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研究的两种取向硅钢(%:No1-0.042C、3.16Si、0.009Al、0.07Mn、0.50Cu、0.015S、0.0084N和No2-0.040C、3.20Si、0.014Al、0.22Mn、0.49Cu、0.016S、0.008 2N)由50 kg真空感应炉冶炼,锻成(mm)350×120×35板坯,经1 250℃30 min加热,开轧温度1 100℃,5道次热轧成2.3 mm板,终轧温度950~1 000℃。实验结果表明,两热轧板沿板厚方向存在组织和织构的不均匀性,热轧板次表层为再结晶组织,有较强的Goss织构组分;中心层为形变组织,具有典型的形变织构。含0.22%Mn的No2钢次表层{110}〈001〉织构组分比含0.07%Mn的No1钢弱,中心层{001}〈110〉织构组分大大强于0.07%Mn No1钢,导致两者磁性能差异,0.22%Mn No2钢磁感应强度(B800)和铁损(P1.7/50)分别为1.87 T和1.24 W/kg,0.07%Mn No1钢分别为1.88 T和1.18 W/kg。 Studied both grain-oriented silicon steels(%:No1- 0.042C,3.16Si,0.009Al,0.07Mn,0.50Cu, 0.015S,0.0084N and No2-0.040C,3.20Si,0.014Al,0.22Mn,0.49Cu,0.016S,0.0082N) are melted by a 50 kg vacuum induction furnace,forged to(mm) 350×120×35 slab,heated at 1 250℃for 30 min,with beginning rolling temperature 1 100℃hot-rolled to 2.3 mm plate by 5 passes,finishing-rolled at 950~1000℃.Test results show that the structure and texture along thickness of both hot-rolled plates are inhomogeneous:the subsurface ... 
2011-01-28 150 5.8

采用XRD物相分析、金相组织观察及TEM精细组织分析研究了奥氏体组织结构状态对Fe-0.88C-1.35Si-1.03Cr-0.43Mn钢中温等温相变鼻温和孕育期的影响,以及不同温度奥氏体化后240℃等温20 min试样的组织结构特征。试验发现,随着奥氏体化温度的升高,中温等温开始转变的鼻温移向更低温度并且相变孕育期缩短;不同温度奥氏体化后同为240℃等温20 min处理,虽然均形成由贝氏体铁素体亚条平行排列构成的束状贝氏体组织,但贝氏体组织的精细结构状态不同,突出的差别在于对应低温奥氏体化贝氏体亚条端部边界具有凸起结构,而对应高温奥氏体化贝氏体亚条端部边界较为平齐且呈现楔形结构。不能简单地以马氏体切变机制认识试验钢中贝氏体组织的形成。 The influence of austenitization temperature on the incubation period and the bainitic phase transformation behaviour in high-carbon silicon steel has been investigated using X-ray diffraction(XRD), optical microscopy and transmission electron microscopy(TEM). The microstructure characteristics of the isothermal transformation(240 ℃, 20 min)products were also studied. It was found that the nose temperature of bainite transformation and incubation period decreased with the increasing austenitizin... 
2014-07-28 132 5.8

结合工业化生产的无取向硅钢,探讨了氧硫交互作用对钢中夹杂物生成的影响。借助非水溶液电解+扫描电镜法,研究了不同O、S含量下钢中夹杂物的变化规律。结果表明,本实验条件下,提高O含量、降低S含量,会劣化热轧组织再结晶效果。在劣化效果上,O的作用大于S;低Si、无Al硅钢中,应尽可能降低O含量、适当提高S含量,以粗化钢中微细夹杂物,减少尺寸小于1.0μm的夹杂物的数量;O、S含量与钢中夹杂物数量不具有关联性。生产过程中,不仅要严格控制O、S含量,还要严格控制生产工艺,以免生成较多的有害夹杂物。 Based on the industrial production of non-oriented silicon steel,the effects of interaction between oxygen and sulfur on the formation of inclusions were discussed.The change of non-metallic inclusions in steel sheets was investigated by means of electrolysis with non-aqueous solution under different oxygen and sulfur content.Results show that the recrystallization microstructure of hot rolled sheets will be deteriorated with the increase of oxygen content and the decrease of sulfur content.The ... 
2012-04-28 134 5.8

