钢厂
电子探针波谱仪定量测定硅钢中硅含量结果的不确定度评定
依据GB/T 15616—2008《金属及合金的电子探针定量分析方法》,采用电子探针波谱仪对某W600硅钢中的硅含量进行了定量测定,对影响其定量测定结果的不确定度分量进行了分析,并对不确定度的各个分量进行了计算和合成,最后给出了硅钢中硅含量测定结果的不确定度报告:该硅钢中的硅含量(质量分数)为1.50%,扩展不确定度U=0.20%,取包含因子k=2。 According to GB/T 15616-2008\"Quantitative Method for Electron Prohe Microanalysis of Metals and Alloys\",the quantitative results of Si content in some W600 silicon steel was measured hy EPMA-WDS.The uncertainty components which might affect the measurement results were considered,calculated and synthesized. Finally the uncertainty result for the quantitative value of Si content in the silicon steel was got.The mass content of Si was 1.50%,and expanded uncertainty U=0.20%under the condition of co...
基于爱泼斯坦方圈组合和损耗加权处理技术的取向电工钢磁性能扩展模拟
提出了一种基于爱泼斯坦方圈族(包括标准25cm爱泼斯坦方圈、缩比的17.5cm和20cm爱泼斯坦方圈)和二级加权处理方法对爱泼斯坦测试数据,包括有效磁路长度、比损耗、励磁功率,进行处理的晶粒取向电工钢磁性能扩展模拟方法。详细地考察了励磁频率、试样剪切角度和环境温度对爱泼斯坦方圈测量结果的影响。研究结果表明,利用本文提出的爱泼斯坦方圈组合以及二级加权处理技术,可以有效地建立取向电工钢损耗模拟模型,从而更加准确地确定了取向电工钢的损耗,改善并提高了爱泼斯坦磁性能测试数据的应用价值。 The extended modeling of the magnetic properties of GO(grain oriented) electrical steel is presented in this paper which is based on a set of standard and scaled-down Epstein frames and a proposed two-level weighted processing of Epstein data, including the mean magnetic path length, specific magnetization loss and exciting power. The effects of excitation frequency, strip angle and ambient temperature on the results obtained from the Epstein frames are investigated. It is shown that using the p...
基于Matlab的硅钢连续退火线纠偏系统分析及仿真
硅钢连续退火线是无取向硅钢生产的成品线。由于受机组布置的影响,带钢经转向辊进出口活套后,当套量达到60%后就出现偏离生产线的情况,从而影响最终产品的质量及成材率,甚至损坏设备。针对某冷轧厂硅钢连续退火机组出口活套入口处带钢跑偏开展纠偏研究,利用Matlab对该纠偏系统进行动态仿真研究,分析系统的稳定性。 Silicon steel continuous annealing line is non oriented silicon steel production of finished product line.Due to the influence of unit layout,strip by roll Import & Export loop,when the set volume reached 60% after the emergence of deviation from the production line,thus affecting the quality of the final product and the rate of finished products,and even damage the equipment.For the export of continuous annealing line in cold rolling silicon steel strip deviation rectification loop at the e...
在动态热处理条件下对取向电工钢二次再结晶的研究
对应用动态加热进行短时温度退火的取向电工钢进行了二次再结晶研究。所进行研究的实验用取向电工钢是经过终冷轧和后续罩式退火后的一条工业化生产线生产的。研究结果表明,运用短时热处理条件可引起研究钢完全的异常晶粒长大。在实验室处理的材料的织构和金相组织与工业化生产的经过终退火而获得的相同的取向电工钢类似。但是,在实验室处理的取向电工钢的二次再结晶的矩阵中可观测到\"寄生\"晶粒。从磁性观点看,这些\"寄生\"晶粒含有不理想的{111}取向织构。 The present study was made to investigate secondary recrystallization in grain-oriented steels annealed at short time temperature exposures with application of dynamical heating.The investigated GO(Grain Oriented) steels for experiments were taken from one industrial line after final cold rolling reduction and subsequent box annealing.It was shown that application of short time heat treatment conditions could lead to complete abnormal grain growth in the investigated GO steel.The texture and mic...
