢激光辅助切割有限元模拟
研究了激光加热辅助圆盘剪高速切割技术,以解决现有冷轧生产线硅钢切边技术存在的微裂纹、应力、毛刺和边浪等问题。建立了激光加热温度场有限元分析模型,根据生产线上圆盘剪加工的实际过程,探讨了数值模拟中热源的加载形式,研究了激光对板材进行辅助加热时各个工艺参数如激光功率、光斑尺寸以及激光入射角度对切割工艺的影响,并通过实验对工艺参数进行了优化。最后,进了验证实验。实验结果显示:当激光加热点运动至圆盘剪刃口位置时,温度为100℃左右,此时材料硬度降低到原有硬度的70%~80%,降低了切削力,减少了圆盘剪的磨损,可有效提高圆盘剪的寿命。 Laser assisted trimmer side cutting technology was studied to overcome the problems such as micro cracks,stress,burrs and edge waves existing in a cold rolling production line of silicon steel side cutting.A finite element analysis model for the laser hearting temperature field was established, the loading form of a heating source was determined and influences of various processing parameters like laser powers,spot sizes,and laser incident angles on laser assisted heating sheet materials were di...
高Si电工钢铁芯的MA-SPS制备工艺和磁性能研究
以一种新的Fe-Si合金制备工艺为出发点,研究了不同放电等离子体快速烧结工艺(SPS)和Si含量变化对Fe-Si合金材料显微组织与磁性能的影响。结果表明,在烧结温度为1 000℃时制备的Fe-6.5%Si合金(质量分数,下同)的综合磁性能较好,其在50Hz下的铁损为0.549W/kg,最大磁感应强度为0.124 3T,矫顽力245.6 A/m,磁导率0.338mH/m。另外,材料的最大磁感应强度随Si含量的增加显著增长,1 000Hz下,Fe-10.0%Si的最大磁感应强度可达到Fe-6.5%Si合金的5倍左右。 The effects of Si content and SPS technology on microstructure and magnetic properties of Fe-Si alloy material were studied in the paper.It shows that the magnetic properties are the best when the content of Si is 6.5wt% and the sintering temperature is 1 000℃,the iron loss is 0.549W / kg in 50Hz,maximum magnetic induction is 0.124 3T,coercive force is 245.6A / m and permeability is 0.338mH / m。And,the maximum magnetic induction increases significantly with the increase of Si.The maximum magneti...
取向硅钢初次再结晶退火工艺正交试验
以试验室模拟CSP工艺生产的Fe-3Si热轧钢带为研究对象,采用正交试验及方差分析的方法,研究了取向硅钢初次再结晶退火工艺对高温退火后获得锋锐的高斯织构的影响。结果表明:取向硅钢两段式初次再结晶脱碳退火工艺参数加热段保温时间及加热温度是高温退火后获得锋锐高斯织构的主要影响因素,其可信度分别在90%和85%以上;在本试验条件下,通过正交试验获得的最佳退火工艺为:冷硬板经600℃保温3 min和850℃保温6 min。 Fe-3Si hot rolled strip was produced by simulating CSP technology in the laboratory.Orthogonal experiment and analysis of variance were carried out to investigate the influence of primary recrystallization on the sharp Goss texture of the oriented silicon steel.The results show that holding time of the heating section and the heating temperature for a sharp Goss texture of the samples annealed has important implications in this experiment conditions,the two-step decarburization annealing process...