主要研究了氧化锌对以Al(H2PO4)3为基料的无铬无取向硅钢绝缘涂层各项性能的影响.用盐雾实验和动电位极化研究了不同氧化锌含量对硅钢绝缘涂层的耐蚀性和电化学行为的影响.采用SEM和体视显微镜对涂层的表面形貌和附着性能进行研究.结果表明,氧化锌含量为4.0%时,氧化锌能完全中和涂层表面的游离磷酸,涂层的耐蚀性和附着性最好;氧化锌含量过少或过多时,涂层的耐蚀性和附着性都较差. This paper studies the influence of zinc oxide on the performance of chromium-free non-oriented silicon steel insulating coating which based on aluminum dihydrogen phosphate.Salt spray experiment and potentiodynamic polarization were used to study the influence of zinc oxide content on the corrosion resistance and electrochemical behavior of the insulation coating of silicon steel.The surface morphology and adhesion of coating were tested by SEM and stereo microscope.The results show that when t... 
2013-03-28 143 5.8

为研究退火工艺对普通取向硅钢初次再结晶组织的影响,对经不同温度、保温时间和升温速率退火后的材料组织进行了分析。结果表明:在等温退火条件下,加热至600℃时开始发生初次再结晶,800℃以上初次再结晶组织发展完善;而在最终冷轧板直接进行最终高温退火的情况下,加热温度在500~700℃时,将升温速率提高到80℃/h,初次再结晶组织更易于发展完善。 To investigate the influence of annealing process on the recrystallization of common grain oriented silicon steel,microstructures of sheets annealed at different temperature,soaking time and heating rate are observed.Results show that under the condition of isothermal annealing,recrystallization begins at 600℃ and fully develops above 800℃,while in the case that the final cold rolled sheets are directly thrown to final high temperature annealing,recrystallization is likely to develop with the he... 
2014-04-28 147 5.8

利用电子探针面分析、状态分析及电子背散射衍射相分析技术研究硅钢高温氧化铁皮的显微结构。电子探针面分析可以直观的看出元素的分布状态,初步判断氧化铁皮的结构,而状态分析可以准确表征常规氧化铁皮中铁元素的状态,对于合金元素富集区域则通过电子背散射衍射相分析技术来标定。结果表明,高温氧化铁皮的结构主要有4层,即最外层为厚度约为10μm的Fe2O3相,次外层为Fe3O4相,中间层为FeO相上分布有颗粒状的Fe3O4相,最内层为FeO相和Si元素富集的Fe2SiO4相。其中Fe2SiO4层的分布特征与加热温度密切相关:1 100℃时,Fe2SiO4相呈颗粒状,弥散分布在FeO层;1 200℃时,Fe2SiO4相呈液态,侵入基体和疏松的FeO层,且沿着FeO晶界呈网状分布。 The microstructure of high temperature oxide scale on silicon steel was characterized by electron probe microanalyzer(EPMA)mapping analysis,state analysis and electron backscatter diffraction(EBSD)phase analysis.The element distribution and the initial structure of the oxide scale could be detected by EPMA mapping analysis apparently.And the state of iron in the conventional oxide scales could be determined by state analysis.Meanwhile,the alloy-rich region could be identified by EBSD phase analy... 
2014-10-28 169 5.8

采用热模拟方法及EBSD技术,研究Fe-3 wt%Si电工钢在不同温度下组织的动、静态再结晶及晶粒取向特征,特别是少量奥氏体对铁素体动、静态再结晶组织及取向的影响。结果表明,不同温度形变的组织主要分三类:形变长条铁素体、珠光体和等轴细小铁素体。长条形变铁素体内发生动态回复或连续式的动态再结晶,奥氏体周围的铁素体动态再结晶加速,部分以传统的不连续方式动态再结晶。铁素体、奥氏体都可发生静态再结晶。奥氏体的静态再结晶在1050℃以上明显,铁素体的静态再结晶随温度的升高逐渐进行,最显著的再结晶发生在1050℃。不同温度形变的样品,其形变晶粒取向主要以<111>和<100>为主,小等轴铁素体晶粒除与大形变铁素体取向相近外,出现了<110>取向及其它取向。 Static and dynamic recrystallization and grain orientations in a hot-compressed Fe-3 wt% Si electrical steels were studied at different temperatures using Gleeble simulator and EBSD technique,particularly focusing on the effect of small amount of austenite on ferritic microstructure and orientations.The results show that microstructure of the compressed steel,depending on deformation temperature,consisted of elongated and deformed ferrite,pearlite and fine equal-axed ferrite.The elongated ferrit... 
2011-01-28 183 5.8