纳米TiO_2轧制液对硅钢冷轧性能的影响
分别采用传统冷轧轧制液和纳米TiO2的冷轧轧制液,对无取向硅钢板进行了四辊冷轧实验.重点研究两种冷轧轧制液的轧制润滑性能和对轧后硅钢薄带表面质量和耐蚀性能的影响.通过场发射电子显微镜和能谱仪对使用两种轧制液轧后得到的硅钢薄带表面形貌和成分进行了分析.给出了轧制液中TiO2纳米粒子在轧制过程中的抗磨减摩机理.在轧制载荷较高时,纳米TiO2轧制液具有优良的轧制润滑性能并能显著改善轧后硅钢薄带的表面质量.同时在高载荷作用下,TiO2纳米粒子被压入硅钢薄带基体,形成一个滑动系来支撑载荷,从而使润滑膜的耐磨性提高. Non-oriented silicon steel strips were rolled on a four-high cold rolling mill lubricated by a traditional cold rolling liquid and a nano-TiO2 cold rolling liquid,with emphasis on studying the rolling lubrication performance of both the liquids and their effect on the surface quality and corrosion resisting property of the silicon steel strips.The surface micrograph and composition of the silicon steel strips after being rolled with both the liquids were characterized by field emissio...
无取向硅钢晶粒长大过程中应力对织构和晶界变化的影响
采用EBSD技术研究了有、无拉应力作用下无取向硅钢在晶粒长大过程中织构转变及晶界变化的规律。结果表明:在晶粒生长期间,无应力作用下的硅钢中,{111}〈112〉,{111}〈110〉织构组分强化,而{100}〈001〉织构组分弱化;与无拉应力作用下的情况相比,施加5MPa的拉应力时,{111}〈112〉,{111}〈110〉织构组分强化的速率下降,{100}〈001〉织构组分变化不明显。对于在晶粒生长期间持续变化的{111}〈112〉,{111}〈110〉和{100}〈001〉织构组分而言,虽然有、无拉应力作用下硅钢的{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率均下降,而{100}〈001〉织构组分的高取向差角度晶界频率则上升,但当有拉应力作用后,{111}〈112〉和{111}〈110〉织构组分的高取向差角度晶界频率下降的速率变小,{100}〈001〉织构组分的高取向差角度晶界频率上升的速率稍有变小。通过对无取向硅钢在晶粒长大过程中织构转变及晶界变化规律的研究,分析了合金原子在晶界的偏聚行为。 The rules of texture and grain boundary transformation in the nonoriented silicon steel under applied stress or without applied stress during grain growth were investigated by EBSD.The results show that the {111}〈112〉 and {111}〈110〉 components in the nonoriented silicon steel without stress are strengthened during grain growth whereas {100}〈001〉 component is weakened,but the growth rate of {111}〈112〉 and {111}〈110〉 component decreases,while the area fraction of {100}〈001〉 component doesn’t chang...
制备{100}织构无取向电工钢方法综述
{100}织构因具有两个易磁化方向能够明显的提高磁性能,因此如何在表面获得具有{100}织构一直是无取向电工钢研究焦点。本文主要介绍了获得{100}织构的主要工艺方法及其基本原理,并结合实际生产过程对各工艺方法的优缺点进行了分析;一方面,优化无取向电工钢的成分,降低碳、锰元素含量以避免脱碳退火和真空退火,简化生产工艺;另一方面,调节升温速度、降温速度和退火气氛,使{100}晶面的表面能或弹性应变能最低,制备具有{100}织构柱状晶组织的无取向电工钢是今后的发展方向。 Because { 100} texture has two easy magnetization directions,which can significantly improve magnetization properfies,how to develop { 100} texture is a focus for researchers and manufactures. In the paper,main manufacturing processes and basic principle are introdued,and their advantages and disadvantages in practical production are analyzed. On the one hand,the production process can be simplified by optimizing chemical compositions,such as reducing the content of C and Mn,which can avoid deca...
