硅钢资料

依据GB/T 15616—2008《金属及合金的电子探针定量分析方法》,采用电子探针波谱仪对某W600硅钢中的硅含量进行了定量测定,对影响其定量测定结果的不确定度分量进行了分析,并对不确定度的各个分量进行了计算和合成,最后给出了硅钢中硅含量测定结果的不确定度报告:该硅钢中的硅含量(质量分数)为1.50%,扩展不确定度U=0.20%,取包含因子k=2。 According to GB/T 15616-2008\"Quantitative Method for Electron Prohe Microanalysis of Metals and Alloys\",the quantitative results of Si content in some W600 silicon steel was measured hy EPMA-WDS.The uncertainty components which might affect the measurement results were considered,calculated and synthesized. Finally the uncertainty result for the quantitative value of Si content in the silicon steel was got.The mass content of Si was 1.50%,and expanded uncertainty U=0.20%under the condition of co... 

采用扫描电镜、原子力显微镜研究了铬酸镁半无机绝缘涂层的微观结构。结果表明,涂层厚度为数微米,涂层中的有机树脂乳液颗粒均匀分布在无机涂层的表面,从而保证了涂层具有良好的冲片性能。采用极化曲线研究了涂层的耐蚀性能,发现铬酸镁与铬酸锌绝缘涂层的耐蚀性能相当。 In this paper,the microstructure and anti-corrosion property of magnesium chromate coating on non-oriented silicon steel were studied.The microstructure was observed by SEM and AFM.The anti-corrosion properties were evaluated by polarization curves.The results show that the thickness of coating is several microns and the polymer particles were scattered on the surface of inorganic coating,which is the guarantee for lamination property.The corrosion resistance of the magnesium chromate film was e... 

采用RH精炼添加钙合金方式对硅钢进行钙处理,结果表明,钙合金添加量为0.67、1.00和1.67 kg/t钢时,钢中Ca含量分别为0、2×10-6和4×10-(6质量分数);随着钙合金添加量的增加,钢中夹杂物粒度逐渐由0～2μm向2～4μm、4～6μm偏移;不同钙处理条件下,钢中均存在粒径小于1μm和粒径为1～5μm的MnS、CuxS夹杂物,后者或单独存在,或与AlN、CaS夹杂复合;钢中粒径为5～10μm的夹杂物基本以Ca的氧化物和硫化物为主。与未经钙处理的炉次相比,钙合金添加量为0.67、1.00和1.67 kg/t钢时,粒径小于1.0μm的夹杂物减少幅度分别为68.06%、87.50%和94.94%。钙合金添加量为1.67 kg/t钢时,可以去除钢中绝大部分的微细夹杂物。 In order to improve the properties of final silicon steels,the calcium treatment was adopted by adding Ca alloys into the liquid steel during the RH refining process.Results show that when the addition of Ca alloys is 0.67 kg/t,1.00 kg/t and 1.67 kg/t,the corresponding Ca content in silicon steels is 0,2 × 10-6 and 4 × 10-6 respectively.With the increase of Ca alloy addition,the particle sizes of inclusions in steels become 2～4 μm and 4～6 μm,from 0～2 μm.Under different calcium treatments,there e... 

研究了铝和铬元素在无取向电工钢晶粒长大过程中对织构及晶界变化的影响规律。试验结果表明:电工钢在晶粒长大过程中的主要织构组分均为{111}<112>。在晶粒生长期间,不加铝的1号试样中,{111}<112>、{111}<110>织构组分强化,而{100}<001>织构组分弱化;与1号试样相比,在加入0.2%的铝(质量分数,下同)的2号试样中,{111}<112>、{111}<110>织构组分强化(增加)的速率下降,{100}<001>织构组分变化不明显,甚至稍有增加。在含铝的试样中再加入0.3 5%的铬之后(3号试样),{111}<112>{、111}<110>和{100}<001>织构组分的变化规律与1号试样相似,但当电工钢中加入0.72%的铬之后(4号试样),上述3种织构组分的变化规律与2号试样相似。对于在晶粒生长期间持续变化的3种织构组分而言,1号试样的{1 1 1}<112>和{111}<110>织构组分的高(低)取向差角度晶界频率下降(... The effect rule of Aluminm and Chromium on texture and grain boundary transformation in the nonoriented electrical steel during grain growth was investigated.The experimental result shows that the main texture component is {111}<112> in the electrical steel.The {111}<112> and {111}<110> components in specimen 1 without Alumium were strengthened during grain growth whereas {100}<001> component was weakened.But the growth rate of {111}<112> and {111}<110> compon... 

