硅钢资料

为了消除硅钢在连续退火机组产生的浪形缺陷,对浪形缺陷产生的主要原因进行了分析。制定了相应控制措施,对炉内带钢张力、冷却段输出、碳套辊与带钢的同步性、无氧化炉燃烧状态等参数进行了调整;在生产组织上安排高低牌号宽窄规格穿插生产、定期更换碳套辊等,实施后效果明显。 The main cause leading to waviness defects of silicon steel is analyzed in order to eliminate the waviness defects of silicon steel in continuous annealing line.And thus corresponding measures for controlling these defects are made by means of adjusting these parameters such as the tension of silicon steel coils in continuous annealing furnace,the output in cooling section and the combusting condition of the non-oxidation furnace as well as keeping the synchronization between carbon sleeved roll... 

冷轧无取向硅钢是高技术含量、高附加值产品,工艺复杂,生产周期长,过程控制难度大,被誉为钢铁产品中的\"工艺品\"。热轧生产工艺又是无取向硅钢生产的重中之重,直接决定了硅钢的铁损和电磁性等多项指标。 Cold rolled non-oriented silicon steel is high technology content 、high added value product. Its process is complex, its production cycle is of length, and its process control is difficult, which is known as the iron and steel products \" Arts and crafts\". Hot rolling production process is the top priority of non-oriented silicon steel, which directly determines iron loss of the silicon steel and electromagnetic property,as well as other many index. 

利用EBSD技术研究了电工钢中不同的柱状晶尺寸及退火工艺下{100}织构的演变规律。结果表明,初始晶粒尺寸的影响最显著。细小柱状晶热轧后经过常化处理,组织已均匀,但中心层有强{100}织构。粗大柱状晶中{100}织构的遗传性强,常化及中间退火后,中心层仍有粗大的以{100}取向为主的晶粒;脱碳退火后才能完成组织均匀化和织构梯度的弱化。常化时的升温速度也对织构演变存在影响,低的升温速度有利于{100}织构的保留,但升温速度的影响没有初始晶粒尺寸及退火次数的影响显著。细小柱状晶样品经过热轧及三次退火工艺适合制备取向电工钢。 Evolution of {100} texture of different columnar grains and annealing process was investigated in electrical steels with the help of EBSD technique.The results show that the effect of initial grain size is the strongest.The initial fine-grained specimen shows uniform microstructure after the normalizing process,while {100} grains appear preferentially in the central layer of sheets.The heredity of {100} texture in the initial coarse-grained specimen is more significant.{100} mainly-oriented coar... 

对两种硅钢水溶性极厚绝缘涂层进行了不同温度的热老化实验。通过TG-DTA,GDS,FT-IR,SEM和光泽度仪等测试方法对老化的涂层进行分析表征,提出了评估硅钢水溶性极厚绝缘涂层热老化性能的合理温度区间,探讨了涂层热老化行为,并分析了两种涂层热老化性能的差异。结果表明,涂层附着性随着老化时间的延长逐渐下降。FT-IR表征结果显示,热老化过程中,涂料交联形成的化学键未发生断裂,交联剂氨基树脂的三嗪环被破坏是聚合物三维网络结构坍塌的主要原因。 Thermal aging expriments at different temperature were carried out on two types of water-soluble and extra-thick insulation coatings for non-oriented silicon steel,and a series of test methods such as glossmeters,TG-DTA,FT-IR,GDS,SEM were applied in analysis.For evaluating the thermal aging effect of this kind of insulation coating,the proper temperature range was proposed.The difference of aging performance between two coatings was been investigated and the related behaviors were been discussed... 

