钢厂
0.3 mm厚的高强无取向电工钢的退火组织与性能
借助光学显微镜、扫描电镜、交流磁性能测量仪和万能拉伸试验机研究了0.3 mm厚高强无取向电工钢冷轧板在780、820、860和900℃退火保温2 min后的组织、织构和性能。结果表明:在退火温度范围内,试验钢均发生了完全再结晶,得到等轴状的铁素体晶粒;随着退火温度的升高,平均晶粒尺寸从9.2μm增长到41.3μm,工频铁损和400 Hz高频铁损均先大幅减小后趋于平缓,磁感应强度先升高后降低。在820℃退火时,铁损P1.5/50=5.51 W/kg,P1.0/400=33.22 W/kg均处于较低值,磁感应强度B5000最大,为1.649 T。试验钢的屈服强度和抗拉强度均随退火温度的升高而降低,780℃退火时屈服强度为496 MPa, 900℃退火时降低至407 MPa。综合磁性能和力学性能考虑,试验钢的最佳退火温度是820℃。 Microstructure, texture and properties of 0.3 mm thick high strength non-oriented electrical steel cold rolled sheet annealed at 780 ℃, 820 ℃, 860 ℃ and 900 ℃ for 2 min were studied by means of optical microscope, scanning electron microscopy, AC magnetic property tester and universal tensile testing machine. The results show that in the annealing temperature range, complete recrystallization of the experimental steel occurs and equiaxed ferrite grains are obtained. With the increase of annealin...
铜含量对TSCR工艺生产取向硅钢热轧织构的影响
取向硅钢热轧板中织构梯度对发展完善的二次再结晶十分关键,通过添加铜可以显著降低取向硅钢板坯加热温度,从而影响热轧板织构分布。利用X射线衍射仪,分析了实验室模拟薄板坯连铸连轧(TSCR)工艺的3种不同铜含量的取向硅钢热轧板织构。结果表明:不同铜含量热轧板表面到厚度1/4处均为弱的热轧织构,热轧板心部主要为{100}面织构;铜含量约在0.4%时,热轧板次表层的{110}<001>织构比例最高,而热轧板心部的{100}<110>织构比例最低;铜含量对热轧织构中{114}<110>和{001}<100>织构发展有显著影响。 The texture gradient in hot rolled grain oriented silicon steel strip is one of the essential factors to achieve a perfect secondary recrystallization.The addition of copper can significantly reduce the slab reheating temperature of grain oriented silicon steel,so as to impact the texture distribution in the hot rolled strip.The texture of hot rolled grain oriented silicon steel strip as-rolled by thin slab casting and rolling process(TSCR) in laboratory with three different copper contents was ...
辉光放电发射光谱法测定电工钢中8种元素
通过对辉光放电发射光谱法分析电工钢样品光谱行为的研究,分析其工作参数如:电压、电流、预溅射时间和积分时间对光谱强度和稳定性的影响,并以铁为内标元素,优化了工作参数。确定了直流辉光放电光谱法测定电工钢中碳、硅、锰、磷、硫、铬、镍、铜共8种元素的定量分析方法,并对该方法分析的精密度和准确度进行验证,结果表明,各元素的测定结果与认定值和其他方法测定值一致,测量元素结果RSD值小于2%。 Based on research on analyzing the spectrum behavior of the sample taken from the electrical steel by glow discharge optical emission spectrometry,the effect of its operational parameters such as current,voltage,pre-sputtering time and integrating time on the spectral intensity and spectral stability is analyzed.Taking the Fe as an element applied by internal standard method,these operational parameters are optimized,and therefore the quantitative analysis method for testing eight kinds of eleme...
CSP工艺生产无取向电工钢
介绍了CSP工艺生产无取向电工钢各工序的设备特点、采用的工艺控制手段和电工钢产品质量情况,结合生产实践证明了马钢CSP工艺开发的无取向电工钢产品丰富了薄板坯连铸连轧的品种结构,发挥了薄板坯连铸连轧生产无取向电工钢性能均一、稳定的特点。 The equipment characteristic,the process control method and the quality of non-orientated silicon steel by CSP process were introduced.Combined with the production situation,it is proved that production of non-orientated silicon steel developed on Masteel CSP line would enrich product structure of thin slab continuous casting and rolling,and it exerts stable performance of non-orientated silicon steel.
