钢厂
冷轧产线硅钢激光高速切边实验研究
为了解决目前冷轧产线硅钢现有切边技术存在的微裂纹、应力、毛刺和边浪等问题,采用光纤激光器进行了高速切割实验,对激光功率、切割速度、激光模式等影响因素进行了分析,同时对高速切割时的切割前沿形状进行了研究。结果表明,切割最高速度随着功率的增加而增加;随着离焦量的增加,切割质量下降,挂渣增多,切缝宽度增加,切割深度变浅;基模激光器能量密度更高,所以薄板切割时的切割速度高于多模激光器;切割前沿随着切割速度的增加会变得平缓,速度足够大时,切割前沿甚至接近与切割方向平行,此时切缝下部存在挂渣现象。 In order to solve the problems such as micro crack,stress,burr,edge waves and so on,existing in cold rolling production line of silicon steel side cutting,experimentsof high speed laser cutting using fiber laser were carried out.Laser power,cutting speed,laser mode and other factors were analyzed,at the same time,cutting front geometries were studied.The results show that the maximum speed increases with power.And the increases of defocus result in poor quality,wider kerf and shallowerkerf.Energ...
热处理工艺对含Mn高硅钢热轧带的组织及硬度的影响
研究了热处理工艺(退火温度、保温时间、冷却方式)对含Mn的Fe-6.5wt%Si高硅钢热轧带的显微组织及硬度的影响。结果表明,退火温度对Fe-6.5wt%Si合金的组织和显微硬度均有较大影响,随退火温度升高,平均晶粒尺寸和显微硬度均明显增大。小于1 h退火时,晶粒长大缓慢,而长时间(>1 h)退火时,一些次表层晶粒将发生异常长大。水冷组织比空冷组织略细小,但水冷显著降低了显微硬度。Mn含量提高能抑制850℃退火时晶粒的长大,并且促进退火后高硅钢的软化。 The influences of heat treatment process(annealing temperature,heating time,cooling methods) on the microstructure and microhardness of Fe-6.5wt%Si high silicon steel containing manganese for hot rolled strip were studied.The results show that the annealing temperature has a great effect on the microstructure and microhardness of Fe-6.5wt%Si alloy,and as the annealing temperature increases,the average grain sizes and microhardness will significantly increase.When annealing time for less than 1 h...
电感耦合等离子体质谱法测定硅钢中痕量铝钼钒钛铌
研究了应用电感耦合等离子体质谱(ICP-MS)同时测定硅钢中痕量铝、钼、钒、钛、铌元素的分析方法。通过条件试验对测量参数进行了优化,确定RF功率1 400 W,泵速30rpm,采样深度140,雾化压力0.90。样品采用硝酸分解,以Be、Y混合内标校正了测量过程中高基体引起的信号漂移。根据测量时存在的质谱干扰情况,选择同位素27 Al、98 Mo、51 V、47 Ti和93 Nb作为测定同位素,同时通过调节仪器参数使得双电荷离子和氧化物离子的产率最低,以减少其带来的干扰。采用基体匹配法配制校准溶液,以标准加入法建立工作曲线,并扣除试剂空白。该方法各元素的测定下限均可达到1μg/g。用于硅钢标准样品的测定,所得结果与参考值完全吻合,各元素的RSD小于5.2%。 A method for the determination of trace aluminum,molybdenum,vanadium,titanium and niobium in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was described.A series of single parameter condition experiment was conducted.The optimized operation parameters with RF power 1 400 W,turbo pump rate 30 rpm,sampling depth 140 and nebulizer pressure 0.90 were obtained.The samples were dissolved by HNO3,and the Be and Y mixing internal standard were used to eliminate the signal drift c...