本文对某厂硅钢DR510温度、成分及过程控制水平和成品的组织、力学性能进行了研究,并在此基础上提出了工艺优化方案,有一定的借鉴和推广价值。 In this paper,the critical process and the products quality,including temperature,composition and process controlling level,the organization and mechanical properties of the finished product,were studied.On the basis of that the optimized technical plan provided,and this control technology is worth using and spreading. 

以试验室模拟CSP工艺生产的Fe-3Si热轧钢带为研究对象,采用正交试验及方差分析的方法,研究了取向硅钢初次再结晶退火工艺对高温退火后获得锋锐的高斯织构的影响。结果表明:取向硅钢两段式初次再结晶脱碳退火工艺参数加热段保温时间及加热温度是高温退火后获得锋锐高斯织构的主要影响因素,其可信度分别在90%和85%以上;在本试验条件下,通过正交试验获得的最佳退火工艺为:冷硬板经600℃保温3 min和850℃保温6 min。 Fe-3Si hot rolled strip was produced by simulating CSP technology in the laboratory.Orthogonal experiment and analysis of variance were carried out to investigate the influence of primary recrystallization on the sharp Goss texture of the oriented silicon steel.The results show that holding time of the heating section and the heating temperature for a sharp Goss texture of the samples annealed has important implications in this experiment conditions,the two-step decarburization annealing process... 

采用XRD、SEM和激光粒度仪等手段,观察并研究了不同特性氧化镁在硅钢表面形成硅酸镁底层形貌特点,并结合热力学和差热-失重分析了MgO-SiO2的反应机理。研究结果表明:粒度小,活性值高的特种氧化镁在高温退火过程中与基体表面氧化物生成的硅酸镁底层,界面中硅酸镁底层嵌入基体较多,表面致密,颗粒细小,有利于形成附着性能优良的硅酸镁底层。 Surface microstructure of Mg2SiO4 coatings formed on the surface of oriented silicon steel coated with different kinds of MgO was investigated by XRD and SEM.The reaction mechanism between MgO and SiO2 was analyzed by TG-DSC and thermodynamic calculation.Results revealed that when the MgO with finer microstructure size and higher activity is employed,a dense Mg2SiO4 layer with finer microstructure and good binding to the steel substrate can be obtained.The results are very helpful for the prepar... 

承钢采用铁水预处理(脱硫)→转炉提钒→转炉冶炼→RH精炼→连铸→轧制工艺,成功研发了无取向电工钢CGW800。试制的CGW800钢碳含量≤0.006 0%、氮含量<0.004 0%,热轧后的金相组织为铁素体和少量渗碳体,晶粒度5.5级,获得了较粗大、均匀的晶粒,钢板的成分和力学性能达到了标准要求。 In Cheng Steel,the CGW800 non- oriented electrical steel is successfully developed with process of hot metal pre- treating,vanadium extracting with converter,smelting with converter,RH refining,continuous casting and rolling. In the steel,the carbon content is not higher than 0. 006 0%,nitrogen less than0. 004 0%,the metallographic structure after hot rolling is ferrite and a little amount of cementite,grain size is 5. 5 degree,relative large and even grain got. The composition and mechanical pr... 