钇元素对6.5%Si无取向硅钢组织、高温拉伸及断裂机制的影响
通过微观组织表征、高温拉伸和断口形貌分析,研究了钇(Y)元素对6.5%Si无取向硅钢组织、高温拉伸及断裂机制的影响。研究结果表明,添加Y元素可以在钢液中形成YS和YP的复合析出。YS和YP可以充当异质形核基底,提高形核率,细化凝固组织。热轧组织不均匀,由表层至芯部分别形成等轴晶、等轴晶/拉长晶和拉长晶的混合组织。退火后,热轧变形组织转变为等轴晶,含Y实验钢的退火组织得到明显细化。500℃时效处理后,含Y实验钢具备较低的有序度,300℃的拉伸断口呈现韧性断裂特征,断后伸长率达到20.2%。相反,无Y实验钢发生脆性断裂,断后伸长率仅为2.1%。研究结果证实,Y元素可以通过组织细化和降低有序度提高6.5%Si无取向硅钢的中温塑性。 The effects of yttrium(Y)on microstructure,elevated-temperature tensile properties and fracture mechanism of 6.5% Si non-oriented electrical steel were investigated by means of microstructure characterization,high-temperature tensile test and fracture analysis.The results showed that the doping of Y introduced composite Y-rich precipitates(YS/YP)in the melt.YS and YP precipitates were qualified for heterogeneous nucleation agents,which thus raised the nucleation rate and refined the solidificati...
电工钢显微结构和疲劳性能的研究
研究了电工钢SXRC的显微结构和疲劳性能,并与DP钢进行了比较。结果表明,退火温度低温化能够有效的抑制电工钢的再结晶。该钢在固溶铌的作用下,能够在保证电机磁性的同时具有一定的强度。与DP钢相比,SXRC钢的抗疲劳性能更好。 The microstructures and fatigue properties of the electrical steel SXRC we re investigated, and the properties were also compared with the steel DP. The results show that the recrystallization of the electrical steel can be suppressed at lower annealing temperature. The steel presents favorable motor magnetic and also a compatible strength with the help of solid-solution Nb. Compared with the steel DP, the fatigue resistance of the steel SXRC is preferable.
二次冷轧的中间退火温度对2.3Si无取向硅钢组织和性能的影响
试验2.3Si无取向硅钢(/%:0.003C,2.30Si,0.16Mn,≤0.020P,≤0.005S,0.54Al)冷轧板由常化和未常化的2.5 mm热轧板冷轧至0.6 mm(压下率76%),经750~950℃2.5 min中间退火后再冷轧至0.5 mm(压下率16.7%),成品板经890℃+960℃2.5 min退火。研究了中间退火温度对该钢晶粒尺寸、织构和磁性能的影响。结果表明,随中间退火温度的升高,二次冷轧前晶粒和成品晶粒增大,成品中不利织构组分{111}和{112}减弱,磁性能得到改善。热轧板经过常化时的磁性能明显好于未经常化时的磁性能,但中间退火温度较高时常化对磁性能的有利作用减弱。 The test cold sheet of 2.3Si non-oriented silicon steel(/%:0.003C,2.30Si,0.16Mn,≤0.020P,≤0.005S,0.54Al) is first cold-rolled from normalized and un-normalizing 2.5 mm hot-rolled plate to 0.6 mm sheet(reduction 76%),then intermediate annealed at 750~950℃ for 2.5 min and double cold-rolled to 0.5 mm sheet(reduction16.7%),the finished sheet annealed at 890℃+960℃ for 2.5 min.Effect of the intermediate annealing temperature on grain size,texture and magnetic performance of the steel has been studied....
