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研究了应用电感耦合等离子体质谱法(ICP-MS)测定硅钢中痕量铜和镍的分析方法。采用硝酸分解样品,通过内标校正和基体匹配消除了基体干扰的影响,同时根据测量时存在的质谱干扰情况,选择同位素65Cu和60Ni作为测定元素和通过调节仪器参数使双电荷离子的产率最低,以减少带来的干扰。该方法用于硅钢中痕量铜和镍的测定,所得的结果与ICP-AES法测定结果完全吻合,各元素测定结果的RSD值小于5%,加标回收率为97.3%~100.3%。 A method for the determination trace copper and nickel in silicon steel by inductively coupled plasma mass spectrometry(ICP-MS) was studied.The samples were dissolved in HNO3.The effect of matrix interference was eliminated by internal standard correction and matrix matching.Meanwhile,according to the mass spectral interferences in determination,the isotopes including 65Cu and 60Ni were used as measuring elements.The yield of double-charge ions were minimized by adjusting instrumental parameters... 
2011-05-28 173 5.8

【作者】 康凌晨; 王丽娜; ...
2014-05-28 141 5.8

【摘要】 <正>10月9日至11日,武钢一硅钢技术改造工...
2011-06-28 134 5.8

本实用新型公开了一种能限位的硅钢片,包括主体,主体的上表面设置有限位柱,限位柱的轴心处开设有散热孔,主体的上表面开设有限位槽,主体的外壁设置有凹槽,主体的下表面设置有限位凸起,主体的下表面开设有限位孔;该一种能限位的硅钢片通过在主体的外壁设置凹槽可以方便拿取,在其上下表面分别设置限位柱与限位孔,可以使主体间的位置相对固定不会轻易挪动。
2021-08-23 164 6.8

一种无取向电磁钢板用热轧钢板,其以质量%计,含有C:0.0010~0.0050%、Si:1.90%~3.50%、Al:0.10%~3.00%、Mn:0.05~2.00%、P:0.100%以下、S:0.005%以下、N:0.0040%以下、B:0.0060%以下、Sn:0~0.50%、Sb:0~0.50%、Cu:0~0.50%、REM:0~0.0400%、Ca:0~0.0400%及Mg:0~0.0400%,剩余部分为Fe及杂质;该无取向电磁钢板用热轧钢板的特征在于,在无取向电磁钢板用热轧钢板的板宽方向端部中,板厚中心部(t/2位置)的加工组织的硬度HD为Hv220以下。
2021-02-19 134 6.8

近年来,在节能减排背景之下,国内外众多研究者对无取向电工钢磁性能的提升做了大量研究。为了探索无取向电工钢磁性能提升的方法,对锡或锑对无取向电工钢磁性能的作用机制(晶粒尺寸和晶体织构的控制)进行分析。基于该作用机制,介绍锡或锑的添加对无取向电工钢磁性能的影响。经研究发现,适量的锡或锑在晶界偏聚,不会阻碍晶界的移动并且致使晶粒尺寸降低;与此同时,锡或锑在晶界偏聚不仅抑制{111}织构在原始晶界处形核及生长,还降低(100)晶粒表面能,促进(100)晶粒生长。因此,适量添加锡或锑,可使无取向电工钢铁损下降、磁感提升。最后结合生产工艺,建议无取向电工钢的研究方向应为稀土含量对高牌号无取向硅钢夹杂物尺寸和数量分布的影响,锡或锑的添加量和常化工艺参数(常化时间、常化温度)对常化晶粒尺寸的影响。 In recent years, due to the background of energy saving and emission reduction, numerous researchers all around the world have done a lot of investigations on the improvement of magnetic properties for non-oriented electrical steel. In order to explore the method of improving the magnetic properties of non-oriented electrical steel, the mechanism of tin or antimony on the magnetic properties(the control of grain size and crystallographic texture) of non-oriented electrical steel is illuminated. ... 
2022-05-28 208 5.8

