硅钢资料

试验研究了0.3 mm取向硅钢冷轧板(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005A1)的退火温度(760~880℃7 min)和退火时间(820℃3~9 min)对该钢的晶粒尺寸,再结晶和织构的影响。结果表明,最佳初次再结晶退火工艺为820℃5 min,该钢的平均晶粒尺寸为14.20μm,完全再结晶率为92%,不利{111}<110>结构含量为3.16%,有利织构{111}<112>,{012}<001>和高斯织构含量分别0.40%,4.73%和2.46%。 The effect of annealing temperature(at 760 ~ 880 X.for 7 min) and time(at 820℃ for 3~9 min) on grain size,recrystallization rate and texture of 0.3 mm cold-rolled sheet of oriented silicon steel(/%:0.046C,3.07Si,0.09Mn,0.029P,0.004S,0.005Al) has been tested and studied.Results show that with optimum recrystallized annealing at 820℃ for 5 min,the silicon steel average grain size is 14.20 fun,the complete recrystaUization rate is 92%,the unfavourable-texture {111}< 110 > content in steel is ... 

采用双辊薄带连铸工艺试制了2.6 mm厚5.28%Si-1.11%Al高硅钢薄带,对比了1050℃×5 min正火及不正火铸带280℃冷轧至0.5 mm后,再经900～1100℃退火的磁性能。结果表明,高硅钢铸带显微组织为等轴晶组织,正火后铸带边部晶粒长大,中心层晶粒变化较小。成品中析出物主要为较粗大的AlN和AlN+MnS复合析出物,尺寸为0.5～2.5μm。与不正火试样相比,正火试样成品铁损大幅降低,磁感小幅下降;随退火温度的升高,两种工艺下铁损和磁感都是先降低后升高,在1050℃出现最低值。 2.6 mm thickness 5.28% Si-1.11% Al non-oriented high silicon steel was produced by twin roll thin strip casting.Magnetic property of the strip un-normalized and normalized at 1050 ℃×5 min was contrasted after cold rolled to 0.5 mm at 280 ℃ and 900-1100 ℃ final annealing.The results show that microstructure of the strip is equiaxed crystal.The surface grain is coarsened and the center layer grain has little change of the normalized strip.The main precipitates are AlN and MnS+AlN with 0.5-2.5 μm s... 

【摘要】 <正>日前,宝钢自主研发的新型高磁感取向...

采用双辊薄带连铸技术试制了3.98%Si-0.71%Al无取向硅钢铸带,研究了二次冷轧法对硅钢组织和磁性能的影响。结果表明:硅钢铸带显微组织为等轴晶组织,铸带再结晶较完全,常化对铸带显微组织影响较小。二次冷轧工艺和一次冷轧工艺下,最终退火后成品显微组织为等轴晶组织,二次冷轧法最终退火后的晶粒尺寸小于一次冷轧法。二次冷轧法能够提高成品磁性能. Effect of double cold rolling on magnetic properties and microstructure of 3.98%Si-0.71%Al non-oriented silicon Steel Sheets cast by twin-roll thin strip casting process were investigated.The results show that the structure of the thin strip is equiaxed crystal,the recrystallization is complete and normalizing has lesser effect on microstructure.Using both cold rolled and double cold rolled process,the microstructure is equiaxed grain after final annealing.The average grain size of annealed shee... 

对西昌钢钒炼钢厂200 t BOF(顶底复吹)-RH-CC工艺生产50PRW800无取向硅钢RH精炼过程中主要成份进行了分析。找出了目前工艺中影响钢液质量的主要因素是钢水脱氧处理不彻底,造成加入的部分硅元素烧损。操作工艺改为铝的脱氧即合金化操作一步完成,保证了钢水中氧处于一个较低的范围,从而减少对硅元素的烧损,提高合金收得率。 The factors of BOF-RH-CC process affecting the compositions of liquid steel were systematically investigated and studied of Xichang Steel and Vanadium Company. The main factors affecting the steel cleanliness were picked out. All results showed that the loss of silicon elements resulting from the deoxidization of liquid steel was not completely. It was suggested that the addition of aluminum for deoxidizing and alloying of molten steel was executed as one step in order to lower the oxygen potent... 