硼酸对无铬无取向硅钢涂层性能的影响
研究了硼酸对以Al(H2PO4)3为基料的无铬无取向硅钢绝缘涂层各项性能的影响。用盐雾实验、动电位极化及交流阻抗等试验手段研究了不同硼酸含量对硅钢绝缘涂层的耐蚀性和电化学行为的影响,同时采用SEM对涂层的表面形貌进行了研究。结果表明,硼酸含量为9.7%时,涂层的耐盐雾性及电化学性能最好;硼酸含量过少或过多时,涂层的耐蚀性和电化学性能都较差。 Influence of boric acid on the performance of chromium-free non-oriented silicon steel insulating coating based on aluminum dihydrogen phosphate was investigated.Salt spray experiment,potentiodynamic polarization and electrochemical impedance spectroscopy were used to study the influence of boric acid content on the corrosion resistance and electrochemical behavior of the insulation coating of silicon steel.Surface morphologies of the coatings were tested by SEM.Result shows that when the boric ...
双辊连铸无取向硅钢铸带特征及常化作用研究
双辊连铸技术是冶金及材料领域内的一项前沿技术,对于生产高品质硅钢具有独特优势.本实验研究了一种双辊铸轧w[Si]=4.5%的无取向硅钢,考察其铸态和常化处理后样品的组织、织构及析出相尺寸特征.结果表明:铸带组织以与铸带法向成5~20(°)倾角的柱状晶为主,晶内存在少量0.3~0.4μm的AlN析出相,铸带织构以λ(<001>//ND)织构为主,表层织构漫散.950℃/10 min常化处理后,析出相尺寸增大,表层λ织构增强. As an advanced technique of metallurgy and material science,twin- roll strip casting has unique advantages for producing high quality silicon steel. The present study was aimed at a 4. 5% Si non- oriented electrical steel for analyzing the structure,texture and the size of precipitates at the initial and normalized state. The results revealed that the initial structure mainly consisted of columnar grains with 5 ~ 20( °) angle to the normal of cast strip,and some AlN precipitates of 0. 3 ~ 0. 4 μ...
承钢无取向电工钢CGW800的研发
承钢采用铁水预处理(脱硫)→转炉提钒→转炉冶炼→RH精炼→连铸→轧制工艺,成功研发了无取向电工钢CGW800。试制的CGW800钢碳含量≤0.006 0%、氮含量<0.004 0%,热轧后的金相组织为铁素体和少量渗碳体,晶粒度5.5级,获得了较粗大、均匀的晶粒,钢板的成分和力学性能达到了标准要求。 In Cheng Steel,the CGW800 non- oriented electrical steel is successfully developed with process of hot metal pre- treating,vanadium extracting with converter,smelting with converter,RH refining,continuous casting and rolling. In the steel,the carbon content is not higher than 0. 006 0%,nitrogen less than0. 004 0%,the metallographic structure after hot rolling is ferrite and a little amount of cementite,grain size is 5. 5 degree,relative large and even grain got. The composition and mechanical pr...
陶瓷辊除瘤方法在瑞致电工钢的应用
针对陶瓷辊表面结瘤清除时间长、清除效果差等缺陷,研究正反转陶瓷辊除瘤法,以缩短除瘤时间,增强除瘤效果。 The general removal of ceramic roller surface tumor costs a long time and the effect is poor.This paper probed into the ceramic roller tumor removal in order to shorten time and enhance the effect of eliminating.
硅钢水溶性极厚绝缘涂层的热老化行为研究
对两种硅钢水溶性极厚绝缘涂层进行了不同温度的热老化实验。通过TG-DTA,GDS,FT-IR,SEM和光泽度仪等测试方法对老化的涂层进行分析表征,提出了评估硅钢水溶性极厚绝缘涂层热老化性能的合理温度区间,探讨了涂层热老化行为,并分析了两种涂层热老化性能的差异。结果表明,涂层附着性随着老化时间的延长逐渐下降。FT-IR表征结果显示,热老化过程中,涂料交联形成的化学键未发生断裂,交联剂氨基树脂的三嗪环被破坏是聚合物三维网络结构坍塌的主要原因。 Thermal aging expriments at different temperature were carried out on two types of water-soluble and extra-thick insulation coatings for non-oriented silicon steel,and a series of test methods such as glossmeters,TG-DTA,FT-IR,GDS,SEM were applied in analysis.For evaluating the thermal aging effect of this kind of insulation coating,the proper temperature range was proposed.The difference of aging performance between two coatings was been investigated and the related behaviors were been discussed...