对低温加热工艺生产的普通取向(common grain-oriented,CGO)硅钢的高温退火过程进行了中断实验,材料为含3.0%Si、0.5%Cu、0.009 8%S(均为质量分数)的以Cu2S为主抑制剂的普通取向CGO钢。原始板坯厚度为230 mm,于1 200℃均热后经4道次粗轧、7道次精轧至2.3mm;热轧板采用两次冷轧法轧至0.3mm,中间完全脱碳退火,最后于1 200℃高温退火。最后样品的磁性能:铁损P17/50为1.182W/kg,磁感应强度B8为1.897T。借助配有EDAX OIM电子背散射衍射(EBSD)系统的ZEISS SUPRA 55VP扫描电子显微镜,对高温退火过程中高斯晶粒的演变进行了研究,结果表明:升温过程中晶粒尺寸增长缓慢,650℃时取向分布函数(ODF)图出现高斯织构组分,但强度很弱,高斯晶粒偏离角小于9°;950℃时高斯晶粒平均生长速度超过其他晶粒;950~1 000℃时高斯晶粒异常长大,偏离角降至约3°;在950℃之前高斯取向晶粒相比于其他晶粒没有尺寸优势。 The high-temperature annealing process of common grain-oriented(CGO)silicon steel was investigated by interrupting test.The samples were rolled from CGO silicon steel slab under low reheating temperature.The CGO silicon steel,taking Cu2S as the main inhibitor,contains3.0%Si,0.5%Cu,and 0.0098%S.The original casting slab is 230mm in thickness.After 1 200℃reheating,four-pass rough rolling and seven-pass finish rolling were conducted to make the thickness of the slab get to 2.3mm.Then the hot rolled... 

综述了退火温度、时间对无取向电工钢磁性的影响。退火温度主要影响无取向电工钢不同织构的占有率,退火时间主要影响晶粒尺寸的大小,晶粒尺寸的变化对织构的形成也有一定的影响。磁感最高点出现在纤维组织完全消失,(111)面织构组分较弱的组织状态。铁损的降低主要依赖于磁滞损耗的降低,织构的影响不大。 The effects of annealing temperature and time on the non-oriented electrical steel magnetic properties were reviewed.Annealing temperature and time mainly affects the different textures share and the grain sizes of non-oriented electrical steel respectively.Changes of the grain sizes also have a certain effect on textures formation.The highest point of the magnetic induction value in the fibrous tissue completely disappears and{111} plane texture has a lower state of the component content.Iron l... 

通过热力学计算,分析了实验钢中主要析出物析出的可能性。结果表明:在液相和固液两相区中,AlN和MnS均不能析出;在奥氏体区,AlN和MnS具备热力学析出条件,平衡析出温度分别为1547、1582 K。成品退火板中的析出物主要为AlN和MnS。扫描电镜下观察到的AlN形貌多为长条状,MnS形貌多为棒状或近似球形。这两种析出物占了析出物总量的85%以上,尺寸集中分布在400~800nm;复合析出物主要是(Al2O3+MnS)和(AlN+MnS),形貌不规则,尺寸集中在0.7~1.5μm;透射电镜下观察到了少量100nm以下独立的AlN析出。 According to thermodynamic calculation, the precipitation probability of precipitates was analyzed, AlN and MnS can not precipitate in liquid phase area and solid-liquid two-phase area. In austenite area, both the AlN and MnS have precipitation condition in thermodynamics and precipitates at 1547 K and 1582 K, respectively. The precipitates in annealing plate are mainly AlN and MnS. The shape of AlN is mostly strip, and MnS is stick or near sphericity. They accounted for over 85% of the total qu... 

两炉次无取向硅钢XG800WR（/%:0.003～0.004C、0.71～0.75Si、0.32～0.33Mn、0.004～0.007S、0.016P）的炼钢流程为铁水预处理（KR）-210 t顶底复吹转炉-钢包吹氩-RH脱碳精炼-230mm×1220 mm板坯连铸。53 t中间包钢水过热度为25～30℃,钢包到中间包采用长水口全程吹氩保护浇铸,中间包至结晶器采用浸入式水口浇铸。结果表明,在RH、中间包、结晶器过程中钢中总氧以及夹杂物数量和尺寸均明显降低;但在钢包到中间包过程T[O]、[N]和钢中夹杂物数量增加,说明长水口浇铸过程存在二次氧化。连铸坯中T[O]、[N]平均他分别为11×10^-6和30×10^-6,显微夹杂物数量平均为4个/mm²。铸坯中的显微夹杂物主要为3～5μm的AlN,同时存在少量的MnS、Al₂O₃·AlN和Al₂O₃·MgO·MnS。 The steelmaking flow sheet for two heats non-oriented silicon steel XG800WR（/%:0.003～0.004C. 0.71～0.75Si,0.32～0.33Mn,0.004～0.007S,0.016P） is hot metal pretreatment（KR）-210 t top and bottom combined blown converter-ladle argon blowing-RH decarburization refining-230 mm×1 220 mm slab casting.The superheating extent of liquid in 53 t tundish is 25～30℃,whole casting is shielded by blowing argon with long nozzle from ladle to tundish and the submerged nozzle is adopted in casting from tundish to mold... 