取向硅钢因其高磁导率、低矫顽力和大电阻系数等特性，被广泛应用于大中型变压器和大型电动机铁芯的制造。因取向硅钢性能和成分控制严格，生产工艺复杂，故其产品代表了钢铁企业特殊钢生产的最高水平。本文介绍了新钢公司卷板厂1580热连轧线生产取向硅钢过程中出现的窄尺问题，研究了取向硅钢产品的特点，分析了热轧过程中的组织转变，并结合生产实际提出了改进措施。通过对加热炉钢坯加热模式、粗轧轧制策略、精轧轧制工艺、二级模型等方面的优化和改进，取向硅钢窄尺情况明显好转，提高了产品的成材率和市场口碑。 The oriented silicon steel is widely used in the iron core manufacture of large and mediumsized transformers and large motors because of its high permeability, low coercivity and large resistance coefficient. Due to the performance and composition control of oriented silicon steel is strict, the production process is complex,therefore, its products represent the highest level of special steel production in iron and steel enterprises. This paper introduces the problem of narrow gauge in the produ... 

利用FE-SEM、EDS分析了含不同抑制剂成分的成品取向硅钢中夹杂物的组成和形貌,统计其尺寸及数量分布;结合对磁性能测试的结果,分析了Sn、Cu、Nb和Cr对取向硅钢磁性能影响的机理。结果表明:含Sn的取向硅钢试样中夹杂物主要为块状的微米级Al-Ti-C-N-O复合物,还有少量的球形Al-N-O颗粒和块状Ti-C-N-O颗粒,棒状夹杂物较少;含Cr的取向硅钢试样中夹杂物主要为球形的微米级Al2O3,还有少量Cu-Al-N-O-S复合物,棒状夹杂物和不规则夹杂物均较少;含Cr试样中1~3μm夹杂物的平均尺寸较含Sn试样小,但数量多,而大于3μm夹杂物的平均尺寸较含Sn试样大,但数量很少。磁性能测试结果表明,外场为800A/m和2500A/m时,含Cr试样磁感应强度偏低,铁损值P1.7/50较含Sn试样高,为1.171W/kg。 The composition and morphology of inclusions in the finished grain-oriented silicon steels are analyzed by using FE-SEM and EDS, and the number density and size distribution of the inclusions are counted. The influence mechanism of Sn, Cu, Nb, and Cr on the magnetic properties of the steel is also discussed. Results show that the inclusions composition in the grain-oriented silicon steel samples containing Sn is mainly block Al-Ti-C-N-O, compounding with a few spherical Al-N-O and block Ti-C-N-O... 

根据相关的取向电工钢典型专利技术,概述了日本高磁感低铁损取向电工钢低温板坯加热、抑制剂合理调节、关键成分Mn、C、Sn和Sb调节与利用、新型退火剂和绝缘溶液的制备及细化磁畴等生产工艺最新动态和进展情况,并提出了国内企业申请取向电工钢专利时应当借鉴之处。 According to related typical patent technology for grain-oriented electrical steel sheets,the recent trends and progress situation for production process of grain-oriented electrical steel sheets with high magnetic flux density and low core loss in Japan are summarized including low temperature slab heating,suitably regulating inhibitors,adjusting and utilizing key element Mn,C,Sn and Sb,manufacturing for new annealing agent and insulating solutions,and fining magnetic domain,and some suggestion... 