双辊连铸技术是冶金及材料领域内的一项前沿技术,对于生产高品质硅钢具有独特优势.本实验研究了一种双辊铸轧w[Si]=4.5%的无取向硅钢,考察其铸态和常化处理后样品的组织、织构及析出相尺寸特征.结果表明:铸带组织以与铸带法向成5~20(°)倾角的柱状晶为主,晶内存在少量0.3~0.4μm的AlN析出相,铸带织构以λ(<001>//ND)织构为主,表层织构漫散.950℃/10 min常化处理后,析出相尺寸增大,表层λ织构增强. As an advanced technique of metallurgy and material science,twin- roll strip casting has unique advantages for producing high quality silicon steel. The present study was aimed at a 4. 5% Si non- oriented electrical steel for analyzing the structure,texture and the size of precipitates at the initial and normalized state. The results revealed that the initial structure mainly consisted of columnar grains with 5 ~ 20( °) angle to the normal of cast strip,and some AlN precipitates of 0. 3 ~ 0. 4 μ... 
2014-03-28 137 5.8

采用中、厚板坯生产技术对取向硅钢进行了研制和开发,对热轧及后工序样品进行了金相组织观察和EBSD分析,探讨了两种组织及织构的差异性,研究结果表明:除高温退火样品外,中板坯生产的取向硅钢各工序样品平均晶粒尺寸大;厚板坯生产的取向硅钢热轧和常化样品亚表层Goss织构强;中板坯和厚板坯的脱碳退火板织构没有明显区别。中板坯生产的取向硅钢成本低,产品磁性能和质量与厚板坯相当。 Grain oriented silicon steel was researched and developed by medium thickness slab and thick slab.Microstructures observation and EBSD analysis to the samples of hot rolling and following processes were carried out,respectively.The differences between the two kinds of microstructures and textures were discussed.The results show that the average grain sizes of every process samples are larger except that of high temperature annealing samples of grain oriented silicon steel produced by medium thic... 
2014-03-28 150 5.8

介绍在取向硅钢生产中抑制剂的作用以及多元抑制剂的机理和应用情况,分析多元抑制剂方案中各种元素对高磁感取向硅钢性能的影响,并根据生产实践提出了进一步研究的方向. The role of an inhibitor in the production of grain oriented silicon steel,and the mechanism of multiplex inhibitor in the production are described in the present article.In addition,the influence of various elements in the multiplex inhibitor on the performance of grain oriented silicon steel with high magnetic induction is elucidated.Further work needed in this research is also indicated. 
2013-01-28 136 5.8

本文对某厂硅钢DR510温度、成分及过程控制水平和成品的组织、力学性能进行了研究,并在此基础上提出了工艺优化方案,有一定的借鉴和推广价值。 In this paper,the critical process and the products quality,including temperature,composition and process controlling level,the organization and mechanical properties of the finished product,were studied.On the basis of that the optimized technical plan provided,and this control technology is worth using and spreading. 
2012-05-28 138 5.8

目前随着电工钢用户冲压设备的升级,冲压速度逐步提高,对电工钢产品的硬度和强度指标提出了更高的要求。与普通硬度级别的无取向硅钢相比,高硬度50BW600的Hv硬度提高15~20,达到125以上,同时对电磁性能指标也有较高要求。本钢通过化学成份和热轧及冷轧连退生产工艺的设计,经过小批量生产试验,满足用户要求。通过对工艺的严格控制,在大批量生产过程中,保证了产品的力学性能和电磁性的检验合格率。 Currently with upgrading of stamping equipment of silicon steel user, gradually increasing of stamping speed, propose higher demand for hardness and strength of silicon steel. Compared with conventional 50BW600, high hardness 50BW600 have higher hardness, reach greater than 125Hv. Through design of chemical composition with hot mill and annealing, production test of small quantities, stamping performance meet user request. 
2014-02-28 141 5.8

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