硅钢资料

以青海盐湖水氯镁石为初级原料,采用喷雾热解法制备原料氧化镁,原料氧化镁通过水化制备硅钢级氧化镁前驱体氢氧化镁。原料氧化镁水化实验中对水化剂、水化温度、水化时间、液固比、搅拌速度及陈化时间对水化率、过滤速度和纯度的影响进行系统研究。采用均匀实验设计和DPS数据处理,(依次)通过建模分析、二次多项式模型回归建立数学模型,再通过各因素方差分析和总方差分析,确定了理论最优实验条件,再用理论最优条件作重复实验进行验证,最终确定了原料氧化镁的最佳水化条件。在水化温度60℃,水化时间105 min,液固比4,陈化时间4 h,水化剂1含量4.0%,水化剂2含量3.15%,洗水量4倍,搅拌速度120 r/min时,原料氧化镁的水化率达99.50%以上,得到的硅钢级氧化镁前驱体氢氧化镁纯度高、过滤性能良好。 By spray pyrolysis method,bischofite in Qinghai salt Lake,as primary raw material,was used to prepare precursor raw material MgO for silicon-steel MgO.The precursor raw material MgO was used for preparing Mg(OH)2 which was the precursor of silicon-steel MgO,by hydration method.In the hydration experiment of precursor raw material MgO,some experiment parameters were investigated systematically.such as the hydrated agent,the temperature and time of hydration,liquid/solid ratio that affected the hy... 

【作者】 康凌晨； 王丽娜； ...

采用铸坯低倍组织检验和化学分析的方法,研究板坯连铸机二冷区电磁搅拌器电流和频率参数对无取向电工钢XG800WR板坯中心偏析和等轴晶率的影响,结果表明:铸坯等轴晶率随着搅拌器电流强度和电流频率的增大而增加。采用二冷区电磁搅拌可减小中心易偏析元素S的偏析,试验得出:减小铸坯S偏析效果最好的电磁搅拌参数为电流380～400A,频率6Hz。 The effect of electromagnetic stirring current and frequency parameter at secondary cooling area on the central segregation and equiaxed crystal ratio of XG800WR non - oriented electrical steels slab was investigated through the methods of chemical and macrostructure analysis.The results shows that the rate of equiaxed crystal zone is going up with increasing of current intensity and current frequency.Electromagnetic stirring in the secondary cooling area can be easily reduced segregation caused... 

承钢采用铁水预处理(脱硫)→转炉提钒→转炉冶炼→RH精炼→连铸→轧制工艺,成功研发了无取向电工钢CGW800。试制的CGW800钢碳含量≤0.006 0%、氮含量<0.004 0%,热轧后的金相组织为铁素体和少量渗碳体,晶粒度5.5级,获得了较粗大、均匀的晶粒,钢板的成分和力学性能达到了标准要求。 In Cheng Steel,the CGW800 non- oriented electrical steel is successfully developed with process of hot metal pre- treating,vanadium extracting with converter,smelting with converter,RH refining,continuous casting and rolling. In the steel,the carbon content is not higher than 0. 006 0%,nitrogen less than0. 004 0%,the metallographic structure after hot rolling is ferrite and a little amount of cementite,grain size is 5. 5 degree,relative large and even grain got. The composition and mechanical pr... 

西安重型机械研究所为武钢开发了目前国内第一台自动化水平较高的先进可靠的硅钢热轧试验轧机。本文介绍了该轧机的工艺参数、设备组成,技术特点及轧制流程,该轧机在规定的终轧温度范围内,实现了2.5 m/s的快速轧制速度,保证了控制系统准确及时的采集到轧件进出轧辊时的信号,缩短道次间隙时间,实现了自动控制,保证了产品板形及精度的高水平要求,对于硅钢尤其是对其取向硅钢新产品、新工艺的开发具有深远意义。 An experimental prototype of 400 mm silicon steel hot rolling mill was developed by Xi’an Heavy Machinery Research Institue for Wu Gang.The technological parameters,configuration and characteristic of advanced control system in the experimental prototype are introduced in detail.The experimental prototype was realized the fast rolling of 2.5 m/s in the range of specified rolling temperature.Its automatic rolling control system can acquisite the signals that a rolled piece enters in and exits fro... 

借助OM、激光共聚焦显微镜、质谱仪和电解萃取等设备和方法，研究了添加微量稀土La（质量分数0.001 1%）的取向硅钢在轧制前采用不同加热保温时间对抑制剂固溶行为的影响。结果表明：当稀土取向硅钢在1 250℃分别保温10、20、30 min后，试验钢晶粒尺寸随保温时间延长有先快后慢的长大趋势；三种抑制剂元素Mn、Cu和Al均发生固溶，保温时间对Mn和Cu两种元素的固溶影响明显，固溶量分别由69.8%和43.7%增加至84.2%和85.2%；随着保温时间的延长，稀土取向硅钢中抑制剂的小尺寸未溶物逐渐减少直至消失，较大尺寸未溶物（300～600 nm）逐渐转变为小尺寸未溶物逐步溶入基体中，数量减少且未溶物的类型由复杂逐渐转变为单一。 In this paper the solid solution behavior of the inhibitor under various holding time in 0.001 1 %La oriented silicon steel during reheating had been investigated by using OM, LM, methods of electrolytic extraction and mass spectrometer. The results showed that grain size of the test steel increased significantly with the holding time prolonging when the rare earth oriented silicon steel was heated to1 250 ℃ and held for 10, 20 min and 30 min respectively, and the growth trend slowed down after ... 