对低温法生产的以AlN为主抑制剂的Hi-B取向硅钢高温退火过程进行了中断实验,借助EBSD及TEM技术对高温退火连续升温过程中织构与析出物的演变进行了研究。实验结果表明,800℃时ODF图出现高斯织构组分,但强度很弱,高斯晶粒偏离角在10°以上;950~1 000℃时高斯晶粒异常长大,偏离角3~6°;高温退火过程析出物主要有球形、规则立方形及不规则多面体形3种形貌,由于渗N的影响,Zener因子先增大再减小,并且析出物在高斯晶界前沿优先粗化。 The annealing process at high temperature of Hi-B silicon steel using low slab reheat temperature and with AlN as the inhibitor has been studied by interrupting test,and the evolution of texture and precipitates during continuous heating-up in the annealing process at high temperature was analyzed by EBSD and TEM. The results showed that Goss texture appears in ODF at 800 ℃,but the intensity of Goss texture was very weak and the deviation angle was more than10°. Goss grains grow abnormally durin... 

利用EBSD技术研究了电工钢中不同的柱状晶尺寸及退火工艺下{100}织构的演变规律。结果表明,初始晶粒尺寸的影响最显著。细小柱状晶热轧后经过常化处理,组织已均匀,但中心层有强{100}织构。粗大柱状晶中{100}织构的遗传性强,常化及中间退火后,中心层仍有粗大的以{100}取向为主的晶粒;脱碳退火后才能完成组织均匀化和织构梯度的弱化。常化时的升温速度也对织构演变存在影响,低的升温速度有利于{100}织构的保留,但升温速度的影响没有初始晶粒尺寸及退火次数的影响显著。细小柱状晶样品经过热轧及三次退火工艺适合制备取向电工钢。 Evolution of {100} texture of different columnar grains and annealing process was investigated in electrical steels with the help of EBSD technique.The results show that the effect of initial grain size is the strongest.The initial fine-grained specimen shows uniform microstructure after the normalizing process,while {100} grains appear preferentially in the central layer of sheets.The heredity of {100} texture in the initial coarse-grained specimen is more significant.{100} mainly-oriented coar... 

利用X-射线衍射织构分析和线形分析技术测定了交叉轧制双取向硅钢在制备工艺各阶段的织构及微结构,进而探讨了立方织构({100}<001>)的形成过程。通过对实验结果的分析可知,二次冷轧和交叉轧制工艺为立方织构提供了内能优势和有利的形变织构,而低温预退火工艺既强化了立方织构的内能优势,又为立方织构的异常长大提供了有利的组织保证,最终在抑制剂(AlN和MnS)的协同作用下,硅钢在二次再结晶退火后形成了强烈的立方织构。 The texture and substructure of the double oriented electrical steels produced by the cross rolling technology during the difference process has been measured by means of the X-ray texture and diffraction peak profile analysis technology,and research the formation mechanism of cube texture,{100}<001>.The results show that the dominances of inner energy and deformation texture were supplied by secondary cold rolling and the cross rolling technology and strengthened by pre-annealing at a low... 

研究了CSP流程试制50W270高牌号无取向硅钢热轧→常化→冷轧→退火过程中织构的演变.利用电子背散射衍射技术对全流程织构进行测量和分析.发现热轧板织构在厚度方向上存在较大差异,表层主要为铜型、黄铜和高斯织构,1/4层存在微弱的高斯织构和旋转立方织构,中心层以γ纤维织构和旋转立方织构为主,还含有较弱的α纤维织构.与热轧板相比,常化板表层和1/4层织构变化不大,中心层旋转立方织构和α纤维织构增强.冷轧板各层均具有α纤维织构和γ纤维织构.与冷轧板相比,成品板各层中α纤维织构基本消失,还出现了立方织构和高斯织构. This article focuses on texture evolution in 50W270 high-brand non-oriented silicon steel produced by CSP in hot rolling,normalizing,cold rolling,and annealing processes.The texture in the whole process was measured and analyzed by electron back-scatter diffraction.It is found that the texture along the thickness direction in hot-rolled strips changes obviously;there are mainly copper,brass,and Goss textures in the surface layer;the 1/4 layer has weak Goss texture and rotating cube texture;γ-fib...