硅钢资料

为了确定普通冷轧取向硅钢最优的中间完全脱碳退火工艺,在其一次冷轧后进行5种不同工艺的脱碳退火处理,借助扫描电镜及电子背散射衍射技术研究了不同工艺脱碳退火后的组织、织构和脱碳效果。结果表明:经5种工艺脱碳退火处理后,初次再结晶的平均晶粒尺寸均约为19μm,且不随退火温度和时间的变化而变化;经840℃×10min工艺退火后的晶粒最均匀,高斯织构位向更准确,高斯织构面积分数最多,为3.1%,可将碳脱至0.003 5%。 In order to determine the optimal intermediate complete decarburizing annealing processes for common grain-oriented(CGO)silicon steel,five kinds of intermediate decarburizing annealing processes were conducted,the microstructure,texture and decarbonization after different decarburizing annealing processes were studied by scanning electron microscopy and electro back-scattered diffraction(EBSD)technology.The results show that the average grains sizes of primary recrystallization were about 19μm a... 

【作者】 杨佳直； ...

某冷连轧机生产无取向硅钢板材时,其边缘降的长度合格率频繁超标。为满足用户的叠片厚度精度要求,这类产品必须以增大切边量的方式来保证交货质量,而这种方式又直接降低了金属收得率,提高了生产成本。基于此,以该产线现有设备特性为基础,详细分析其软、硬件功能模式,分别对辊形与反馈控制进行全面分析与优化改进。通过现场试验论证,充分明确依托辊形优化与反馈控制程序的改进能显著提高边缘降的控制水平,该技术的使用为生产现场的边缘降控制提供了合理的技术支撑。 A cold rolling mill production of non-oriented silicon steel sheet,the thickness difference of the edge( edge-drop) is usually exceed the preset standard value,In order to meet the accuracy requirements of the user flatness,these production must be trimed wider length to meet the delivery quality of the user need, which directly reduce the metal yield and increase the manufacturing cost. Therefor,the software and hardware of the production line has been analyzed, and the work roll shape and feed... 

运用EBSD和光学显微镜,研究了0.25%~0.45%Cu对无取向电工钢热轧板显微组织,成品板显微组织、织构和磁性能的影响。实验结果表明:卷取过程中Cu元素在热轧板表层的偏聚作用显著阻碍了热轧板表层再结晶晶粒长大,导致热轧板表层晶粒尺寸随着Cu含量增加而逐渐较小,但热轧板中间晶粒尺寸变化不大。同时发现Cu元素能够明显改善织构类型,使有利织构组分增加,不利织构组分减少,同时减弱织构强度。从实验结果可知0.35%Cu能够显著改善电工钢的磁性能,铁损P15/50最低达到4.1 W/kg,磁感B50最高值达到1.8 T。 Effects of high content Cu on microstructure of hot rolled plates and microstructure,texture and magnetic properties of annealed finish product plates of non-oriented electrical steel were examined by means of EBSD technique and optical microscope. The results show that surface segregation of Cu significantly hindered recrystallized grain growth of surface layer in hot rolled plate during the coiling,as a result,the surface grain sizes of the hot-rohed plates decrease with the increase of Cu con... 

为进行磷酸盐系无铬无取向硅钢涂层烧结固化工艺研究,首先对磷酸盐系无铬无取向硅钢涂层进行热重-差示扫描量热(TG-DSC)分析;然后在不同烧结固化温度条件下,测定涂层板温随时间变化曲线;最终获得涂层烧结固化温度与时间(T-t)工艺曲线。通过中性盐雾试验、动电位极化、交流阻抗、涂层附着力以及扫描电子显微镜(SEM)和能谱(EDS)分析验证。结果表明,根据涂层烧结固化温度与时间(T-t)工艺曲线制备的涂层结构致密、性能优异,证明该工艺曲线具有合理性与正确性。 In order to study the curing process of chromium-free non-oriented silicon steel coatings,phosphatic chromium-free non-oriented silicon steel insulating coating was prepared and TG-DSC analysis of the coating was conducted,then the change of the actual temperature of the coated non-oriented silicon steel sheet with time at different curing temperatures was studied. Based on the experiments,the processing curves of curing temperature vs. curing time( T-t) for the chromium-free non-oriented silico... 