取向硅钢生产工艺技术分析和发展趋势
介绍了普通取向硅钢(CGO)和高磁感取向硅钢(Hi-B)铸坯高温加热两次冷轧、一次冷轧和铸坯低温加热两次冷轧、一次冷轧法4种成熟生产工艺的主要技术参数,取向硅钢理论研究(Goss晶核和抑制剂)和生产技术现状。取向钢的发展趋势为:提高(110)[001]晶粒取向度,降低取向硅钢铁损,发展铸坯低温加热(≤1 300℃)和薄板坯连铸连轧流程生产取向硅钢工艺。 Main technology parameters of four developed process:cast bloom higher temperature heating-double cold rolling or single cold rolling,lower temperature heating-double cold rolling or single rolling process for production of common grain oriented silicon steel(CGO) and high magnetic induction grain oriented silicon steel(Hi-B),theory research on grain oriented steel(Goss nucleus and inhibitor) and present situation of process are summarized in this paper.The development trend of grain oriented si...
冷轧大压下量下新型无取向电工钢的退火组织演变
研究了冷轧大压下量,950℃退火时间对一种新型含铜无取向电工钢晶粒度和织构的影响。结果表明,大压下量冷轧,随压下量的增加,退火晶粒向γ线聚集,形成强{111}<112>织构。提高冷轧压下率,退火织构{111}<100>,{110}<001>强度减弱,增加退火时间,退火织构{111}<110>,{100}<001>,{110}<001>强度变弱。采用87.5%冷轧压下率和950℃退火60 s,有利织构{100},{110}占有率最大。 The effect of annealing(950 ℃) time with high cold rolling reduction on grain size and texture of a new non-oriented electrical steel containing copper was investigated.The results show that for high cold rolling reduction,most annealed grains are oriented along γ-fibre with increasing cold rolling reduction ratio and strong texture {111}<112> is formed.With increasing the cold rolling reduction ratio,the intensity of annealed texture {111}<110>,{011}<100> decreases.With increa...
低温取向硅钢热轧析出物与织构的研究
采用低温板坯加热制备取向硅钢,通过透射电镜(TEM)观察并研究热轧板中的析出物,用ODF织构法研究热轧板距表面1/8、1/4和1/2处的织构分布。结果表明,热轧板中的析出物主要是密排六方AlN,AlN形貌呈规则长方形,AlN颗粒大小不等,分布密度低;热轧板中的织构沿板厚方向,由亚表层的{110}<001>织构向1/2中心层的α线织构变化,其中{110}<001>织构在热轧板距表面1/4层处最强。 The low temperature grain-oriented silicon steels were produced by acquired inhibitor method.The precipitates in hot rolling strip were observed and studied by transmission electron microscope,and the texture distribution in 1/8,1/4 and 1/2 layers of hot rolling strip were analyzed by ODF method.The results showed that the square shaped h-AlN is the main precipitates in hot rolling strip.The precipitates are varying in size and distribution.The texture of hot rolling strip in thick direction are...
两段式正火对含Sb冷轧无取向电工钢磁性能的影响
利用OM、EBSD等手段研究了热轧板两段式正火时在700℃保温不同时间(0、10、30、60 min)对含Sb冷轧无取向电工钢磁性能的影响。结果表明,700℃保温10 min处理的样品铁损最小,磁感最高。对成品板的组织分析结果表明,试样的晶粒尺寸随700℃保温时间的延长先增大后减小,保温10 min时晶粒尺寸达到最大;分析成品试样织构发现,有利织构组分随700℃保温时间的延长先增加后减少,保温10 min时有利织构组分所占百分比最高。因此,含Sb冷轧无取向电工钢两段式正火时在700℃保温10 min时磁性能最好。 Effect of two-stage normalization on magnetic property of non-oriented electrical steel containing antimony was investigated by using optical microscope(OM) and electron back-scattered diffraction technology(EBSD).The experimental results show that the iron loss and magnetic permeability of the specimen insulated at 700 ℃ for 10 min are lowest and highest respectively.The grain size of the finish specimens increases first and then decreases with the increase of holding time.Similarly,the advanta...

