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以不断增长的薄板坯流程为背景,与传统流程对比分析了薄板坯流程无取向电工钢热轧晶粒组织特征;以50W800和50W1300钢为典型实例,探讨了两种流程下成品板晶粒组织、织构、磁性能及其磁时效行为的基体差异和相关原理。研究表明,薄板坯流程热轧板组织较粗大,有利于在成品板中获得粗大的晶粒和有利的织构,从而得到较低的铁损和较高的磁感。然而,薄板坯流程会造成第二相粒子的细小弥散分布与不充分析出,容易因磁时效而使磁性能恶化。 Based on the rapid development of compact strip production(CSP) processing,the characteristics of hot band grain structure produced by CSP processing were analyzed in comparison with those of conventional technology.The basic differences in grain size,texture,magnetic properties and the magnetic aging behaviors of the final sheet products produced by the two processing technologies and the corresponding principles were discussed,while steel 50W800 and 50W1300 were taken as examples.It is indicat... 
2013-04-28 150 5.8

试验了通过NaCl-KCl-NaF-SiO2熔盐在电流密度50 mA/cm2、电沉积脉冲电流正反向比9:1和750850℃60min电沉积下阴极(/mm)20×20×0.5的1.6Si无取向冷轧硅钢片断面层硅的分布,并通过计算得出Si的扩散系数。结果表明,电沉积温度由750℃提高至850℃时,试样中Si含量增加,扩散的深度由18μm提高到40μm;电沉积温度与Si在钢中的扩散系数近似符合Arrhenius指数关系。 The distribution of silicon at cross section of cathode(/mm) 20 × 20 × 0.5 sheet of 1.6Si non-oriented cold rolled silicon steel after electro-deposit treatment by NaCl-KCl-NaF-SiO2 molten salt with current intensity 50 mA/cm2,electro-deposit pulse current positive-negative ratio 9:1 at 750 850 ℃ for 60 min has been tested and the diffusion coefficient of Si is obtained by calculation.Results show that with increasing electro-deposit temperature from 750 ℃ to 85... 
2014-06-28 176 5.8

选用国内外无取向硅钢标杆企业A、B、C的产品,采用非水溶液电解提取+SEM(EDS)方法,分析了其典型牌号对应成品试样中的夹杂物。结果表明,从磁性能控制角度而言,受钢的化学成分及生产工艺影响,A、B、C企业成品试样的夹杂物尺寸、种类、数量存在差异,这些差异对其磁性能产生显著影响;从夹杂物控制角度而言,A、B、C企业对应成品试样的夹杂物,以MnS、CuxS复合或者AlN、MnS、CuxS复合为主,其中1.0μm以下的夹杂物数量分别为2.34×107个/mm3、2.98×107个/mm3和11.98×107个/mm3,1.0μm以上夹杂物数量均很少,夹杂物的平均尺寸从大到小依次为A企业、B企业、C企业。 According to the production of three benchmarking manufacture enterprises A,B and C of non-oriented silicon steel at home and abroad,the inclusions in finished steel samples with typical grades were investigated by electrolytic extraction from non-aqueous solution and SEM(EDS).Results show that,from the viewpoint of improving the magnetic properties,affected by chemical composition and production technique,the size,type and amount of inclusions in finished steel samples are various,which will af... 
2013-01-28 155 5.8

研究了硅钢铸坯再加热过程中夹杂物的析出行为。采用非水溶液电解提取+扫描电镜观察方法,观察了试样的显微组织,统计了夹杂物的尺寸、种类、数量、分布。结果表明,均热温度为1 523 K时,水淬试样的夹杂物尺寸绝大部分小于0.5μm,0.5~5.0μm的夹杂物数量很少,没有发现5.0μm以上的夹杂物。此外,均热时间为10、30、60、90、120、240 min时,对应试样中0.05~0.2μm的夹杂物数量分别为4.04×104、4.73×104、3.70×104、3.33×104、3.10×104、1.56×104个/mm3。绝大部分夹杂物以MnS、AlN、CuxS类为主,并以三类夹杂物中的两类复合或三类复合居多。三类复合夹杂物总量占每组试样夹杂物总量的90%或以上。随均热时间延长,典型的夹杂物组成会发生如下变化:MnS+AlN+CuxS MnS+AlN AlN。与此同时,MnS、AlN、CuxS三者复合比例从45.2%(均热10 min)降为9.7%(均热240 min)。 The methods of electrolysis extraction from nonaqueous solution and scanning electron microscope were adopted to study the precipitation behavior of non-metallic inclusions in Si steel slabs during reheating processes.The morphologies,chemical compositions,quantity and size distribution of non-metallic inclusions in these steel samples were analyzed.Results show that,when the soaking temperature is 1 523 K,almost all of the non-metallic inclusions are smaller than 0.5 μm,few are in the range of ... 
2013-02-28 152 5.8

利用EBSD技术研究了电工钢中不同的柱状晶尺寸及退火工艺下{100}织构的演变规律。结果表明,初始晶粒尺寸的影响最显著。细小柱状晶热轧后经过常化处理,组织已均匀,但中心层有强{100}织构。粗大柱状晶中{100}织构的遗传性强,常化及中间退火后,中心层仍有粗大的以{100}取向为主的晶粒;脱碳退火后才能完成组织均匀化和织构梯度的弱化。常化时的升温速度也对织构演变存在影响,低的升温速度有利于{100}织构的保留,但升温速度的影响没有初始晶粒尺寸及退火次数的影响显著。细小柱状晶样品经过热轧及三次退火工艺适合制备取向电工钢。 Evolution of {100} texture of different columnar grains and annealing process was investigated in electrical steels with the help of EBSD technique.The results show that the effect of initial grain size is the strongest.The initial fine-grained specimen shows uniform microstructure after the normalizing process,while {100} grains appear preferentially in the central layer of sheets.The heredity of {100} texture in the initial coarse-grained specimen is more significant.{100} mainly-oriented coar... 
2013-08-28 163 5.8