为了消除硅钢在连续退火机组产生的浪形缺陷,对浪形缺陷产生的主要原因进行了分析。制定了相应控制措施,对炉内带钢张力、冷却段输出、碳套辊与带钢的同步性、无氧化炉燃烧状态等参数进行了调整;在生产组织上安排高低牌号宽窄规格穿插生产、定期更换碳套辊等,实施后效果明显。 The main cause leading to waviness defects of silicon steel is analyzed in order to eliminate the waviness defects of silicon steel in continuous annealing line.And thus corresponding measures for controlling these defects are made by means of adjusting these parameters such as the tension of silicon steel coils in continuous annealing furnace,the output in cooling section and the combusting condition of the non-oxidation furnace as well as keeping the synchronization between carbon sleeved roll... 

针对硅钢连续生产线设备存在的故障、隐患以及精度等影响产品质量的问题进行分析及改造,实现保证生产线设备稳定运行、提高设备精度及硅钢产品质量的目的。 This paper analyzes and transforms the electrical equipment failures, risks existed in slicon continuous production line, and the effect of accuracy to product quality, in order to ensure stable operation of equipment in production line and improve the accuracy of device, quality of silicon. 

【作者】 党其； ...

【作者】 陈迪安； 李春生； ...

利用背散射衍射技术(EBSD)和XRD,研究了两段式脱碳退火工艺对取向硅钢纵截面初次再结晶的微区取向、取向差分布、特殊晶界(CSL)及高温退火试样高斯织构。分析了初次再结晶晶界特征对取向硅钢高温退火后宏观织构的影响。结果表明:初次再结晶的纵截面基体中Σ3和Σ5晶界使得高斯晶粒有着较高的迁移率,在高温退火时借助20o～45°的大角度晶界的界面能吞并周围{111}<112>晶粒迅速长大,形成密度水平较高的高斯织构。 Micro area orientation of primary recrystallization,the misorientation distribution,special boundaries under different two-stage decarburization annealing and the Goss texture under high temperature annealing the longitudinal section of grain-oriented silicon steel were detected by electron back scattering diffraction(EBSD) and X-ray diffraction(XRD).The effect of primary recrystallization grain boundary on macrotexture after high temperature annealing was analyzed.The results show that the Σ3 a... 

为了解决目前冷轧产线硅钢现有切边技术存在的微裂纹、应力、毛刺和边浪等问题,采用光纤激光器进行了高速切割实验,对激光功率、切割速度、激光模式等影响因素进行了分析,同时对高速切割时的切割前沿形状进行了研究。结果表明,切割最高速度随着功率的增加而增加;随着离焦量的增加,切割质量下降,挂渣增多,切缝宽度增加,切割深度变浅;基模激光器能量密度更高,所以薄板切割时的切割速度高于多模激光器;切割前沿随着切割速度的增加会变得平缓,速度足够大时,切割前沿甚至接近与切割方向平行,此时切缝下部存在挂渣现象。 In order to solve the problems such as micro crack,stress,burr,edge waves and so on,existing in cold rolling production line of silicon steel side cutting,experimentsof high speed laser cutting using fiber laser were carried out.Laser power,cutting speed,laser mode and other factors were analyzed,at the same time,cutting front geometries were studied.The results show that the maximum speed increases with power.And the increases of defocus result in poor quality,wider kerf and shallowerkerf.Energ... 

为了确保硅钢铬酸盐涂料的环保性,需要严格控制涂料的固化工艺,保证涂料固化过程中涂料中的六价铬充分转化为三价铬。对涂料及原料进行热重分析(TG)及差示扫描量热法分析(DSC)。结果表明,MgO与铬酐混合转化为MgCrO4,使六价铬稳定性增强,其中大部分Cr6+转变为Cr3+发生在620~700℃,在450~500℃高于铬酐发生大量失重,因此必须加入还原剂保证涂料中六价铬被充分还原;超过360℃后树脂会发生分解,因此实际板温不能超过360℃;加入了还原剂的整体涂料的失重温度区间主要在260~320℃,因此涂料固化时钢板的实际温度最佳区间为320~360℃。 Because of the silicon steel chromate coating’s environmental requirements,the paint curing process must be controlled strictly to ensure all Cr( Ⅵ) transforms to Cr( Ⅲ). The TG and DSC analyses of the paint are studied. The reaction of MgO and CrO3 would generate MgCrO4,enhancing the stability of Cr( Ⅵ). The most r( Ⅵ) in MgCrO4 changes to Cr( Ⅲ) at 620-700 ℃,while the CrO3 has a large weight loss at 450-500 ℃. The reductant must be added in the paint to make sure the Cr( Ⅵ) could transform suf...