钢厂
电工钢显微结构和疲劳性能的研究
研究了电工钢SXRC的显微结构和疲劳性能,并与DP钢进行了比较。结果表明,退火温度低温化能够有效的抑制电工钢的再结晶。该钢在固溶铌的作用下,能够在保证电机磁性的同时具有一定的强度。与DP钢相比,SXRC钢的抗疲劳性能更好。 The microstructures and fatigue properties of the electrical steel SXRC we re investigated, and the properties were also compared with the steel DP. The results show that the recrystallization of the electrical steel can be suppressed at lower annealing temperature. The steel presents favorable motor magnetic and also a compatible strength with the help of solid-solution Nb. Compared with the steel DP, the fatigue resistance of the steel SXRC is preferable.
奥氏体化温度对高碳含硅钢等温转变的影响
采用XRD物相分析、金相组织观察及TEM精细组织分析研究了奥氏体组织结构状态对Fe-0.88C-1.35Si-1.03Cr-0.43Mn钢中温等温相变鼻温和孕育期的影响,以及不同温度奥氏体化后240℃等温20 min试样的组织结构特征。试验发现,随着奥氏体化温度的升高,中温等温开始转变的鼻温移向更低温度并且相变孕育期缩短;不同温度奥氏体化后同为240℃等温20 min处理,虽然均形成由贝氏体铁素体亚条平行排列构成的束状贝氏体组织,但贝氏体组织的精细结构状态不同,突出的差别在于对应低温奥氏体化贝氏体亚条端部边界具有凸起结构,而对应高温奥氏体化贝氏体亚条端部边界较为平齐且呈现楔形结构。不能简单地以马氏体切变机制认识试验钢中贝氏体组织的形成。 The influence of austenitization temperature on the incubation period and the bainitic phase transformation behaviour in high-carbon silicon steel has been investigated using X-ray diffraction(XRD), optical microscopy and transmission electron microscopy(TEM). The microstructure characteristics of the isothermal transformation(240 ℃, 20 min)products were also studied. It was found that the nose temperature of bainite transformation and incubation period decreased with the increasing austenitizin...
电感耦合等离子体质谱法测定硅钢中痕量铝钼钒钛铌
研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c...
新日铁高强度无取向电工钢的研究进展
针对新日铁公开的相关专利,总结日本高强度无取向电工钢的研究进展,分析了各专利化学成分、生产工艺及产品性能的特点,指出固溶强化、细晶强化、析出强化、位错强化都有可能被用来提高无取向电工钢的强度。在高强度无取向电工钢的研发过程中,需要根据其具体用途确定目标性能,再采用合适的强化手段,从而实现力学性能、磁性能和生产性能之间的平衡。 Authors summarize the research progress of high strength non-oriented electrical steel in Japan by learning related patents brought into the public by Nippon Steel. Authors also analyze the characteristics of the chemical composition, production technology and properties of products in the patents and point out that any ones of solution strengthening method, fine-grain strengthening method, precipitation strengthening method or dislocations strengthening method may be used to improve the strengt...
无取向硅钢夹杂物分析
采用非水溶液电解方法来提取无取向硅钢中夹杂物。通过扫描电镜(SEM)观察结果表明:无取向硅钢中主要夹杂物为六棱柱的AlN、不规则硅酸盐及球状的铁的硫化物和氧化物,其中AlN夹杂尺寸在1~5μm,数量较多,还有部分AlN的复合夹杂。进一步研究了AlN复合夹杂形成机理,采用了Thermo-Calc热力学计算软件计算出该钢样中AlN、MnS析出温度分别为1 240℃、1 200℃,而Al2O3析出温度大于1 800℃,从而为AlN复合夹杂形成机理提供了一个理论依据。 Extracting inclusions from non-oriented silicon steel in non-aqueous electrolysis is a nondestructive method to gain inclusions.Scanning electron microscopy shows that the main inclusions in non-oriented silicon steel were hexagonal AlN,which was of large quantity,irregular silicate,spherical iron sulfide and oxide.The size of AlN inclusions ranged from 1to 5μm,and there were some duplex inclusions of AlN.To further study the formation mechanism of AlN duplex inclusions,Thermo-Calc thermodynamic...
稀土在无取向电工钢中应用的研究进展
稀土元素在许多钢中发挥着独特而且不可替代的重要作用。半个世纪以来,它的作用已经在各种低合金和特殊合金钢中的研究及应用中得到充分的证明;然而,作为具有稀土资源优势的中国,在属于重要功能材料的无取向电工钢中稀土的应用却落后于国外,本文就中国稀土在无取向电工钢中的应用研究作简要的评述,希望能够进一步推进此领域的研究,并且促进中国稀土在无取向电工钢中应用技术的发展,缩短与国外差距,并提出了在此应用领域今后需深入开展的研究方向。 Rare earth elements play a unique and irreplaceable role in a lot of steels,it has given the full proof by the practice of various low alloy steels and special alloy steels since half century.However,as our country has the advantage of rare earth resources,RE application technology in non-oriented electrical steels has lagged behind abroad.The application researches of rare earth in non-oriented electrical steel in our country are briefly reviewed in this paper,which hope to promote the research...