采用扫描电镜、原子力显微镜研究了铬酸镁半无机绝缘涂层的微观结构。结果表明,涂层厚度为数微米,涂层中的有机树脂乳液颗粒均匀分布在无机涂层的表面,从而保证了涂层具有良好的冲片性能。采用极化曲线研究了涂层的耐蚀性能,发现铬酸镁与铬酸锌绝缘涂层的耐蚀性能相当。 In this paper,the microstructure and anti-corrosion property of magnesium chromate coating on non-oriented silicon steel were studied.The microstructure was observed by SEM and AFM.The anti-corrosion properties were evaluated by polarization curves.The results show that the thickness of coating is several microns and the polymer particles were scattered on the surface of inorganic coating,which is the guarantee for lamination property.The corrosion resistance of the magnesium chromate film was e... 
2011-03-28 152 5.8

采用低温板坯加热制备取向硅钢,通过透射电镜(TEM)观察并研究热轧板中的析出物,用ODF织构法研究热轧板距表面1/8、1/4和1/2处的织构分布。结果表明,热轧板中的析出物主要是密排六方AlN,AlN形貌呈规则长方形,AlN颗粒大小不等,分布密度低;热轧板中的织构沿板厚方向,由亚表层的{110}<001>织构向1/2中心层的α线织构变化,其中{110}<001>织构在热轧板距表面1/4层处最强。 The low temperature grain-oriented silicon steels were produced by acquired inhibitor method.The precipitates in hot rolling strip were observed and studied by transmission electron microscope,and the texture distribution in 1/8,1/4 and 1/2 layers of hot rolling strip were analyzed by ODF method.The results showed that the square shaped h-AlN is the main precipitates in hot rolling strip.The precipitates are varying in size and distribution.The texture of hot rolling strip in thick direction are... 
2011-04-28 176 5.8

利用本钢技术中心试验厂技术手段,并与北京钢铁研究院合作,试制了用作家电用电机、微电机、小电机或部分中型电机铁芯的冷轧无取向电工钢。试制钢硅含量小于0.5%,钢板表面平滑,公称厚度0.5mm,且厚度均匀偏差小,性能测定结果表明,产品的磁性能、力学性能满足其使用要求。 BX STEELTechnology Center pilot plant using technical means,and with Beijing Iron and Steel Research Institute,trial cold rolled non-oriented electrical steel that has been used as appliance motor core,micro motor core,small motor core,or part of the medium-sized motor core。Trial steel of silicon content is less than 0.5%,steel plate surface is smooth,the nominal thickness of 0.5mm,and the thickness deviation is small,performance measurement results show that the magnetic properties,mechanical p... 
2011-01-28 187 5.8

研究了取向硅钢制备过程中常见的两种冷轧工艺,主要研究了一阶段冷轧与两阶段冷轧+中间退火工艺对初次再结晶组织及织构的影响.结果表明:采用两阶段冷轧+中间退火工艺制备以Cu2S为主抑制剂的取向硅钢,其初次再结晶平均晶粒尺寸为18.1μm,高斯晶粒的体积分数为0.6%,迁移性强的重位点阵晶界(Σ5+Σ9)和高能晶界(20°~45°取向偏差角)所占比例分别为1.8%和50.4%.与一阶段冷轧工艺相比,其初次再结晶晶粒较细,且高斯晶核与特征晶界所占的比例较高,有利于高斯晶粒发生二次再结晶. Two common cold-rolling processes of grain oriented silicon steel and the effects of the single stage cold rolling and tw o-stage cold rolling w ith intermediate annealing processes on the primary recrystallization microstructure and texture w ere investigated. The results revealed that for the grain oriented silicon steel prepared under the tw o-stage cold rolling process w ith intermediate annealing w ith Cu 2 S as the main inhibitor,the average grain size of the primary recrystallization micr... 
2014-02-28 168 5.8

阐述了影响硅钢卷材下料利用率的因素,并结合具体事例利用计算机排样系统进行了详细分析,对提高硅钢卷材的利用率具有一定的指导作用。 It describes the factors influenceing the the utilization ratio of the roll of Silicon steel,and analyzes it in detail combined with concrete examples by a computer arrangement system,which can give a guide for increasing the utilization ratio of the roll of Silicon steel. 
2011-02-28 164 5.8

常化快冷是生产高牌号无取向硅钢和高磁感取向硅钢不可缺少的一个工艺环节,气-雾冷却则是实现常化快冷的关键方式之一。介绍了国内自主设计建设的常化酸洗机组气雾冷却系统的技术特性,并对其特点进行了系统分析,最后给出该系统在设计、运行参数的选择上若干注意事项,对气-雾冷却系统设计和使用具有一定的指导作用。 The normalizing rapid cooling is a indispensable process to high grade non-oriented silicon steel and high magnetic induction oriented silicon steel’ s production. The fog cooling is a key ways of coming true the normalizing rapid cooling. This paper introduces the technical features of the fog cooling system in normalizing pickling line which is the domestic independent design and construction. Meanwhile,the fog cooling system’s characteristic is analyzed systematacially. In the end,this paper ... 
2014-03-28 146 5.8

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