【作者】 朱一知； 高军军； ...

利用加热炉模拟、动态再结晶以及热模拟等试验方法以及扫描电镜、金相显微镜等分析观察手段对无取向硅钢边裂的成因进行了探讨。结果表明,长时间加热使得板坯边部晶粒异常长大,晶界氧化并脱碳,轧制过程中边部温度过低,动态再结晶过程变弱,使得板坯边部延伸性能变差,是导致硅钢边裂的主要原因。建议通过适当降低铸坯加热温度、缩短保温时间、提高终轧温度来改善硅钢边裂缺陷。 The behaviors of high temperature oxidation,dynamic recrystallization,and hot ductility,microstructure evolution were investigated on the non-oriented electrical steel sheets to discuss the formation of edge crack.The key causes of cracking was found to be the coarse as-cast microstructure,grain boundary oxidation and decarburization in reheating furnace,as well as reduced temperature at strip edge region during hot rolling process resulting in reduced hot ductility and lack of enough dynamic re... 

为了解决在纹理背景下冷轧硅钢表面缺陷的分割问题,提出了基于局部信息结构张量和活动轮廓模型的硅钢表面缺陷分割方法。将图像的局部信息引入到结构张量中;在结构张量提取的特征空间中,以KL距离作为区域的概率密度相似性度量建立分割图像的活动轮廓模型;采用Split-Bregman数值解法对模型进行求解。运用提出的分割方法对硅钢表面的一些常见缺陷如纵向划伤、横向划伤、异物和孔洞等进行分割实验。实验结果表明,该方法可以准确地分割出硅钢表面缺陷区域,验证了该方法的有效性。 In order to address the segmentation problem for cold rolled silicon steel surface defect based on the texture background,a novel method based on structure tensor and active contour model is proposed.Image local information is introduced to the structure tensor.In the extracted feature space of structure tensor,KL distance is treated as a regional similarity measure of the probability density to establish active contour model for image segmentation.The numerical solution of Split-Bregman is used... 

利用光学显微镜（OM）和扫描电镜（SEM）研究了不同稀土Ce含量的50W470无取向硅钢的铸坯、热轧板和冷轧退火板的宏观和微观组织，并采用磁性能测试仪测定其磁性能。结果表明：当稀土Ce的加入量从0增加到66×10^-6（质量分数）时，铸坯的柱状晶平均宽度从3.82 mm减小到3.24 mm,等轴晶率从43.1%增加到51.3%;热轧板的平均晶粒尺寸逐渐增加，从26.2μm增加到33.3μm,再结晶百分数从24%增加到37%;退火板的平均晶粒尺寸从36.2μm增加到39.3μm;磁性能测试表明，微观组织的变化有利于50W470无取向硅钢铁损降低和磁感提高。 Macro-structure and microstructure of as-cast plate, hot rolled plate and cold rolled annealed plate of 50 W470 non-oriented silicon steel with different rare earth Ce content was studied by optical microscope（OM） and scanning electron microscopy（SEM）, and their magnetic properties were measured by magnetic property tester. The results show that when the addition amount of rare earth Ce increases from 0 to 66×10^-6（mass fraction）, the average width of columnar crystal of the as-cast pl... 

以质量分数为25%的丙烯酸乳液MC-102、15%Al(H2PO4)3溶液、0.01%H3BO3、0.01%Zn(Ac)2·2H2O和2%二乙二醇丁醚组分,在不同固化工艺下制备涂层。极化曲线和电导率测试发现300℃处理60 s得到的涂层具有良好的耐腐蚀性和绝缘性;水煮实验证明该涂层具有良好的耐水性;断口线扫描发现涂层具有良好的附着性。 A formula comprising MC-102 acrylic emulsion 25%,aluminium dihydrogen phosphate15%,boric acid 0. 01%,zinc acetate dihydrate 0. 01% and diethylene glycol monobutyl ether 2% was used to prepare coatings via different treatment process. The conductivity test and polarization curves revealed that a coating cured at 300 ℃ for 60 s showed good insulative and anticorrosive properties. The water boiling test indicated that the said coating had good water resistance. A cross section of the coating was in... 

通过Axio Imager金相显微镜考察4.5%~7.0%硅(质量分数)对高硅钢材料组织形貌的影响,并利用Fe-6.5%Si高硅钢薄板制备方法对其进行轧制,通过DDL50电子万能试验机对阶段产品进行力学性能测试。结果证明,硅含量为5.58%的高硅钢在实验硅含量区间内存在最大延伸率及最小铸态组织晶粒尺寸。 An investigation about the influence of 4.5%-7.0% Si on microstructure and mechanical properties of high-silicon steel was presented.SEM was adopted to take an observation towards microstructure during fabrication,and DDL50electronic universal testing machine was applied into the detection of tensile curves.The results show that silicon steel with 5.58% Si provides the maximum elongation and minimum grain size as cast.