晶粒尺寸对无取向硅钢磁性能影响的主成分回归分析
采用电子背散射衍射技术测定50SW1300冷轧无取向硅钢中不同尺寸范围晶粒的含量,利用主成分回归分析法,综合研究不同尺寸范围晶粒的含量对无取向硅钢磁性能的影响。结果表明:通过主成分回归分析法能够从不同尺寸范围晶粒的含量的多个影响因素中获取主要的因素,定量研究它们对无取向硅钢磁性能的影响规律。分析表明,无取向硅钢的铁损与不同尺寸范围晶粒的含量之间存在着可靠的多元线性关系,在一定范围内,较大尺寸晶粒的含量越多,其对铁损优化的作用越明显;而无取向硅钢的磁感与不同尺寸范围晶粒的含量之间并无线性关系。 Distribution of grain size in cold rolled non-oriented silicon steel 50SW1300 was measured by EBSD.The effects of the distribution of grain size on magnetic properties of the non-oriented silicon steel were comprehensively researched by means of principal component regression method.The results indicate that the main factors influencing the magnetic properties in the distribution of grain sizes,which can be used to guantitative study the magnetlic properies of the steel,are obtained by principal...
硅钢常化炉段工艺特征及问题分析
连续酸洗退火机组(CPAL)对于当前生产高磁感取向硅钢和高牌号无取向硅钢是必不可少的一个环节。常化炉是常化酸洗机组关键的组成部分。本文对国内自主建造的两条退火酸洗机组的工艺流程,特别是常化炉段进行了对比分析。总结出了常化炉的工艺及组成特点,对生产过程中暴露的问题进行了仔细的分析并提出了改进的意见,对于以后新建常化炉具有一定的提示作用。 The continous pickling annealing line(CPAL) is an essential step in producing high magnetic induction grain-oriented silicon steel and high grade non-oriented silicon steel.The normalizing furnace is a very important part of the CAPL.In this paper,the process flows of two CAPL with independent manufacture in our country have been compared,especially the part of normalizing furnaces.The characteristics of process and component are summarized and problems of the normalizing furnace during the prod...
双取向硅钢在制备过程各阶段的织构和微结构
利用X-射线衍射织构分析和线形分析技术测定了交叉轧制双取向硅钢在制备工艺各阶段的织构及微结构,进而探讨了立方织构({100}<001>)的形成过程。通过对实验结果的分析可知,二次冷轧和交叉轧制工艺为立方织构提供了内能优势和有利的形变织构,而低温预退火工艺既强化了立方织构的内能优势,又为立方织构的异常长大提供了有利的组织保证,最终在抑制剂(AlN和MnS)的协同作用下,硅钢在二次再结晶退火后形成了强烈的立方织构。 The texture and substructure of the double oriented electrical steels produced by the cross rolling technology during the difference process has been measured by means of the X-ray texture and diffraction peak profile analysis technology,and research the formation mechanism of cube texture,{100}<001>.The results show that the dominances of inner energy and deformation texture were supplied by secondary cold rolling and the cross rolling technology and strengthened by pre-annealing at a low...
基于GTN损伤模型对含边部缺陷硅钢薄板冷轧时边裂的预测
采用拉伸试验和显微组织观测的方法确定了GTN损伤模型中的9个损伤参数,运用GTN损伤模型对冷轧硅钢薄板边部缺陷的扩展及边裂的产生进行了有限元模拟,并与预置缺口的钢板轧制试验进行对比。结果表明:轧制过程中边部缺陷是造成钢板边部裂纹萌生和扩展的一个重要原因,GTN损伤模型可用来预测含边部缺陷硅钢薄板在冷轧过程中边裂的产生;预测结果与试验结果基本一致。 The crack initiation and propagation of silicon steel strip with edge defect during cold rolling process was studied by using GTN damage model in this paper.Nine damage parameters in GTN model were identified by tensile testing and microstructure observing,and then the FE simulation of edge defect evolution of silicon steel strip during rolling process was conducted on the base of GTN damage model,and then the results were compared with rolling experimental results.The results show that the edge...
中低牌号无取向硅钢冷轧工艺优化生产实践
无取向硅钢特别是中牌号以上的无取向硅钢,随着含硅量的提高,常温下塑性较差,冷轧过程中轧制力明显提高,如果存在原料质量问题,极易发生断带事故,影响硅钢冷轧过程的成材率和生产效率。通过优化冷轧工艺参数,可提高冷轧稳定性。生产中通过合理分配冷轧各道次压下量和轧制速度,保证了轧制过程的稳定,很大程度减少了冷轧断带事故的发生。 Non-oriented silicon steel, especially in the low and middle grade, with the increase of silicon content, plasticity is poor at room temperature, rolling force in cold rolling process significantly improved .If there is the quality defect of raw materials , easily sheet is rolling off. Affect finished product rate and production efficiency in process of cold-rolled silicon steel. Through optimization of cold rolled process parameter , improve the stability of cold-rolling process. Through reason...