含铜抑制剂作为取向硅钢的主抑制剂或辅助抑制剂不仅可以抑制初次晶粒的长大,促进二次再结晶,还可以降低铸坯的加热温度。取向硅钢中主要抑制剂为10～50 nm Cu₂S,在钢的铸坯、热轧、冷轧、脱碳等工艺过程均可析出;（Cu,Mn）_1.8S、Cu_1.8S、ε-Cu等主要作为辅助抑制剂,尺寸一般为30～50 nm（或大于50 nm）,主要在热轧阶段析出。总结了国内外有关取向硅钢中含铜抑制剂析出行为的研究进展,当前主要研究不同生产流程和工序中含铜抑制剂的析出行为和作用机理。 As main inhibitor or auxiliary inhibitor for grain-oriented silicon steel,the particles of inhibitor bearing copper not only inhibit the primary crystal growing and promote the secondary recrystallization,but also decrease the heat temperature of casting slab.The main inhibitor for grain-oriented silicon steel is 10～50 nm Cu₂S,which precipitate in process and procedure including steel casting slab,hot rolling,cold rolling and decarburizing process,while the 30～50 nm or more than 50 nm... 

采用X-射线衍射分析技术测定了取向硅钢热轧板在不同压下率下不同厚度处的织构。结果表明,在压下率低于80%的情况下,几乎所有试样的不同厚度处的织构均为旋转立方织构类型{100}<011>,但不同压下率、不同厚度处的织构强度存在很大差异;在压下率大于80%的情况下,不同试样的不同厚度处的织构类型发生了变化,其织构类型为旋转立方织构或高斯织构{011}<100>,且当织构类型为旋转立方织构时,织构强度存在很大差异,而当织构类型为高斯织构时,织构强度差异相对较小。 The texture of the grain oriented silicon steel hot rolled plate at different compressibility has been measured.The experimental results have shown that the texture of all samples at different thickness is {100}<011> when the compressibility is below 80%,and its intensity at different compressibility and thickness is difference.The texture of all samples at different thickness is variable when the compressibility is above 80%,it is {100}<011> or {011}<100>,and the intensity of ... 

通过对辉光放电发射光谱参数的优化,以铁元素为内标来消除基体效应,建立了测定硅钢薄板中微量硼元素的方法。优化的实验参数为:放电电压1200 V,放电电流50 mA,预溅射时间40 s,积分时间10 s。校准曲线硼元素含量范围0.0001%~0.022%,相关系数大于0.999,测量结果与认定值一致,相对标准偏差小于10%。完全能够满足日常分析测试的要求。 A glow discharge optical emission spectrometry(GD-OES) method for determining trace boron element in silicon steel sheets were established through optimization of instrumental parameters and using Fe element as an internal standard to eliminate the matrix effect.The optimized instrumental parameters included discharge voltage,discharge current,pre-sputtering time and integration time,which are 1200 V,50 mA,40 s,and 10 s,respectively.The content of boron element that can be determined from the ca... 

针对传统工艺生产硅钢周期长、能耗大等缺点,采用双辊连铸工艺制备3%Si无取向硅钢连铸薄带,利用MEM,SEM和TEM观察了铸带的组织、织构及析出物,同时对比了Al的质量分数为0.6%和0.9%的连铸薄带在组织、织构及析出物特征方面的异同.结果表明:双辊连铸工艺生产的3%Si无取向硅钢铸带的组织为均匀等轴晶粒,平均晶粒尺寸约为300μm;织构组成随Al质量分数的不同具有明显差别,Al质量分数为0.9%的铸带中{100}织构强度是随机织构的7倍;铸带中的析出物为AlN和MnS,最大尺寸分别为500和50 nm左右. Given the lengthy production cycle,high energy consumption,and other shortcomings of the traditional process for producing silicon steel,a twin-roll casting process was used to produce 3%Si non-oriented silicon steel casting strips. MEM,SEM,and TEM were used to compare micro-structure,texture,and precipitate characteristics of a casting strip containing 0.6%Al with another containing 0.9%Al.The structure of 3%Si non-oriented silicon steel produced by the twin-roll casting process was a uniform i...