采用自主研发的脉冲磁场退火装置,在取向硅钢脱碳退火过程中分别施加不同强度的磁场,并采用光学显微镜和X射线衍射仪研究了脉冲磁场脱碳退火后试样的显微组织和宏观织构。结果表明,脱碳退火过程中施加脉冲磁场后取向硅钢的平均晶粒尺寸均增加,当磁场强度为40 mT时,平均晶粒尺寸最大,为13.06μm。此外,取向硅钢试样的立方织构{001}<100>强度减弱,高斯织构{110}<001>和{111}<112>织构增强,有利于获得更好的成品织构和磁性能。 Self-developed pulsed magnetic field annealing device was used to apply magnetic field of different intensities during decarburization annealing of an oriented silicon steel, and microstructure and macro-texture of the specimens after decarburization annealing in a pulsed magnetic field were studied by using optical microscope and X-ray diffractometer. The results show that the average grain size of the oriented silicon steel increases with the application of pulsed magnetic field during decarbu... 
2022-02-28 194 5.8

综述了退火温度、时间对无取向电工钢磁性的影响。退火温度主要影响无取向电工钢不同织构的占有率,退火时间主要影响晶粒尺寸的大小,晶粒尺寸的变化对织构的形成也有一定的影响。磁感最高点出现在纤维组织完全消失,(111)面织构组分较弱的组织状态。铁损的降低主要依赖于磁滞损耗的降低,织构的影响不大。 The effects of annealing temperature and time on the non-oriented electrical steel magnetic properties were reviewed.Annealing temperature and time mainly affects the different textures share and the grain sizes of non-oriented electrical steel respectively.Changes of the grain sizes also have a certain effect on textures formation.The highest point of the magnetic induction value in the fibrous tissue completely disappears and{111} plane texture has a lower state of the component content.Iron l... 
2013-10-28 151 5.8

本发明公开了一种高牌号硅钢的穿带激光焊接方法,包括:将焊缝中硅含量降低到Si焊<1.9%。采用激光+填丝焊接,填丝ER50‑6碳钢焊丝;根据焊缝截面积和激光焊接速度;激光填丝焊接时,激光线能量应足够大,达到填丝在熔池中充分混合,均匀分布,不至于填丝的成分浮在熔池的上半部分。采用此方法使焊缝组织从粗大铁素体变成细小、致密的无碳贝氏体,晶内沉淀相和晶间脆性相相对大幅减少,提高了焊缝韧性和成形性能,保证了高硅硅钢带的穿带焊接和连续生产。
2021-05-12 150 6.8

采用扫描电镜、场发射扫描电镜、能谱仪等对50SW1300冷轧无取向硅钢中的夹杂物分不同尺寸区间进行数量统计,利用主成分回归分析法,即数据的标准化处理—主成分分析—回归分析—标准化的变量还原成原始变量—确定显著影响因素,综合分析夹杂物总量及各尺寸区间的夹杂物数量对无取向硅钢磁性能的影响。结果表明:主成分回归分析能够从夹杂物尺寸区间及数量的多个影响因素中提取主要的因素,定量研究其对磁性能的影响。分析表明,显著影响无取向硅钢铁损的夹杂物为100~500nm的AlN、AlN+MnS、MnS、Al2O3、AlN+Al2O3,而劣化磁感最明显的夹杂物尺寸区间为100~200nm。 Different size intervals of inclusions in cold rolled non-oriented silicon steel 50SW1300 were counted by scanning electron microscope(SEM),field emission scanning electron microscope(FESEM)and energy disperse spectroscopy(EDS).With principal component regression method:standardization for experimental data,principal component analysis,regression analysis,transform standardized variables into original variables,determination of significant factor,effects of the total number of inclusions and the... 
2014-10-28 204 5.8

本发明公开了一种酸洗低牌号无取向硅钢的方法,从酸洗线前拉矫机的延伸率设定、酸液浓度、酸液温度、酸洗槽内液位的控制、酸液中铁离子的含量等方面入手,解决酸洗低牌号无取向硅钢的问题。
2021-01-13 158 6.8

【作者】 O.M.Гбанов; A.E.Чеглов; ...
2014-03-28 115 5.8

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