研究了取向硅钢制备过程中常见的两种冷轧工艺,主要研究了一阶段冷轧与两阶段冷轧+中间退火工艺对初次再结晶组织及织构的影响.结果表明:采用两阶段冷轧+中间退火工艺制备以Cu2S为主抑制剂的取向硅钢,其初次再结晶平均晶粒尺寸为18.1μm,高斯晶粒的体积分数为0.6%,迁移性强的重位点阵晶界(Σ5+Σ9)和高能晶界(20°~45°取向偏差角)所占比例分别为1.8%和50.4%.与一阶段冷轧工艺相比,其初次再结晶晶粒较细,且高斯晶核与特征晶界所占的比例较高,有利于高斯晶粒发生二次再结晶. Two common cold-rolling processes of grain oriented silicon steel and the effects of the single stage cold rolling and tw o-stage cold rolling w ith intermediate annealing processes on the primary recrystallization microstructure and texture w ere investigated. The results revealed that for the grain oriented silicon steel prepared under the tw o-stage cold rolling process w ith intermediate annealing w ith Cu 2 S as the main inhibitor,the average grain size of the primary recrystallization micr... 

【摘要】 <正>近日,从重钢集团获悉,日前重钢炼钢厂...

利用OM、EBSD等手段研究了热轧板两段式正火时在700℃保温不同时间(0、10、30、60 min)对含Sb冷轧无取向电工钢磁性能的影响。结果表明,700℃保温10 min处理的样品铁损最小,磁感最高。对成品板的组织分析结果表明,试样的晶粒尺寸随700℃保温时间的延长先增大后减小,保温10 min时晶粒尺寸达到最大;分析成品试样织构发现,有利织构组分随700℃保温时间的延长先增加后减少,保温10 min时有利织构组分所占百分比最高。因此,含Sb冷轧无取向电工钢两段式正火时在700℃保温10 min时磁性能最好。 Effect of two-stage normalization on magnetic property of non-oriented electrical steel containing antimony was investigated by using optical microscope(OM) and electron back-scattered diffraction technology(EBSD).The experimental results show that the iron loss and magnetic permeability of the specimen insulated at 700 ℃ for 10 min are lowest and highest respectively.The grain size of the finish specimens increases first and then decreases with the increase of holding time.Similarly,the advanta... 

2.9 mm热轧3%Si高牌号无取向硅钢板（/%:0.004 6C、3.04Si、0.32Mn、0.49Als、0.004S、0.013P、0.0042N）由CSP（Compact Strip Production紧凑式带材生产线）流程:120 t BOF-70 mm CC-热轧工艺生产。热轧终轧温度872℃,卷取温度683℃。铸坯及热轧板的组织和夹杂物的分析结果表明,铸坯组织为典型的贯穿柱状晶组织;热轧板边部为再结晶组织,中部为纤维组织带有少量再结晶晶粒;高牌号无取向硅钢的主要夹杂物为铸坯-Al₂O₃,AlN和Cu₂S+MnS;热轧板-Al₂O₃,AlN,AIN+MnS和Cu₂S+MnS。 The 2.9 mm hot rolled 3%Si high grade non-oriented silicon steel plate（/%:0.004 6C,3.04Si, 0.32Mn,0.49Als,0.004S,0.013P,0.004 2N） is produced by CSP（Compact Strip Production） flow sheet i.e.120 t BOF-70 mm CC-hot rolling process with end rolling at 872℃and coiling at 683℃.The analysis results on structure and inclusions in casting slab and hot rolled plate show that the structure of slab is typical trans-columnar crystal,the structure of hot rolled plate at edge is recrystallized grain and in ce...