无取向硅钢铬酸镁绝缘涂层高温固化工艺
为了确保硅钢铬酸盐涂料的环保性,需要严格控制涂料的固化工艺,保证涂料固化过程中涂料中的六价铬充分转化为三价铬。对涂料及原料进行热重分析(TG)及差示扫描量热法分析(DSC)。结果表明,MgO与铬酐混合转化为MgCrO4,使六价铬稳定性增强,其中大部分Cr6+转变为Cr3+发生在620~700℃,在450~500℃高于铬酐发生大量失重,因此必须加入还原剂保证涂料中六价铬被充分还原;超过360℃后树脂会发生分解,因此实际板温不能超过360℃;加入了还原剂的整体涂料的失重温度区间主要在260~320℃,因此涂料固化时钢板的实际温度最佳区间为320~360℃。 Because of the silicon steel chromate coating’s environmental requirements,the paint curing process must be controlled strictly to ensure all Cr( Ⅵ) transforms to Cr( Ⅲ). The TG and DSC analyses of the paint are studied. The reaction of MgO and CrO3 would generate MgCrO4,enhancing the stability of Cr( Ⅵ). The most r( Ⅵ) in MgCrO4 changes to Cr( Ⅲ) at 620-700 ℃,while the CrO3 has a large weight loss at 450-500 ℃. The reductant must be added in the paint to make sure the Cr( Ⅵ) could transform suf...
冷轧大压下量下新型无取向电工钢的退火组织演变
研究了冷轧大压下量,950℃退火时间对一种新型含铜无取向电工钢晶粒度和织构的影响。结果表明,大压下量冷轧,随压下量的增加,退火晶粒向γ线聚集,形成强{111}<112>织构。提高冷轧压下率,退火织构{111}<100>,{110}<001>强度减弱,增加退火时间,退火织构{111}<110>,{100}<001>,{110}<001>强度变弱。采用87.5%冷轧压下率和950℃退火60 s,有利织构{100},{110}占有率最大。 The effect of annealing(950 ℃) time with high cold rolling reduction on grain size and texture of a new non-oriented electrical steel containing copper was investigated.The results show that for high cold rolling reduction,most annealed grains are oriented along γ-fibre with increasing cold rolling reduction ratio and strong texture {111}<112> is formed.With increasing the cold rolling reduction ratio,the intensity of annealed texture {111}<110>,{011}<100> decreases.With increa...
取向硅钢含铬无机绝缘涂层的研究进展
绝缘涂层可以有效提高硅钢片的耐蚀、耐腐、磁、绝缘等性能,因此取向硅钢涂装绝缘涂层是取向硅钢生产过程中重要的一环。本文对取向硅钢含铬无机绝缘涂层以及氮化铬涂层的性能优缺点进行了介绍,并对国内无机含铬取向硅钢绝缘涂层及氮化铬涂层的研究现状进行了综述。最后对未来含铬无机绝缘涂层的研发方向进行了展望。 Insulation coating can effectively improve the corrosion resistance of silicon steel sheet, such as corrosion, magnetic, insulation performance, thus oriented silicon steel insulation coating is the important part of oriented silicon steel production process. In this paper, the inorganic insulation coating oriented silicon steel containing chromium and chromium nitride coating performance advantages and disadvantages are introduced.In addition, the research status of insulation coating and chrom...
低温取向硅钢高温退火抑制剂的演化
取向硅钢利用析出物作为抑制剂,抑制初次再结晶晶粒的长大,抑制剂是取向硅钢发生二次再结晶的基本条件之一。文中通过低温板坯加热技术制备取向硅钢,采用透射电镜(TEM)观察并研究了高温退火阶段抑制剂的演化过程。结果表明,渗氮后形成的非晶态Si3N4析出物不稳定,在700~750℃退火升温阶段转化为(Al,Si)N;(Al,Si)N颗粒在800℃发生团聚,随后长大并粗化;(Al,Si)N是低温取向硅钢主要抑制剂,随退火温度的升高,(Al,Si)N抑制力大幅下降。 Precipitates as inhibitor are used to inhibit the grain growth of primary recrystallization in grain-oriented silicon steel,and inhibitor is one of the basic conditions for occurring of secondary recrystallization.The grain-oriented silicon steel was produced by low temperature slab heating and nitriding technique.The evolution of inhibitor was observed by transmission electron microscopy.The results show that Si3N4 particles are precipitated after nitriding,and Si3N4 particles are amorphous and...
铬、锰及退火温度对无取向硅钢组织性能影响
为探究铬、锰元素及退火温度对高强无取向硅钢性能的影响规律,借助OM、SEM、EBSD与万能拉伸试验机等分析不同制造工艺下3组不同含量铬、锰元素的无取向硅钢热轧、常化及退火处理后组织与性能。结果表明,试验钢热轧后组织不均匀,心部为沿轧向分布纤维状组织,边部为少量再结晶晶粒,常化处理能显著改善热轧板组织均匀性,消除热轧板中心部位的纤维状组织。经冷轧及退火后得到多边形铁素体晶粒,其中960℃退火,晶粒尺寸偏大,有利织构{100}组分体积分数减少,不利织构{111}组分体积分数增加,成分为0.2Mn-1Cr的1号试验钢960℃退火后铁损最大,磁感强度偏小;成分为0.5Mn-1Cr的2号试验钢930℃退火后,磁性能与强度等综合性能最佳,工频铁损P1.5/50为2.41W/kg,高频铁损P1.0/400为17.36W/kg,磁感应强度B5 000为1.638T,抗拉强度为685MPa。 In order to study the effect of Cr,Mn and annealing temperature on the properties of high-strength non-oriented silicon steel,the microstructure and properties of three groups of non-oriented silicon steel with different Cr,Mn content under different manufacturing processes were analyzed by means of OM,SEM,EBSD and universal tensile tester.The results show that the structure of experimental steel is not uniform after hot rolling,and the core is distributed in fibrous structure along the rolling ...
热轧组织对无取向硅钢织构的影响
采用X射线衍射仪分析无取向硅钢冷轧织构和再结晶退火织构的演化,研究了热轧组织对无取向硅钢织构以及磁性能的影响。结果表明,具有均匀、粗大晶粒组织的热轧板,冷轧形成更多的剪切带,导致成品板形成高的高斯织构组分,并提高了{100}织构强度,降低了γ纤维织构,最终导致成品磁感应强度升高,铁损下降。 The texture evolution of non-oriented silicon steel during cold-rolling and recrystallization annealing was investigated by X-ray diffractometer.The effects of hot band microstructure on the texture and magnetic properties of non-oriented silicon steel were analyzed.The results show that more shear bands appear during cold rolling due to homogeneous coarse grain in hot band.So strong{110}<001> texture after recrystallization annealing forms.At the same time,the {100} texture components inc...
硅钢芯片冲裁工艺分析与对策
分析了冲裁硅钢芯片时出现的质量问题,针对影响硅钢芯片冲裁质量的4大因素——人、原材料状态、工艺和工装进行了工艺试验和分析,根据原材料状态的差异,采用不同工艺方案,特别是如何合理选择冲裁模具间隙,解决了硅钢芯片冲裁时产生的主要质量问题,使冲裁的硅钢芯片达到最佳质量状态,并满足硅钢芯片的使用性能。 The problems occurred during silicon steel chip punching and the factors that affect the quality of silicon steel chip punching were analyzed,the factors include 4aspects,that is,people,raw material status,process and frock,at the same time,process tests and analysis aimed at the factors that affect punching quality were did,according to the difference of raw material status,corresponding process schedules wee taken,especially in how to reasonably select punching dies clearance,which solved the ...
冷轧无取向硅钢表面麻面缺陷成因分析及其控制措施
针对某厂DMS森吉米尔轧机生产无取向硅钢表面麻面缺陷的问题,根据生产实际,对其形成原因从乳化液及工作辊两方面因素进行了分析。结果表明:乳化液对麻面缺陷的产生有一定影响,但不是主要因素,主要原因是由于二十辊森吉米尔轧机工作辊辊径较小,轧制相同长度带钢轧辊运转周期较大,容易产生疲劳失效而导致。为此,提出通过调整冷轧工序成品轧制道次的压下率以减小轧制力,从而减小工作辊的磨损疲劳;通过对轧制乳化液浓度、温度的合理控制,以改善润滑效果、提高轧制速度,而进一步缓解轧辊疲劳的改进措施,使该钢厂无取向硅钢麻面缺陷发生率由原来的18%降至0.8%,带钢表面质量明显改善。 For the problem of surface pockmarks of non-oriented silicon steel strip produced by a DMS Sendzimir mill, based on the production practice, the formation causes were analyzed from two aspects of emulsion and working roll. The results show that the emulsion has a certain effect on the formation of surface pockmarks defects, but it is not the main factor. The main reason is that the working roll diameter of the 20-high Sendzimir mill is small, and the running period of the roll rolling the same l...

